Assessment of Mechanical Properties and Biocompatibility of Pellethane®

1982 ◽  
Vol 5 (3) ◽  
pp. 191-194 ◽  
Author(s):  
F.D. Biester ◽  
D.M. Behrend ◽  
H. Klinkmann
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Uniaxial Tension ◽  
Modulus Of Elasticity ◽  
Dynamic Modulus ◽  
Elongation At Break ◽  
X Ray ◽  
Effective Combination ◽  
High Degree

Pellethane® CPR 2363-80A nonreinforced (PUR), nonreinforced and twice sterilized (PUR F2), reinforced with Dacron® (Dm), Grisuten® (DG) and glassfibre (PUG) and fabricated under different conditions have been examinated. Tests included uniaxial tension at 310 K, torsional movement from 293 to 319 K, X-ray structure, SEM, visual surface clotting, thrombocyte adhesion and degree of albumenisation. Typical in vitro results were: modulus of elasticity E [MPa] (PUR: 1.33, Dm: 4.22, DG: 1.86, PUG: 622.5), tensile strength δB [MPa] (43.4, 12.5, 21.7, 24.9), elongation at break δ [%] (1122, 109, 660, 479), dynamic modulus of sliding G', G” [MPa] at 293 K (8.7, 0.4/ 15.9, 0.9/ 12.1, 1.3/ 17.1, 1.5), damping tanδ (0.13, 0.1, 0.16, 0.12), orientational degree at 5% elongation fx [%] (PUR: 0.5), low thrombogenicity and high degree of albumenisation. The results indicate a strong dependency of mechanical and biocompatibility properties on membrane and housing fabrication. The most effective combination is a thin PUR membrane and a PUG housing fabricated under special conditions.

scholarly journals Structure, Composition, and Mechanical Properties of Australian Orthodontic Wires

2009 ◽  
Vol 79 (1) ◽  
pp. 97-101 ◽  
Author(s):  
Brian M. Pelsue ◽  
Spiros Zinelis ◽  
T. Gerard Bradley ◽  
David W. Berzins ◽  
Theodore Eliades ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Vickers Hardness ◽  
Modulus Of Elasticity ◽  
Sem Analysis ◽  
Orthodontic Wires ◽  
Vickers Hardness Number ◽  
X Ray ◽  
Level Of Significance ◽  
Lower Tensile Strength

Abstract Objective: To investigate the surface morphology, structure, elemental composition, and key mechanical properties of various sizes and tempers of Australian wires. Materials and Methods: Three types of Australian wire were used: 0.016″ regular, 0.018″ regular+, and 0.018″ special+ (A.J. Wilcock, Whittlesea, Victoria, Australia). Each type of wire was subjected to scanning electron microscopy (SEM) analysis, x-ray energy dispersive spectroscopy (EDS) investigation, Vickers hardness testing, and tensile testing. The modulus of elasticity and ultimate tensile strength were determined. Hardness, modulus, and strength data were analyzed with one-way analysis of variance (ANOVA) and Tukey testing at the .05 level of significance. Results: All three types of Australian wire were found to possess considerably rough surfaces with striations, irregularities, and excessive porosity. All three wire types had high levels of carbon and a similar hardness, which ranged within 600 VHN (Vickers hardness number), and a similar modulus of elasticity (173 to 177 GPa). The 0.018″ special+ had a significantly lower tensile strength (1632 MPa) than the 0.016″ regular and the 0.018″ regular+ wire (2100 MPa). Conclusions: Australian wires did not show variation implied by the size or temper of the wires.

Study the Effect of the Addition of HAp from Crocodile Bones on the Mechanical Properties of PLA/HAp Composites

2013 ◽  
Vol 834-836 ◽  
pp. 237-240 ◽  
Author(s):  
Kanyakorn Pawarangkool ◽  
Wirunya Keawwattana
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Impact Strength ◽  
Thermal Process ◽  
Weight Ratio ◽  
Melt Blending ◽  
Elongation At Break ◽  
X Ray ◽  
Infrared Spectrometer ◽  
Scanning Electron

In this work, hydroxyapatite (HAp) was produced from crocodile bones by thermal process at 900°C. X-ray diffractometer (XRD), Fourier transform infrared spectrometer (FTIR) and Scanning electron microscope (SEM) were used to characterize the obtained HAp. Polylactic acid (PLA)/HAp composites were prepared by melt blending as follows: 95/5, 90/10 and 85/15 (weight ratio). The effect of the amount of HAp on the mechanical properties including tensile strength, modulus, elongation at break and impact strength of PLA/HAp composites was undertaken. It was found that tensile strength and elongation at break of the composites decreased with an increase of HAp content, while modulus and impact strength showed no significant effect.

