scholarly journals Preparation of Hydroxytyrosol by Acid Hydrolysis from Olive Leaves

Separations ◽  
2021 ◽  
Vol 8 (9) ◽  
pp. 159
Author(s):  
Yujie Wang ◽  
Siyuan Luo ◽  
Jieling Luo ◽  
Jipeng Qu ◽  
Shiling Feng ◽  
...  
Keyword(s):  
Hydrochloric Acid ◽  
Flow Rate ◽  
Bioactive Compound ◽  
Extraction Process ◽  
Extraction Methods ◽  
Hydrochloric Acid Concentration ◽  
Macroporous Resin ◽  
Olive Leaves ◽  
Ultrasonic Time ◽  
Optimal Extraction Condition

Hydroxytyrosol (HT) is the main bioactive compound in olive leaves. However, olive leaves contain a lower level of HT and the extraction process of HT was rarely optimized. In this study, compared with two extraction methods, ultrasound was found to have a positive effect on improving the yield of HT. Therefore, ultrasound was used to assist hydrolysis of hydrochloric acid to extract HT from olive leaves. Response surface method and macroporous resins were applied to optimize the extraction process as well as enrichment of HT. The results showed that ultrasonic extraction time had a significant effect on the yield and the optimal extraction conditions were obtained: ultrasonic time was 120 min, hydrochloric acid concentration was 1.60 mol/L and the liquid-to-material ratio was 60.00 mL/g. Under the optimal extraction condition, the yield of HT was 14.11 ± 0.12 mg/g. NKA-Ⅱ macroporous resin was proved to be a suitable resin to enrich HT from extraction solution. The optimal condition for enriching HY was 250 mL of loading solution at the flow rate of 1.5 mL/min with 40 mL volume of 75% ethanol–eluent at a flow rate of 1.0 mL/min. The concentration of HT changed from 2.27% to 9.25% after enrichment by macroporous resin.

scholarly journals Solvent Extraction of Molybdenum from Hydrochloric Acid Solutions with Tri-Octyl Phosphine Oxide: Comparison between Conventional and Microwave-Assisted Extraction Techniques

2020 ◽  
Vol 21 (1) ◽  
pp. 65-79
Author(s):  
Ahmed Boucherit ◽  
◽  
Hussein Khalaf ◽  
Keyword(s):  
Solvent Extraction ◽  
Hydrochloric Acid ◽  
Phosphine Oxide ◽  
Irradiation Time ◽  
Extraction Process ◽  
Hydrochloric Acid Concentration ◽  
Microwave Assisted Extraction ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Hydrochloric Acid Solutions

In this paper, the solvent extraction of molybdenum from 0.01-1 M aqueous hydrochloric acidusing tri-octyl phosphine oxide (TOPO) as solvent diluted with n-hexane has been investigated. The extraction efficiencies of TOPO inthe extraction of molybdenum werecarried out using conventional extraction and microwave-assisted extraction (MAE) techniques.Molybdenum extraction efficiency wasdetermined by varying separately the different parameters affecting the extraction process including agitationtime, hydrochloric acid concentration, solventconcentration (in the organic phase), as well as the irradiation time and microwave power.The MAE technique greatly enhanced the solvent extraction of molybdenum where high extraction percentageswere obtained under favorable conditions. In some cases, thepercentages extraction of molybdenum obtained with two methods were comparable.The use of MAE technique also showed obvious advantages in terms of a drastic reduction of the extraction time as it was shortened from 15 min to 10 s in comparison with conventional solvent extraction method.

scholarly journals Increasing Yield and Antioxidative Performance of Litchi Pericarp Procyanidins in Baked Food by Ultrasound-Assisted Extraction Coupled with Enzymatic Treatment

Molecules ◽  
2018 ◽  
Vol 23 (9) ◽  
pp. 2089 ◽  
Author(s):  
Shuyi Li ◽  
Yanjie Yang ◽  
Junsheng Li ◽  
Zhenzhou Zhu ◽  
Jose Lorenzo ◽  
...  
Keyword(s):  
Extraction Process ◽  
Extraction Methods ◽  
Enzyme Concentration ◽  
Ultrasonic Power ◽  
Ultrasound Assisted Extraction ◽  
Solid Ratio ◽  
Assisted Extraction ◽  
Ultrasonic Time ◽  
Functional Components ◽  
Litchi Pericarp

