scholarly journals TECHNOLOGICAL AND ANALYTICAL STUDY OF THE WATER EXTRACTS FROM THE LEAVES OF LINGONBERRY

2017 ◽  
Vol 25 (2) ◽  
pp. 296-302
Author(s):  
N. G. Selezenev ◽  
A. N. Nikolashkin ◽  
S. V. Dobina
Keyword(s):  
Aqueous Extract ◽  
Analytical Study ◽  
Ph Value ◽  
Raw Materials ◽  
Water Extract ◽  
Water Extracts ◽  
Plant Raw Materials ◽  
Herbal Medicinal ◽  
Package Filter ◽  
First Time

In urological practice there is a sufficient demand for herbal medicinal preparations, of which the most widely used drugs are derived from arbutin-containing herbs. These medicines have diuretic, anti-inflammatory and antimicrobial activity. Currently, in connection with the decrease in number of production departments and pharmacies, water extraction can be made by the consumer at home from powdered medicinal herbs in filter bags and from packaged shredded medicinal plant raw materials in batches according to the instructions on the package. The object of the study was the aqueous extract obtained from the leaves of lingonberry. The article presents the study of manufacturing technology of water extracts from lingonberry leaves with the establishment of quality indicators in them. Investigated water extract obtained from raw materials packaged in bundles according to the instructions on the package, filter packages according to the instructions on the packaging of packaged raw materials in batches according to the method of State Pharmacopea XIII. The following were analyzed in the obtained water extracts: description, authenticity, dry residue, pH, content of phenolglucoside - arbutin. The research results were processed statistically. All of the studied aqueous extracts were transparent dark brown liquid that had a bitter, astringent taste characteristic of leaves of lingonberry. Dry residue in an aqueous extract, depending on the composition and technology was 0,65, 0,8% and of 1,93%. The content of arbutin was 0,43, 0,39 and 0,99%, pH of water extracts made from the crushed leaves of lingonberry, had close values of 5,03, 4,95 and, while in the extracts from powdered of lingonberry leaves in filter bags had pH value of 5,35, which may be attributed to the influence of the material of the filter bag. For the first time technologo-analytical study of the water extracts obtained at different technologies, established indicators of quality.

scholarly journals THE SWEET ICES FOR PREGNANT WOMEN

2019 ◽  
Vol 13 (1) ◽  
Author(s):  
J. Kozonova ◽  
L. Telegenko ◽  
A. Salavelis
Keyword(s):  
Pregnant Women ◽  
Raw Materials ◽  
Chromatographic Study ◽  
Plant Raw Materials ◽  
Daily Food ◽  
Sodium Magnesium ◽  
Magnesium Salts ◽  
First Time ◽  
Average Woman ◽  
Acid Index

Daily food consumption norms of an average woman and a pregnant woman have been analysed. It has been established that in a pregnant woman’s diet, it is necessary to increase the content of proteins, fibre, vitamins C, E, D, PP, and B, and reduce fats, carbohydrates (easily digestible), vitamins B5 and H, sodium, magnesium, salts, and water. Taking into account the above-mentioned requirements, eight recipe compositions of sweet ices based on plant raw materials have been suggested. The recipes were selected by linear programming using MS Excel. The products have a low calorific content (26–137 kcal per 80 g), and an increased nutritional value (due to vitamin C, carotene, etc.). For the first time, cereals, various types of seeds, nuts, have been put into the recipe of sweet ices, as well as raw materials, which eliminate physiological complications during pregnancy. The products developed differ in their composition and are made without sugar. However, some recipes include small quantities of honey as it is highly palatable. The chemical composition of the new sweet products has been studied and analysed in details and sugar/acid indices have been calculated. The developed ices have a slightly acidic taste or no acidity at all, which corresponds to the values of sugar/acid indices 13.4–26.6, while the sample from the store, selected for comparison, contains a large amount of sugars, as evidenced by the cloying taste and high sugar/acid index (more than 30). The source of fatty acids in sweet ice for pregnant women Joy is almond nuts. The results of the chromatographic study have shown that this product as for the quantitative fatty acid composition, meets the current requirements. We recommend introducing the sweet ice manufacture technology on the equipment already in use in canneries. The products are formed (poured into moulds where wooden sticks are then inserted) in a Hassia machine. One of the main operations, freezing, is done in a quick freezer GyroFreze. We also recommend manufacturing sweet ices using existing restaurant equipment.