Mechanical Properties of TPNR-MWNTs-OMMT Hybrid Nanocomposites

2012 ◽  
Vol 501 ◽  
pp. 194-198 ◽  
Author(s):  
Mou'ad A. Tarawneh ◽  
Sahrim H. Ahmad ◽  
A.R. Shamsul Bahri ◽  
Yu Lih Jiun
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Aspect Ratio ◽  
Interfacial Adhesion ◽  
Hybrid Nanocomposites ◽  
X Ray Diffraction ◽  
Elongation At Break ◽  
X Ray ◽  
Maximum Value ◽  
The Matrix

This paper discusses the processing of a hybrid of TPNR-MWNTs-OMMT nanocomposites with different percentages of filler to determine the optimum mechanical properties of the hybrid nanocomposites. Three types of hybrid nanocomposites with various MWNTs-OMMT compositions (1%wt MWNTs+3%wt OMMT), (2%wt MWNTs+2%wt OMMT) and (3%wt MWNTs+1%wt OMMT) were prepared. The OMMT layers were found to be separated further with higher nanotubes content as exhibited by X-ray diffraction. The result of tensile test showed that tensile strength and Young's modulus increase in the presence of nanotubes and maximum value were obtained for the nanocomposites with highest nanotubes (3%wt) which increased about 33% and 36%, respectively compared with pure TPNR matrix. On other hand, the elongation at break considerably decreased with increasing the percentage of MWNTs. TEM micrographs revealed aspect ratio and fillers orientation in the TPNR matrix also promoted strongly to interfacial adhesion between fillers and the matrix which contributed significantly to the improvement of the mechanical properties

Phase Transformations in Ti-7w/oMo-3w/oMe Alloy

1974 ◽  
Vol 32 ◽  
pp. 514-515
Author(s):  
S. Fujishiro
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Transmission Electron Microscopy ◽  
Tensile Strength ◽  
Mechanical Processing ◽  
Ray Method ◽  
X Ray ◽  
Transmission Electron ◽  
Water Quench ◽  
Alpha Beta

The mechanical properties of three titanium alloys (Ti-7Mo-3Al, Ti-7Mo- 3Cu and Ti-7Mo-3Ta) were evaluated as function of: 1) Solutionizing in the beta field and aging, 2) Thermal Mechanical Processing in the beta field and aging, 3) Solutionizing in the alpha + beta field and aging. The samples were isothermally aged in the temperature range 300° to 700*C for 4 to 24 hours, followed by a water quench. Transmission electron microscopy and X-ray method were used to identify the phase formed. All three alloys solutionized at 1050°C (beta field) transformed to martensitic alpha (alpha prime) upon being water quenched. Despite this heavily strained alpha prime, which is characterized by microtwins the tensile strength of the as-quenched alloys is relatively low and the elongation is as high as 30%.

scholarly journals The Structure and Mechanical Properties of Hemp Fibers-Reinforced Poly(ε-Caprolactone) Composites Modified by Electron Beam Irradiation

2021 ◽  
Vol 11 (12) ◽  
pp. 5317
Author(s):  
Rafał Malinowski ◽  
Aneta Raszkowska-Kaczor ◽  
Krzysztof Moraczewski ◽  
Wojciech Głuszewski ◽  
Volodymyr Krasinskyi ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Electron Beam ◽  
Impact Strength ◽  
Flexural Modulus ◽  
Natural Fibers ◽  
High Energy ◽  
Electron Radiation ◽  
Elongation At Break ◽  
Hemp Fibers

