scholarly journals Characterization of Local Products for Their Industrial Use: The Case of Italian Potato Cultivars Analyzed by Untargeted and Targeted Methodologies

Foods ◽  
2020 ◽  
Vol 9 (9) ◽  
pp. 1216
Author(s):  
Cinzia Ingallina ◽  
Mattia Spano ◽  
Anatoly P. Sobolev ◽  
Cristina Esposito ◽  
Cristina Santarcangelo ◽  
...  
Keyword(s):  
Solanum Tuberosum L ◽  
Potato Cultivars ◽  
Water Soluble ◽  
Raw Material ◽  
Array Detector ◽  
Ionization Mass ◽  
High Quality ◽  
Blue Star ◽  
Italian Regions

The chemical characterization of local Italian potato cultivars is reported to promote their preservation and use as high quality raw material in food industries. Twenty potato (Solanum tuberosum L.) cultivars from Piedmont and Liguria Italian regions were investigated using NMR (Nuclear Magnetic Resonance) and RP-HPLC-PDA-ESI-MSn (Reversed Phase High-Performance Liquid Chromatography with Photodiode Array Detector and Electrospray Ionization Mass Detector) methodologies. Water soluble and lipophilic metabolites were identified and quantified. With respect to literature data, a more complete 1H (protonic) spectral assignment of the aqueous potato extracts was reported, whereas the 1H NMR assignment of potato organic extracts was reported here for the first time. Phenolics resulted to be in high concentrations in the purple–blue colored Rouge des Flandres, Bergerac, Fleur Bleu, and Blue Star cultivars. Servane, Piatlina, and Malou showed the highest amount of galacturonic acid, a marker of pectin presence, whereas Jelly cultivar was characterized by high levels of monosaccharides. Roseval and Rubra Spes contained high levels of citric acid involved in the inhibition of the enzymatic browning in fresh-cut potato. High levels of the amino acids involved in the formation of pleasant-smell volatile compounds during potato cooking were detected in Rouge des Flandres, Blue Star, Bergerac, Roseval, and Ratte cultivars. These results suggest that each local cultivar is characterized by a proper chemical profile related to specific proprieties that can be useful to obtain high quality industrial products.

scholarly journals Analysis of Polyphenolic Composition of a Herbal Medicinal Product—Peppermint Tincture

Molecules ◽  
2019 ◽  
Vol 25 (1) ◽  
pp. 69
Author(s):  
Agnieszka Bodalska ◽  
Adam Kowalczyk ◽  
Maciej Włodarczyk ◽  
Izabela Fecka
Keyword(s):  
High Performance ◽  
Raw Material ◽  
Array Detector ◽  
Ionization Mass ◽  
Medicinal Products ◽  
European Pharmacopoeia ◽  
Dry Extract ◽  
Polyphenolic Composition ◽  
Essential Parameter ◽  
Herbal Medicinal

The pharmacological activity of peppermint leaf (Menthae piperitae folium) for medical use is mainly attributed to the presence of essential oil, which, according to the European Pharmacopoeia (Ph. Eur.), should constitute not less than 12 mL/kg of raw material. The content of polyphenols in peppermint-based preparations, except peppermint leaf dry extract, has not yet been considered as an essential parameter in the pharmacopeial assessment of peppermint quality. This study concerns the evaluation of the presence of representatives of polyphenolic compounds in 23 commercial peppermint tinctures (ethanolic extracts) purchased in pharmacies in Poland. The non-volatile polyphenolic fraction was investigated, and the presence of flavonoids and phenolic acids was quantified. High performance liquid chromatography coupled with a diode-array detector (HPLC-DAD) and an electrospray ionization mass spectrometer (U(H)PLC-ESI-MS) were used in the experiment. The study showed that eriocitrin, luteolin-7-O-rutinoside, and rosmarinic acid were the main polyphenolic components of the peppermint tinctures, as previously reported for peppermint leaf. Despite this, the research shows the extremely diverse content of the mentioned compounds in analyzed commercial medicinal products. In light of these results, it seems that the pharmacopeial assessment for the peppermint leaf (Ph. Eur.) and peppermint tincture (Polish Pharmacopoeia (FP)) requires correction and supplementation.