scholarly journals EFFICIENCY OF SOME PLANT EXTRACTS TO CONTROL OF PENICILLIUM ITALICUM WEHMER CAUSING BLUE MOLD ON LEMON FRUITS IN IRAQ

2019 ◽  
Vol 31 (1) ◽  
pp. 01-05
Author(s):  
Ahed A.H. Matloob ◽  
Hamid A A. Khafaji
Keyword(s):  
Plant Extracts ◽  
Water Extract ◽  
Inhibitory Effect ◽  
Penicillium Italicum ◽  
Blue Mold ◽  
Lemon Fruit ◽  
Water Extracts ◽  
Wild Mustard ◽  
First Time ◽  
High Inhibitory Effect

The study aimed to evaluate the efficacy of the water extract of Propolis, Wild mustard and dates vinegar in the inhibition of Penicillium italicum causal agent of Blue mold on a lemon fruits. The results showed that all tested extracts with concentrations 5, 10 and 15% had a high inhibitory effect against P. italicum. Dates vinegar is highly effective and showed 100% inhibition of P. italicum and protected lemon fruit from infection. First time this type of natural inhibitory water extracts are used in Iraq which resulted that the dates vinegar is the best suitable option for the management of lemon blue mold disease in post-harvest.

Preparation of Xonotlite Whiskers from Carbide Slag

2010 ◽  
Vol 434-435 ◽  
pp. 787-789
Author(s):  
Fei Liu ◽  
Ling Ke Zeng ◽  
Jian Xin Cao ◽  
Qian Lin ◽  
Jing Li
Keyword(s):  
Ph Value ◽  
Raw Materials ◽  
Removal Rate ◽  
Hydrothermal Conditions ◽  
Hydrothermal Route ◽  
Synthesis Conditions ◽  
Ph Values ◽  
Carbide Slag ◽  
Xrd Techniques ◽  
First Time

Carbide slag was used as raw materials for the first time to prepare xonontlite whiskers via a hydrothermal route without special instruments and synthesis conditions. And the effect of pH value of emulsion of carbide slag and hydrothermal conditions on removal rate of impurities, morphology and crystallinity of synthesized xonotlite whiskers were explored using ICP, SEM and XRD techniques. The results indicated that the carbide slag after purification could be used to prepare xonotlite whiskers, and different pH values of emulsion of carbide slag had great impact on the removal rate of impurities and morphology of xonotlite whiskers. Xonotlite whiskers with 20-40 μm in length and 100-500 nm in diameter were hydrothermally synthesized at 230 °C for 15 h with using silicic acid as kiesel material.

scholarly journals Synthesis of a hydrophilic derivative of ecdysterone and development of its water-soluble form

2021 ◽  
Vol 104 (4) ◽  
pp. 138-148
Author(s):  
A.M. Kozhanova ◽  
◽  
B.S. Temirgaziyev ◽  
A. Zhanarbek ◽  
B.I. Tuleuov ◽  
...  
Keyword(s):  
Raw Materials ◽  
Chemical Shifts ◽  
Stoichiometric Composition ◽  
Water Soluble ◽  
Soluble Form ◽  
Nmr Studies ◽  
Polar Solvents ◽  
Plant Raw Materials ◽  
Pharmaceutical Plant ◽  
First Time

