scholarly journals Surface Wettability and Electrical Resistance Analysis of Droplets on Indium-Tin-Oxide Glass Fabricated Using an Ultraviolet Laser System

Micromachines ◽  
2021 ◽  
Vol 12 (1) ◽  
pp. 44
Author(s):  
Hsin-Yi Tsai ◽  
Chih-Ning Hsu ◽  
Cheng-Ru Li ◽  
Yu-Hsuan Lin ◽  
Wen-Tse Hsiao ◽  
...  

Indium tin oxide (ITO) is widely used as a substrate for fabricating chips because of its optical transparency, favorable chemical stability, and high electrical conductivity. However, the wettability of ITO surface is neutral (the contact angle was approximately 90°) or hydrophilic. For reagent transporting and manipulation in biochip application, the surface wettability of ITO-based chips was modified to the hydrophobic or nearly hydrophobic surface to enable their use with droplets. Due to the above demand, this study used a 355-nm ultraviolet laser to fabricate a comb microstructure on ITO glass to modify the surface wettability characteristics. All of the fabrication patterns with various line width and pitch, depth, and surface roughness were employed. Subsequently, the contact angle (CA) of droplets on the ITO glass was analyzed to examine wettability and electrical performance by using the different voltages applied to the electrode. The proposed approach can succeed in the fabrication of a biochip with suitable comb-microstructure by using the optimal operating voltage and time functions for the catch droplets on ITO glass for precision medicine application. The experiment results indicated that the CA of droplets under a volume of 20 μL on flat ITO substrate was approximately 92° ± 2°; furthermore, due to its lowest surface roughness, the pattern line width and pitch of 110 μm exhibited a smaller CA variation and more favorable spherical droplet morphology, with a side and front view CA of 83° ± 1° and 78.5° ± 2.5°, respectively, while a laser scanning speed of 750 mm/s was employed. Other line width and pitch, as well as scanning speed parameters, increased the surface roughness and resulted in the surface becoming hydrophilic. In addition, to prevent droplet morphology collapse, the droplet’s electric operation voltage and driving time did not exceed 5 V and 20 s, respectively. With this method, the surface modification process can be employed to control the droplet’s CA by adjusting the line width and pitch and the laser scanning speed, especially in the neutral or nearly hydrophobic surface for droplet transporting. This enables the production of a microfluidic chip with a surface that is both light transmittance and has favorable electrical conductivity. In addition, the shape of the microfluidic chip can be directly designed and fabricated using a laser direct writing system on ITO glass, obviating the use of a mask and complicated production processes in biosensing and biomanipulation applications.

2008 ◽  
Vol 594 ◽  
pp. 241-248 ◽  
Author(s):  
Fwu Hsing Liu ◽  
Yunn Shiuan Liao ◽  
Hsiu Ping Wang

The material in powder state has long been used by selective laser sintering (SLS) for making rapid prototyping (RP) parts. A new approach to fabricate smoother surface roughness RP parts of ceramic material from slurry-sate has been developed in this study. The silica slurry was successfully laser-gelling in a self-developed laser sintering equipment. In order to overcome the insufficient bonding strength between layers, a strategy is proposed to generate ceramic parts from a single line, a single layer, to multi-layers of gelled cramic in this paper. It is found that when the overlap of each single line is 25% and the over-gel between layers is 30%, stronger and more accurate dimensional parts can be obtained under a laser power of 15W, a laser scanning speed of 250 mm/s, and a layer thickness of 0.1 mm. The 55:45 wt. % of the proportion between the silica powder and silica solution results in suitable viscosity of the ceramic slurries without precipitation. Furthermore, the effects of process parameters for the dimensional accuracy and surface roughness of the gelled parts are investigated and appropriate parameters are obtained.


Materials ◽  
2019 ◽  
Vol 13 (1) ◽  
pp. 9 ◽  
Author(s):  
Andrzej Matras

The paper studies the potential to improve the surface roughness in parts manufactured in the Selective Laser Melting (SLM) process by using additional milling. The studied process was machining of samples made of the AlSi10Mg alloy powder. The simultaneous impacts of the laser scanning speed of the SLM process and the machining parameters of the milling process (such as the feed rate and milling width) on the surface roughness were analyzed. A mathematical model was created as a basis for optimizing the parameters of the studied processes and for selecting the sets of optimum solutions. As a result of the research, surface with low roughness (Ra = 0.14 μm, Rz = 1.1 μm) was obtained after the face milling. The performed milling allowed to reduce more than 20-fold the roughness of the SLM sample surfaces. The feed rate and the cutting width increase resulted in the surface roughness deterioration. Some milled surfaces were damaged by the chip adjoining to the rake face of the cutting tool back tooth.