Extraction with organic solvents is a traditional method to isolate bioactive compounds, which is energy-wasting and time-consuming. Therefore, enzyme and ultrasound treatments were combined to assist the extraction of oligomeric procyanidins from litchi pericarp (LPOPC), as an innovative approach to replace conventional extraction methods. Under optimum conditions (enzyme concentration 0.12 mg/mL, ultrasonic power 300 W, ultrasonic time 80 min, and liquid/solid ratio 10 mL/g), the yield of LPOPC could be improved up to 13.5%. HPLC analysis indicated that the oligomeric procyanidins (OPC) content of LPOPC from proposed extraction was up to 89.6%, mainly including (−)-epicatechin, procyanidin A1, A2, and A-type procyanidin trimer. Moreover, LPOPC powder was added in baked food to inhibit the lipid peroxidation. It was found that 0.2% (w/w) of LPOPC could maintain the quality of cookies in the first 7 days, by decreasing the peroxide values. The procyanidin dimers and trimers in LPOPC played more important roles as antioxidants compared to monomers during storage. The results also showed that the combined extraction process can be considered as a useful and efficient method for the extraction of functional components from other plant sources.

Extraction of Mogroside and Limonin with Different Extraction Methods and its Modeling

2012 ◽  
Vol 8 (2) ◽  
Author(s):  
Jing Liu ◽  
Can Liu ◽  
Yonghai Rong ◽  
Long Rong
Keyword(s):  
Thin Film ◽  
Natural Products ◽  
Mass Production ◽  
Extraction Process ◽  
Extraction Methods ◽  
Ultrasonic Extraction ◽  
Citrus Reticulata ◽  
Comparison Of Methods ◽  
Economical Method ◽  
Siraitia Grosvenorii

The extraction yields of mogroside from Siraitia grosvenorii fruits and limonin from orange (Citrus reticulata Blanco) seeds were compared with different extraction methods, respectively. Maceration extraction, stirring extraction, ultrasonic extraction and flash extraction were used for the extraction. The extraction process was modeled using the concept of thin film which provides the resistance to transfer. The results showed that the maximum yields of mogroside (4.11%) and limonin (0.65%) were obtained by ultrasonic extraction and flash extraction respectively. Owing to its shorter extraction time, flash extraction would be an economical method for the mass production of triterpenes from natural products. The model was found to be fit for the comparison of methods for the extraction and provided good correlation of the data. The model could be mainly used in the practical extraction process.

scholarly journals Phycocyanin content and nutritional profile of Arthrospira platensis from Mexico: efficient extraction process and stability evaluation of phycocyanin

BMC Chemistry ◽  
2021 ◽  
Vol 15 (1) ◽  
Author(s):  
Sanghamitra Khandual ◽  
Edgar Omar Lopez Sanchez ◽  
Hugo Espinosa Andrews ◽  
Jose Daniel Padilla de la Rosa
Keyword(s):  
Storage Temperature ◽  
Extraction Process ◽  
Arthrospira Platensis ◽  
Extraction Methods ◽  
Precipitation Method ◽  
Partial Purification ◽  
Natural Food ◽  
Solvent Ratio ◽  
C Storage ◽  
Dry Biomass

AbstractPhycocyanin is a blue natural food colorant with multiple health benefits. Here we propose an efficient phycocyanin extraction method from Arthrospira platensis from Mexico. Three extraction methods were applied to optimize the extraction process, using water and buffer as solvents, with three pH values at two agitation times. The highest phycocyanin, 54.65 mg/g, was extracted from dry biomass with water as a solvent using an ultrasonication bar. The optimum condition of extraction was determined to be 1:50 biomass/solvent ratio for dry biomass, with the freeze/thaw method for 20 min repeated twice, and then agitated at 120 rpm for 24 h. The phycocyanin content was 48.88 mg/g biomass, with a purity of 0.47. For scalable phycocyanin productivity, the sonication method is recommended as there is no statistical difference. The phycocyanin stability was best at − 20 °C storage temperature at pH 7 for 35 days. Partial purification with ammonium sulfate was found to be suitable as a fractional precipitation method, first at 0–20% and then 20–65%, to get purity nearly 1. Total protein was found to be 55.52%, and total amino acids after phycocyanin extraction was 33%. The maximum phycocyanin yield using water as a solvent was the most interesting result regardless of the method used for extraction.