The article presents materials on the isolation of ecdysterone substance from medicinal plant raw materials Silene wolgensis (Hornem.) Bess. ex. Spreng (Volga smolyovka). For the first time, the optimization of the method for ecdysterone substance obtaining from the aboveground part of the superconcentrator of phytoecdysteroids of the Silene wolgensis was carried out and based on it a pilot industrial regulation for the isolation of ecdysterone and an encapsulated water-soluble form were developed. It was found, that the interaction of the substrate molecule and the clathrate forms a substance that can dissolve in water and other more polar solvents, thereby solving the problem of bioavailability of the main hydrophobic drug. The method developed for producing the substance ecdysterone and its water-soluble encapsulated with β-cyclodextrin form was implemented into production at the Karaganda pharmaceutical plant. NMR studies of changes in the chemical shifts of protons of substrates and receptors illustrated that ecdysterone interacts with β-cyclodextrin to form supramolecular inclusion complexes with stoichiometric composition of 1:1

scholarly journals Chemical Composition of Medicinal Plants Growing Under Conditions of Anthropogenic Load (On the Example of the Kursk Region)

2020 ◽  
Vol 6 (4) ◽  
pp. 89-97
Author(s):  
S.A. Kurbatov ◽  
◽  
V.M. Zubkova ◽  
◽  
Keyword(s):  
Heavy Metals ◽  
Betula Pendula ◽  
Raw Materials ◽  
Biologically Active ◽  
Tilia Cordata ◽  
Plant Raw Materials ◽  
High Level ◽  
First Time ◽  
Kursk Region ◽  
Active Substances

in the conditions of the Kursk region, the analysis of soil samples and plant samples for the content of heavy metals was carried out. It is established that the soils of the studied areas are classified as having a high level of pollution in terms of their content. The priority pollutants of the soil are Pb, Zn, Cd, Cr, Ni, and Cu, the supply of which is mainly associated with the enterprises operating in this territory. The content of heavy metals in medicinal plant raw materials is estimated. For the first time, depending on the biological characteristics of Tilia cordata, Betula pendula, Plantago major, Urtica dioica, Achillea millefollium, data on the content of biologically active substances in conditions of technogenic pollution are presented, and the antioxidant activity of plants in areas characterized by various anthropogenic loads is studied.

scholarly journals STUDY OF COMPARATIVE EXTRACTABILITY OF BIOLOGICALLY ACTIVE SUBSTANCES FROM ST. JOHN’S WORT HERB OF VARIOUS SERIES

2021 ◽  
Vol 9 (1) ◽  
pp. 11-16
Author(s):  
R.M. Streltsova ◽  
◽  
А.B. Denisova ◽  
Z.F. Gromova ◽  
◽  
...  
Keyword(s):  
Particle Size ◽  
Aqueous Extract ◽  
Raw Materials ◽  
Wave Length ◽  
Biologically Active ◽  
High Yield ◽  
Aqueous Extracts ◽  
Solid Residue ◽  
Plant Raw Materials ◽  
Related Substances

Aim. To study extractability of a complex of active and related substances and flavonoids from St. Johns Wort herb of various series and anufacturers and identification of factors affecting the quality of aqueous extracts from St. Johns Wort herb. Materials and Methods. The object of study was St. Johns Wort herb of four series of two manufacturers, and aqueous extracts obtained from these series of St. Johns Wort herb. Aqueous extracts were made in the infusion mode in accordance with the requirements of the Order of the Ministry of Health of the Russian Federation №751n of October 26, 2015. The ratio of raw materials and extractive solvent was 8:100. The obtained aqueous extracts were evaluated by color and smell parameters. A complex of biologically active and related substances extracted from St. Johns Wort herb was evaluated by the solid residue index. Quantitative determination of flavonoids in recalculation for rutin was performed by spectrophotometric method on Bio-RADSmartSpecPlus spectrophotometer at 410 nm wave length. Results. Raw materials of different series differ in external characteristics and fineness. Raw materials of 221218 series contain 17.46% of particles larger than 3 mm, and raw materials of 20218 series – 4.92%. Raw materials of 221218 series include more particles of the coarse parts of the plant. Raw materials of 10119 series have a more uniform distribution of particles by fractions, but a rather large number of small particles. The maximal solid residue was obtained from raw materials of 20218 series – 1.7716%, the minimal – from raw materials of 221218 series – 0.6183%. The maximal flavonoid content was found in aqueous extract obtained from raw materials of 20218 series – 1.988%, the minimal content – from raw materials of 221218 series – 0.6183%. A sufficiently high yield of flavonoids in the aqueous extract was established for raw materials of 10119 series – 1.9711%. Conclusions. It was found that raw materials containing more soft parts of plants and characterized by the presence of a higher percent of fine fractions of particles, have the best extractability. At present, in the SP (Russia) of the 14th edition, only fractions of St. Johns Wort herb with a particle size of more than 7 mm and less than 0.18 mm are normalized. In our opinion, it is reasonable to include requirements to particle size and their content for the main fractions of the feedstock.