Characterization of phenolic compounds from inner bark of Betula pendula

Holzforschung ◽  
2012 ◽  
Vol 66 (2) ◽  
Author(s):  
Jaana Liimatainen ◽  
Maarit Karonen ◽  
Jari Sinkkonen ◽  
Marjo Helander ◽  
Juha-Pekka Salminen
Keyword(s):  
Phenolic Compounds ◽  
High Performance ◽  
Betula Pendula ◽  
Silver Birch ◽  
Biologically Active ◽  
Array Detector ◽  
Ionization Mass ◽  
Inner Bark ◽  
First Time

Abstract A method has been developed for the characterization of biologically active silver birch (Betula pendula) inner bark phenolics based on high-performance liquid chromatography/diode array detector (HPLC-DAD)/electrospray ionization-mass spectrometry (ESI-MS). It was demonstrated that the inner bark contains high amounts of flavonoids, arylbutanoids, diarylheptanoids, simple phenolic compounds, phenolic acids, lignans, and procyanidins. Altogether, 30 individual compounds were characterized based on their ultraviolet (UV) and MS data. Structures of 22 compounds were confirmed by nuclear magnetic resonance (NMR) spectroscopy. In addition to previously reported phenolic compounds, 12 compounds were identified in silver birch inner bark for the first time; two of them are novel compounds: 3-β-glucopyranosyloxy-2-hydroxy-1-(4-hydroxy-3-methoxy-phenyl)-propan-1-one and 1,7-bis-(4-hydroxyphenyl)-3-heptanol 3-O-β-ap-iofuranosyl-(1→2)-β-glucopyranoside.

Synthesis and Characterization of Rosinyl Amine Salt Surfactant

2011 ◽  
Vol 183-185 ◽  
pp. 1888-1891 ◽  
Author(s):  
Yan Jin ◽  
Shuang Yue Li ◽  
Shu Jun Li ◽  
Li Jun Zhang
Keyword(s):  
Chemical Structure ◽  
Foam Stability ◽  
Critical Micellar Concentration ◽  
Amine Salt ◽  
Raw Material ◽  
Ionization Mass ◽  
Reaction Conditions ◽  
1H Nuclear Magnetic Resonance ◽  
Optimal Reaction

Rosin is reputed as green petroleum because it is renewable, not expensive, and environmental friendly. China is rich in rosin resources. In this report, rosin was used as raw material to prepare rosinyl amine salt (RAS) surfactant. The optimal reaction conditions of RAS was modified rosin and dimethylamine mole ratio of 1:2, reaction temperature of 78 oC and reaction time of 2 h. The chemical structure of the product was identified by Fourier transform infrared spectroscopy (FTIR), electrospray ionization-mass spectrometry (ESI-MS) and 1H nuclear magnetic resonance (NMR) analysis. As a surfactant, it has a critical micellar concentration (CMC) of 7.07×10-5mol/L, a surface tension of 44.36 mN/m, an emulsification activity of 5min, a height of foam of 165 mm, and a foam stability of 143 mm.

scholarly journals Characterization of bentonite clay from 'Greda' deposit

2011 ◽  
Vol 5 (2) ◽  
pp. 97-101 ◽  
Author(s):  
Nadezda Stankovic ◽  
Mihovil Logar ◽  
Jelena Lukovic ◽  
Jelena Pantic ◽  
Miljana Miljevic ◽  
...  
Keyword(s):  
Ceramic Industry ◽  
Bentonite Clay ◽  
Nitrogen Adsorption ◽  
Raw Material ◽  
X Ray Diffraction ◽  
High Quality ◽  
X Ray ◽  
High Silica ◽  
Representative Samples

Based on mineralogical and technological investigations of the deposit 'Greda' important characteristics of bentonite clay were determined. Representative samples of the deposit were characterized with X-ray diffraction, low-temperature nitrogen adsorption, chemical analysis, differential thermal analysis and scanning electron microscopy. It was determined that the main mineral is montmorillonite and in subordinate quantities kaolinite, quartz and pyrite. The chemical composition generally shows high silica and alumina contents in all samples and small quantities of Fe3+, Ca2+ and Mg2+ cations. Based on technological and mineralogical research, bentonite from this deposit is a high-quality raw material for use in the ceramic industry.

scholarly journals Identification of the Secondary Metabolites and Characterization of Lagerstroemia Loudonii T. & B.