The need for the development of new biodegradable materials and modification of the properties the current ones possess has essentially increased in recent years. The aim of this study was the comparison of changes occurring in poly(ε-caprolactone) (PCL) due to its modification by high-energy electron beam derived from a linear electron accelerator, as well as the addition of natural fibers in the form of cut hemp fibers. Changes to the fibers structure in the obtained composites and the geometrical surface structure of sample fractures with the use of scanning electron microscopy were investigated. Moreover, the mechanical properties were examined, including tensile strength, elongation at break, flexural modulus and impact strength of the modified PCL. It was found that PCL, modified with hemp fibers and/or electron radiation, exhibited enhanced flexural modulus but the elongation at break and impact strength decreased. Depending on the electron radiation dose and the hemp fibers content, tensile strength decreased or increased. It was also found that hemp fibers caused greater changes to the mechanical properties of PCL than electron radiation. The prepared composites exhibited uniform distribution of the dispersed phase in the polymer matrix and adequate adhesion at the interface between the two components.

scholarly journals Effect of Moisture Content on the Processing and Mechanical Properties of a Biodegradable Polyester

Polymers ◽  
2021 ◽  
Vol 13 (10) ◽  
pp. 1616
Author(s):  
Vincenzo Titone ◽  
Antonio Correnti ◽  
Francesco Paolo La Mantia
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Moisture Content ◽  
Mechanical Testing ◽  
Hydrolytic Degradation ◽  
Slight Reduction ◽  
Biodegradable Polyester ◽  
Molding Process ◽  
Elongation At Break ◽  
Effect Of Moisture

This work is focused on the influence of moisture content on the processing and mechanical properties of a biodegradable polyester used for applications in injection molding. The pellets of the biodegradable polyester were exposed under different relative humidity conditions at a constant temperature before being compression molded. The compression-molded specimens were again placed under the above conditions before the mechanical testing. With all these samples, it is possible to determine the effect of moisture content on the processing and mechanical properties separately, as well as the combined effect of moisture content on the mechanical properties. The results obtained showed that the amount of absorbed water—both before processing and before mechanical testing—causes an increase in elongation at break and a slight reduction of the elastic modulus and tensile strength. These changes have been associated with possible hydrolytic degradation during the compression molding process and, in particular, with the plasticizing action of the moisture absorbed by the specimens.

scholarly journals Roller Compacted Concrete with Recycled Concrete Aggregate for Paving Bases

2020 ◽  
Vol 12 (8) ◽  
pp. 3154 ◽  
Author(s):  
Hedelvan Emerson Fardin ◽  
Adriana Goulart dos Santos
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Modulus Of Elasticity ◽  
Splitting Tensile Strength ◽  
Recycled Concrete ◽  
Concrete Aggregate ◽  
Recycled Concrete Aggregate ◽  
Roller Compacted Concrete ◽  
Flexural Tensile Strength ◽  
Mechanical And Physical Properties

This research aimed to investigate the mechanical and physical properties of Roller Compacted Concrete (RCC) used with Recycled Concrete Aggregate (RCA) as a replacement for natural coarse aggregate. The maximum dry density method was adopted to prepare RCC mixtures with 200 kg/m³ of cement content and coarse natural aggregates in the concrete mixture. Four RCC mixtures were produced from different RCA incorporation ratios (0%, 5%, 15%, and 30%). The compaction test, compressive strength, splitting tensile strength, flexural tensile strength, and modulus of elasticity, porosity, density, and water absorption tests were performed to analyze the mechanical and physical properties of the mixtures. One-way Analysis of Variance (ANOVA) was used to identify the influences of RCA on RCC’s mechanical properties. As RCA increased in mixtures, some mechanical properties were observed to decrease, such as modulus of elasticity, but the same was not observed in the splitting tensile strength. All RCCs displayed compressive strength greater than 15.0 MPa at 28 days, splitting tensile strength above 1.9 MPa, flexural tensile strength above 2.9 MPa, and modulus of elasticity above 19.0 GPa. According to Brazilian standards, the RCA added to RCC could be used for base layers.