scholarly journals Determination of the antioxidant activity of Ficus carica aqueous extract

2012 ◽  
pp. 25-31 ◽  
Author(s):  
Svetlana Trifunski ◽  
Dorina Ardelean
Keyword(s):  
Antioxidant Activity ◽  
Traditional Medicine ◽  
Potassium Permanganate ◽  
Aqueous Extract ◽  
Room Temperature ◽  
Colorimetric Method ◽  
Water Extract ◽  
Leaf Water ◽  
Water Extracts

The aim of this study was to examine the antioxidant activity of water extracts from fig leaf. Water extracts were prepared according to traditional medicine. The antioxidant activity of the extracts was spectrophotometrically determined. Using the potassium permanganate colorimetric method it was found that the water extract that was maintained at the refrigerator had lower antioxidant activity than extract that was maintained at the room temperature.

scholarly journals FLAVONOIDS FROM THE BUDS OF THE HORSE CHESTNUT (AESCULUS HIPPOCASTANUM L.)

2020 ◽  
pp. 123-129
Author(s):  
Vladimir Aleksandrovich Kurkin ◽  
Pavel Viktorovich Belov
Keyword(s):  
Medicinal Plant ◽  
Raw Materials ◽  
Uv Spectroscopy ◽  
Raw Material ◽  
Aesculus Hippocastanum ◽  
Horse Chestnut ◽  
Plant Raw Materials ◽  
Wide Range ◽  
New Type ◽  
First Time

The buds of horse chestnut (Aesculus hippocastanum L., Hippocastanaceae family) is a new promising species of medicinal plant raw material. The prospect of studying the buds of this plant is due to the content of flavonoids in them, which have a wide range of pharmacological effects. Flavonoids are interesting for their capillary-strengthening action, which allows them to be used in the treatment of chronic venous insufficiency. This fact is consistent with the practice of using drugs from other organs of horse chestnut (seeds, leaves) as venotonic and angioprotective drugs. In addition, flavonoids are also characterized by antioxidant, anti-inflammatory, antimicrobial and antifungal activity. The actuality of the study of horse chestnut buds as a new type of medicinal plant material is also supported by the need to develop of the new effective and safe drugs based on the raw materials of this plant. The aim of this study was to determine the flavonoid composition of the buds of Aesulus hippocastanum. In the course of the work from the buds of horse chestnut by the method of column chromatography on silica gel L 100/160 was for the first time there were isolated and characterized using 1H-NMR, 13C-NMR, UV spectroscopy and mass spectrometry the flavonoid compounds rhamnocitrin (7-O-methylkaempferol), and accompanying 7,4′-dimethylkaempferol. The dominant and diagnostic significant flavonoid for the horse chestnut buds is rhamnocitrin. The results indicate the prospects for further study of the buds of the horse chestnut as a new type of medicinal plant raw materials.

scholarly journals Identification of anise (Anisum vulgare Gaertn.) herbs by morphological and anatomical characteristics