scholarly journals Integrated Metabolomics and Transcriptomics Using an Optimised Dual Extraction Process to Study Human Brain Cancer Cells and Tissues

Metabolites ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 240
Author(s):  
Alison Woodward ◽  
Alina Pandele ◽  
Salah Abdelrazig ◽  
Catherine A. Ortori ◽  
Iqbal Khan ◽  
...  
Keyword(s):  
Metabolic Pathways ◽  
Extraction Method ◽  
Limit Of Detection ◽  
Rna Extraction ◽  
Extraction Process ◽  
Extraction Methods ◽  
Serum Starvation ◽  
Extraction Techniques ◽  
Metabolic Genes ◽  
Dual Extraction

The integration of untargeted metabolomics and transcriptomics from the same population of cells or tissue enhances the confidence in the identified metabolic pathways and understanding of the enzyme–metabolite relationship. Here, we optimised a simultaneous extraction method of metabolites/lipids and RNA from ependymoma cells (BXD-1425). Relative to established RNA (mirVana kit) or metabolite (sequential solvent addition and shaking) single extraction methods, four dual-extraction techniques were evaluated and compared (methanol:water:chloroform ratios): cryomill/mirVana (1:1:2); cryomill-wash/Econospin (5:1:2); rotation/phenol-chloroform (9:10:1); Sequential/mirVana (1:1:3). All methods extracted the same metabolites, yet rotation/phenol-chloroform did not extract lipids. Cryomill/mirVana and sequential/mirVana recovered the highest amounts of RNA, at 70 and 68% of that recovered with mirVana kit alone. sequential/mirVana, involving RNA extraction from the interphase of our established sequential solvent addition and shaking metabolomics-lipidomics extraction method, was the most efficient approach overall. Sequential/mirVana was applied to study a) the biological effect caused by acute serum starvation in BXD-1425 cells and b) primary ependymoma tumour tissue. We found (a) 64 differentially abundant metabolites and 28 differentially expressed metabolic genes, discovering four gene-metabolite interactions, and (b) all metabolites and 62% lipids were above the limit of detection, and RNA yield was sufficient for transcriptomics, in just 10 mg of tissue.

Surface Morphology and the Adsorptive Behavior of Coconut Active Carbon

2013 ◽  
Vol 690-693 ◽  
pp. 1029-1032
Author(s):  
Xiao Qiang Li ◽  
Li Juan Lan
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Hydrochloric Acid ◽  
Active Carbon ◽  
Adsorption Process ◽  
Hydrochloric Acid Concentration ◽  
Impregnation Method ◽  
Adsorption Experiment ◽  
Adsorptive Behavior ◽  
Scanning Electron

Active carbon modified by hydrochloric acid was prepared with impregnation method. The synthesized material was characterized by scanning electron microscopy. It was proved that plenty of pores with diameter of about 5-10μm were exist on the surface of active carbon. The adsorption process with toluene was performed over the modified active carbon to investigate the adsorptive efficiency. For comparison, other porous materials were also performed the adsorption experiment. The results showed that active carbon modified by hydrochloric acid has high adsorptive efficiency for toluene. The results proved that adsorptive performance of active carbon increased with the hydrochloric acid concentration.