Coatings ◽  
2020 ◽  
Vol 10 (5) ◽  
pp. 451
Author(s):  
Jinchang Guo ◽  
Yu Shi ◽  
Peibiao Geng ◽  
Gang Zhang ◽  
Ming Zhu

A fiber laser was used to nitride Ti–6Al–4V titanium alloy the effect of the process parameters on the surface morphology was studied. The surface chemical composition of the nitride layer and the phase of black powder on the surface were analyzed, the two-dimensional and three-dimensional surface topography of the nitride layer surface were measured, and the cross-section microstructure of the nitride layer was photographed. The effects of laser power, laser scanning speed, nozzle distance, and nitrogen flow rate on the surface morphology were studied. The experiments show that the laser power mainly affects the surface oxidation, the laser scanning speed mainly affects the surface roughness, and the nozzle distance has a great influence on the surface morphology. The gas flow rate, however, had a slight effect on the surface morphology. A large heat input and a high nitrogen flow rate caused an increase in TiN and TiO2 black powders. Surface oxidation did not affect the formation of a continuous TiN layer nor surface roughness. Finally, the critical energy density leading to increased surface roughness was calculated.


2013 ◽  
Vol 668 ◽  
pp. 283-287
Author(s):  
Sheng Feng Zhou ◽  
Xiao Qin Dai

In order to characterize the dissolution of cast WC particles in Ni-based WC coatings by laser induction hybrid rapid cladding, NiCrBSi+50 wt.% WC coatings are produced on A3 steel by low and high speed laser induction hybrid cladding (LIHC). When laser scanning speed is only 600 mm/min, the crack-free coating has pores and its dilution is as high as 45%. At the bottom of coating, the cast WC particles are dissolved completely and the herringbone M6C eutectics are precipitated. In the center of coating, the cast WC particles are also dissolved completely and the acicular, blocky and dendritic carbides with relatively low hardness are precipitated. At two sides of coating, some cast WC particles are dissolved partially and interact with Ni-based alloy to form an alloyed reaction layer, while others preserve the primary eutectic structure and high hardness. When laser scanning speed and powder feeding rate are increased to 1500 mm/min and 85.6 g/min, the coating has cracks but no pores. Its dilution can be markedly decreased to 7.8%. Moreover, a majority of WC particles are still composed of primary eutectic structure and keep their high hardness, which can play a positive role in strengthening Ni-based metallic matrix.


2021 ◽  
Vol 410 ◽  
pp. 203-208
Author(s):  
I.S. Loginova ◽  
N.A. Popov ◽  
A.N. Solonin

In this work we studied the microstructure and microhardness of standard AA2024 alloy and AA2024 alloy with the addition of 1.5% Y after pulsed laser melting (PLM) and selective laser melting (SLM). The SLM process was carried out with a 300 W power and 0.1 m/s laser scanning speed. A dispersed microstructure without the formation of crystallization cracks and low liquation of alloying elements was obtained in Y-modified AA2024 aluminum alloy. Eutectic Al3Y and Al8Cu4Y phases were detected in Y-modified AA2024 aluminum alloy. It is led to a decrease in the formation of crystallization cracks The uniform distribution of alloying elements in the yttrium-modified alloy had a positive effect on the quality of the laser melting zone (LMZ) and microhardness.


2020 ◽  
Vol 861 ◽  
pp. 35-40
Author(s):  
Yu Liu ◽  
Tian Hao Xu ◽  
Ying Liu ◽  
Hai Cheng Zhang ◽  
Xing Xing Li ◽  
...  

The surface of 45 steel is quenched by CO2 laser with scanning speed 1000 mm/min and different laser power 1000W, 1200W, 1400W, 1600W and 1800W. Experiments are carried out to analyze microstructure, friction and wear properties of quenched 45 steel. The results show that the quenching layer thickness increases gradually with the increase of laser power,and the maximum value of quenching layer hardness increases first and then decreases. When the laser power is 1600W, the maximum hardness value is 883HV0.5. But when the laser power is 1800W, the hardness of quenching layer becomes to decrease. The reason is the surface of 45 steel becomes to melt. The wear volume increases first and then decreases too. When laser power is 1600W, the minimum wear volume is 0.08mm3, which is 6.4% to the wear volume of 45 steel matrix without laser quenching. Therefore, better microstructure and properties of 45 steel can be obtained when laser scanning speed is 1000mm/min and laser power is 1600W.


Metals ◽  
2019 ◽  
Vol 9 (8) ◽  
pp. 912 ◽  
Author(s):  
Yuelong Yu ◽  
Min Zhang ◽  
Yingchun Guan ◽  
Peng Wu ◽  
Xiaoyu Chong ◽  
...  

The surface of bainitic steel was remelted by fiber laser, and the microstructure and mechanical properties of the melted layer were studied by scanning electron microscopy (SEM), transmission electron microscopy (TEM), a nanoindentation instrument, and wear equipment. The study of changing the laser scanning speed showed that the depth of the melted layer increases with decreases of the laser scanning speed. The wear-resistance property increased by 55% compared with the matrix and decreased with the reduction of laser scanning speed within a certain range. In the study of changing the laser-scanning space, the thermal effect of laser melting in the back channel on the front channel was further validated. At the same time, it was found that the solidified layer surface of hardness alternating with softness can be obtained by appropriately expanding the scanning space, which is conducive to improving the wear-resistant properties of the steel surface, and properly improving the production efficiency of the laser remelting treatment.


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