2021 ◽  
Vol 14 (1) ◽  
pp. 39-44
Author(s):  
S. V. Kolisnyk ◽  
T. M. Gontova ◽  
U. A. Umarov ◽  
K. R. Hordiei
Keyword(s):  
Antibacterial Effect ◽  
Raw Materials ◽  
Microscopic Analysis ◽  
Anatomical Structure ◽  
Biologically Active ◽  
Professional Literature ◽  
Plant Raw Materials ◽  
Naked Eye ◽  
Normative Documentation ◽  
First Time

The fruits of anise contain different classes of biologically active compounds, due to which they have antidepressant, antiperoxidant, antidiabetic effect; extracts of this plant have an antibacterial effect. Professional literature lacks information on the chemical composition of anise herbs and prospects for their use in medicine. The aim of the work is to study of the morphological and anatomical structure of the aboveground organs of anise and to establish of macro- and microscopic diagnostic characters necessary for the identification of the plant raw materials. Materials and methods. Anise herbs consisting of stems, leaves flowers, and unripe fruits were used for the study. Fresh and dried raw materials were macroscopically analyzed with the naked eye and using a magnifying glass (×10). Studies of transverse and longitudinal sections, epidermis and surface preparations were performed using conventional techniques: with microscopes MBS 9, MS 10 (glasses ×5, ×10, ×15, lenses ×10, ×40), Micromed XS-4130 (eyepiece WF15X, lenses ×40/0.65, ×10/0.25) with a photomicrographic attachment. The micrographs were taken with Samsung PL50 camera. Results. As a result of the macro- and microscopic analysis, diagnostic properties of anise herbs were established. Conclusions. It is for the first time that macro- and microscopic characteristics of anise herbs were studied, which confirms the identity of raw materials. The obtained results will be used for the development of domestic normative documentation on anise herbs raw materials.

scholarly journals DEVELOPMENT AND VALIDATION OF COMPLEXOMETRIC METHODS FOR THE DETERMINATION OF CAL-CIUM AND MAGNESIUM IN MEDICINAL PLANT MATERIALS (ON THE GRASS PERSICARIA MACULOSA GRAY.)

2020 ◽  
pp. 155-162
Author(s):  
Anna Sergeyevna Chistyakova ◽  
Alevtina Alekseyevna Gudkova ◽  
Ol'ga Valer'yevna Trineeva ◽  
Alla Anatol'yevna Sorokina ◽  
Sof'ya Aleksandrovna Vasil’eva
Keyword(s):  
Ph Value ◽  
Raw Materials ◽  
Calcium Content ◽  
Pyrocatechol Violet ◽  
Plant Materials ◽  
Plant Raw Materials ◽  
Optimum Ph ◽  
Calcium And Magnesium ◽  
Development And Validation

The relevance of the study of the mineral composition of plant objects is undoubted. In plant organisms, macro and micronutrients are present in an easily digestible form. The macroelements most accumulated in plants include calcium and magnesium, whose sources are members of the family Polygonaceae Juss, in particular the genus Persicaria Mill. The aim of the work was to develop a technique for quantitative complexometric determination of calcium and magnesium in plant raw materials after the burning procedure and its validation. As a result, optimal conditions for the quantitative determination of calcium and magnesium in plant objects were experimentally selected using the example of Persicaria maculosa Gray. mountaineer grass using complexometric titration after ashing and calcination. For the determination of calcium, the optimum pH value is 11–12, the acidic indicator is dark blue – chromium, the optimum pH for magnesium is 8–9, the indicator is pyrocatechol violet. The calcium content in the plant varies from 0.12% to 0.58%, the amount of magnesium is about 0.02%. The relative error of the mean determination with a 95% probability was no more than 1.60% and no more than 1.84% when determining calcium and magnesium, respectively. Studies have shown the validity of the developed methodology for indicators of authenticity, precision (convergence, reproducibility), specificity, linearity.

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