2021 ◽  
Vol 6 (1) ◽  
pp. 1-6
Author(s):  
Fahrauk Faramayuda ◽  
Faizal Hermanto ◽  
Ari Sri Windyaswari ◽  
Soraya Riyanti ◽  
Viola Aditya Nurhayati
Keyword(s):  
Herbal Medicine ◽  
Specific Gravity ◽  
Traditional Medicine ◽  
Ash Content ◽  
Water Soluble ◽  
Raw Material ◽  
Bark Extract ◽  
Phytochemical Screening

Bungur  (Lagerstroemia loudonii T. B) is a type of plant widely grown in Indonesia and can be found in teak forests, mixed forests, and is found as ornamental plants or protective trees on the roadside. In the fruit section, Lagerstroemia loudonii is used as antituberculous and antimalarial. On the bark, the part is used as antidiarrheal. Based on some parts of the Lagerstroemia loudonii  plants' activity data, this plant has the potential to be developed into traditional medicine. Standardized traditional medicine material is necessary to identify efficacious compounds and characterization in some parts of Lagerstroemia loudonii. The purpose of this research is to develop Lagerstroemia loudonii into traditional herbal medicine or standardized herbal medicine. Identification of efficacious compounds and characterization of crude leaf drugs, bark, stems, and fruit of Lagerstroemia loudonii. The phytochemical screening phase of the crude drugs of leaves, bark, stems, and fruit ofLagerstroemia loudonii against includes examining alkaloids, flavonoids,  quinones, tannins, polyphenols, saponins, steroids and triterpenes, monoterpenoids and sesquiterpenoids. The determination of the characteristics of raw material carried out includes nonspecific parameters. Nonspecific parameters are the determination of total ash content, water-soluble ash content, acid insoluble ash content. each experiment was carried out three times and calculated the average yield and deviation.  Identification results of the class of efficacious compounds in some parts of the Lagerstroemia loudonii  plant are on the leaves and fruits containing alkaloids, flavonoids, saponins, quinones, tannins, polyphenols, monoterpenoids, and sesquiterpenoids as well as steroids and triterpenoids. At the bark and stem, the bark contains alkaloids, flavonoids, saponins, quinones, tannins, polyphenols, monoterpenoids, and sesquiterpenoids. Characterization results of Lagerstroemia loudonii  leaf extract total ash content 4.45 ± 0.30% w/w, water-soluble ash content 4.08 ± 0.27% w/w, acid insoluble ash content 0.59 ± 0.06% w/w, the extract specific gravity was 0.59 ± 0.063. Lagerstroemia loudonii  stem bark extract, total ash content 1.94 ± 0.12% w/w, water-soluble ash content 1.47 ± 0.03% w/w, acid insoluble ash content 0.24 ± 0.02% w/w, the extract specific gravity is 0.82 ± 0.01. Lagerstroemia loudonii  stem extract, total ash content3.18 ± 0.16% w/w, water-soluble ash content 2.36 ± 0.38% w/w, acid insoluble ash content 0.43 ± 0.07% w/w, extract specific grafity 0.81 ± 0.01. Lagerstroemia loudonii  fruit extract, total ash content 11.45 ± 1.16%w/w, water-soluble ash content 10.1 ± 1.49% w/w, acid insoluble ash content 1.46 ± 0.88% w/w,extract specific grafity 0.81 ± 0.01. Based on phytochemical screening data and the characterization of bungur plants potential to be developed into raw materials for traditional medicineKeywords: Lagerstroemia loudonii, secondary metabolite, raw material characterization

Evaluation and Characterization of Cellulose Nanofibers from Flaxseed Fiber Bundles