Effect of Castor Oil Impregnation on the Physical and Mechanical Properties of Bacterial Cellulose

2012 ◽  
Vol 3 (1) ◽  
pp. 13-26
Author(s):  
Myrtha Karina ◽  
Lucia Indrarti ◽  
Rike Yudianti ◽  
Indriyati
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Bacterial Cellulose ◽  
Young’S Modulus ◽  
Castor Oil ◽  
Young's Modulus ◽  
Physical And Mechanical Properties ◽  
Scanning Electron Micrographs ◽  
Elongation At Break ◽  
Acetone Water

The effect of castor oil on the physical and mechanical properties of bacterial cellulose is described. Bacterial cellulose (BC) was impregnated with 0.5–2% (w/v) castor oil (CO) in acetone–water, providing BCCO films. Scanning electron micrographs revealed that the castor oil penetrated the pores of the bacterial cellulose, resulting in a smoother morphology and enhanced hydrophilicity. Castor oil caused a slight change in crystallinity indices and resulted in reduced tensile strength and Young's modulus but increased elongation at break. A significant reduction in tensile strength and Young's modulus was achieved in BCCO films with 2% castor oil, and there was an improvement in elongation at break and hydrophilicity. Impregnation with castor oil, a biodegradable and safe plasticiser, resulted in less rigid and more ductile composites.

Graphite/Bio-Based Epoxy Composites: The Mechanical Properties Interface

2015 ◽  
Vol 799-800 ◽  
pp. 115-119 ◽  
Author(s):  
Anika Zafiah M. Rus ◽  
Nur Munirah Abdullah ◽  
M.F.L. Abdullah ◽  
M. Izzul Faiz Idris
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Elastic Modulus ◽  
Filler Content ◽  
Weight Percent ◽  
Epoxy Composites ◽  
Elongation At Break ◽  
Graphite Content ◽  
Dispersion Condition ◽  
Strong Interfacial Bonding

Graphite reinforced bio-based epoxy composites with different particulate fractions of graphite were investigated for mechanical properties such as tensile strength, elastic modulus and elongation at break. The graphite content was varied from 5 wt.%, 10 wt.%, 15 wt.%, 20 wt.%, 25 wt.%, 30 wt.% by weight percent in the composites. The results showed that the mechanical properties of the composites mainly depend on dispersion condition of the treated graphite filler, aggregate structure and strong interfacial bonding between treated graphite in the bio-based epoxy matrix. The composites showed improved tensile strength and elastic modulus with increase treated graphite weight loading. This also revealed the composites with increasing filler content was decreasing the elongation at break.

scholarly journals Fabrication and Characterization of Electrospun Polycaprolactone Blended with Chitosan-Gelatin Complex Nanofibrous Mats

2014 ◽  
Vol 2014 ◽  
pp. 1-7 ◽  
Author(s):  
Yongfang Qian ◽  
Zhen Zhang ◽  
Laijiu Zheng ◽  
Ruoyuan Song ◽  
Yuping Zhao
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Weight Ratio ◽  
Degree Of Crystallinity ◽  
X Ray Diffraction ◽  
Tissue Engineering Scaffolds ◽  
Elongation At Break ◽  
Nanofibrous Scaffolds ◽  
Two Peaks

Design and fabrication of nanofibrous scaffolds should mimic the native extracellular matrix. This study is aimed at investigating electrospinning of polycaprolactone (PCL) blended with chitosan-gelatin complex. The morphologies were observed from scanning electron microscope. As-spun blended mats had thinner fibers than pure PCL. X-ray diffraction was used to analyze the degree of crystallinity. The intensity at two peaks at 2θof 21° and 23.5° gradually decreased with the percentage of chitosan-gelatin complex increasing. Moreover, incorporation of the complex could obviously improve the hydrophilicity of as-spun blended mats. Mechanical properties of as-spun nanofibrous mats were also tested. The elongation at break of fibrous mats increased with the PCL content increasing and the ultimate tensile strength varied with different weight ratios. The as-spun mats had higher tensile strength when the weight ratio of PCL to CS-Gel was 75/25 compared to pure PCL. Both as-spun PCL scaffolds and PCL/CS-Gel scaffolds supported the proliferation of porcine iliac endothelial cells, and PCL/CS-Gel had better cell viability than pure PCL. Therefore, electrospun PCL/Chitosan-gelatin nanofibrous mats with weight ratio of 75/25 have better hydrophilicity mechanical properties, and cell proliferation and thus would be a promising candidate for tissue engineering scaffolds.

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