2021 ◽  
Vol 8 (4) ◽  
pp. 8-14
Author(s):  
Sayed Waqar Azhar ◽  
Fujun Xu ◽  
Yiping Qiu
Keyword(s):  
Cellulose Nanofibers ◽  
Agricultural Residues ◽  
Raw Material ◽  
Fiber Bundles ◽  
High Quality ◽  
Simple Method ◽  
New Approach ◽  
Rational Management ◽  
Novel Applications

In recent decades, rational management of agricultural residues presented a new approach for extraction, characterization, and utilization of cellulose nanofibers (CNF). In this context, the valorization of flaxseed fibers, providing an annual yield of millions of metric tons, as an abundant sustainable fiber source, was carried out. The cleaned and ground raw material was delignified and bleached, followed by 2,2,6,6-tetramethylpiperidine-1-oxyl radical (TEMPO)/NaBr/NaClO oxidization along with mechanical homogenization. The resulting extracted cellulose and cellulose nanofibers were characterized by various analytical methods. The overall yield of CNF based on the raw material was 31.2% ± 1.5%. This study explored a simple method for converting flaxseed fibers to fluorescent, high quality, nano-sized cellulosic precursors for novel applications in pharmaceutical and bio-composite applications.

scholarly journals RP-HPLC-DAD-MSn Analysis and Butyrylcholinesterase Inhibitory Activity of Barbacenia blanchetii Extracts

2015 ◽  
Vol 10 (6) ◽  
pp. 1934578X1501000
Author(s):  
Jósquia S Barbosa ◽  
Verônica M Almeida ◽  
Rosilene M Marçal ◽  
Alexsandro Branco
Keyword(s):  
High Performance ◽  
Methanol Extract ◽  
Array Detector ◽  
Ionization Mass ◽  
Diode Array Detector ◽  
Rp Hplc ◽  
Dependent Form ◽  
Ellman’S Method ◽  
First Time

High-performance liquid chromatography (HPLC) coupled to a diode-array detector (DAD) and electrospray ionization mass spectrometry (MS) was applied for the separation and identification of phenolic compounds in the n-hexane, ethyl acetate and methanol crude extract of Barbacenia blanchetii. The MS, MSn and UV data together with chemosystematic evidence allowed the structural characterization of five compounds: tricin, chrysoeriol, epi-gallocatechin, kaempferol 3- O-glucoside and caffeoylquinic acid. At the same time, these extracts were evaluated against butyrylcholinesterase using Ellman's method. All extracts inhibited BuChE in a concentration-dependent form; however, the methanol extract showed a better effect that the other extracts. These compounds have been identified previously in the Velloziaceae family, but for the first time as constituents of B. blanchetii.

Characterization of the ozone response of potato leaf protoplasts

1985 ◽  
Vol 63 (11) ◽  
pp. 1936-1941 ◽  
Author(s):  
B. L. Illman ◽  
E. J. Pell
Keyword(s):  
Solanum Tuberosum L ◽  
Air Pollutant ◽  
Potato Cultivars ◽  
Fluorescein Diacetate ◽  
Ozone Exposure ◽  
Potato Leaf ◽  
Cellular Effects ◽  
Relative Differences ◽  
Leaf Protoplasts

Ozone response of Solanum tuberosum L. leaf protoplasts was characterized to better understand the cellular effects of this important air pollutant. 'Norchip' and 'Cherokee' potato cultivars relatively tolerant of and sensitive to ozone, respectively, were studied. Protoplasts were exposed to ozone, air, or oxygen for 0, 1, 3, 5, 10, or 15 min. Two criteria, lysis and fluorescein diacetate staining, were used to measure protoplast response. Protoplasts exposed to ozone exhibited a significant increase in lysis and reduction in fluorescein diacetate staining during the first 10 min of exposure. During the following 5 min there were no further significant changes in lysis or fluorescein diacetate staining. The two ozone responses paralleled each other, probably reflecting two different nonsequential cellular effects. Neither oxygen nor air elicited the protoplast responses observed after ozone exposure. The relative differences in ozone response observed in intact plants of 'Norchip' and 'Cherokee' were not observed in experiments performed with protoplasts of these cultivars. The experimental results reported herein illustrate the importance of the plasma membrane to the ozone response but do not support its role in explaining the differential tolerance of the two potato cultivars studied.

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