Experimental Study on Concentrating Scandium by Leaching from Associated Scandium Ore

2013 ◽  
Vol 734-737 ◽  
pp. 1033-1036
Author(s):  
Gui Fang Zhang ◽  
Peng Yan ◽  
Qing Rong Yang
Keyword(s):  
Experimental Study ◽  
Particle Size ◽  
Hydrochloric Acid ◽  
Acid Concentration ◽  
Hydrochloric Acid Concentration ◽  
Leaching Rate ◽  
Optimal Conditions ◽  
Research Results ◽  
Solid Ratio ◽  
Leaching Residue

Based on the benefication of the complex silicate ore containing scandium, the research about aid-leaching agent used in the leaching of the scandium concentrate was been conducted. And the suitable leaching agent and aid-leaching agent which the useful ions entered into leaching liquid and the harmful ions were kept in leaching residue were been found according to the experiment results. For the scandium of sample existed various complex silicate ore as isomorphism form, the research has adopted hydrochloric acid with aid-leaching agent to dissociate the silicate ore and make scandium entering into solution. The research results has shown that the scandium leaching rate could reach 92.06% under the optimal conditions which the hydrochloric acid concentration is 22.8%, the dosage of aid leaching agent is 6%, liquid solid ratio is 4:1, particle size of leaching material totally is less than 0.15mm and leaching time is 8h.

Mercury Removal from Fish Protein Concentrate

1972 ◽  
Vol 29 (12) ◽  
pp. 1777-1779 ◽  
Author(s):  
L. W. Regier
Keyword(s):  
Hydrochloric Acid ◽  
Acid Concentration ◽  
Extraction Procedure ◽  
Extraction Process ◽  
Alcohol Concentration ◽  
Mercury Removal ◽  
Protein Concentrate ◽  
Fish Protein ◽  
Proteinaceous Food

The potential reclamation of mercury contaminated proteinaceous food by an extraction procedure such as employed in making fish protein concentrate was investigated. The addition of hydrochloric acid to the isopropanol extractant was found to give removals as high as 93% from dry swordfish protein concentrate. The normal Halifax isopropanol extraction process did not effect any significant removal of the mercury.Preliminary studies of the variables indicated acid concentration, kind of alcohol (ethanol and isopropanol), alcohol concentration, extractant volume, and number of extractions were important in the extraction.

Effects of high hydrochloric acid concentration on aniline chemical polymerization

Polymer ◽  
1997 ◽  
Vol 38 (20) ◽  
pp. 5247-5250 ◽  
Author(s):  
Gustavo M. Morales ◽  
Marcos Llusa ◽  
Maria C. Miras ◽  
Cesar Barbero
Keyword(s):  
Hydrochloric Acid ◽  
Acid Concentration ◽  
Hydrochloric Acid Concentration ◽  
Chemical Polymerization

scholarly journals Comparison between Two Solid-Liquid Extraction Methods for the Recovery of Steviol Glycosides from Dried Stevia Leaves Applying a Numerical Approach

Processes ◽  
2018 ◽  
Vol 6 (8) ◽  
pp. 105 ◽  
Author(s):  
Monica Gallo ◽  
Andrea Formato ◽  
Gaetano Formato ◽  
Daniele Naviglio
Keyword(s):  
Stevia Rebaudiana ◽  
Value Added ◽  
Numerical Approach ◽  
Extraction Process ◽  
Extraction Methods ◽  
Liquid Extraction ◽  
Steviol Glycosides ◽  
Stevia Rebaudiana Bertoni ◽  
Solid Liquid Extraction ◽  
Solid Liquid

Abstract: Stevia rebaudiana Bertoni is a perennial shrub belonging to the Asteraceae family. The leaves contain a mixture of steviol glycosides with extraordinary sweetening properties, among which the most important are stevioside and rebaudioside A. These components have a high sweetening power, which is about 300 times that of sucrose, and a negligible calorie content. However, their extraction and purification are not easy. In this paper, the extraction technique under cyclic pressure, known as rapid solid-liquid dynamic extraction (RSLDE), was compared using a Naviglio extractor (NE) with conventional maceration. The aim was to identify an efficient and economically viable method for obtaining high amounts of steviol glycosides in a short time. Furthermore, a numerical model was set up for the solid-liquid extraction process of value-added compounds from natural sources. Several parameters must be evaluated in relation to the characteristics of the parts of the plant subjected to extraction. Therefore, since diffusion and osmosis are highly dependent on temperature, it is necessary to control the temperature of the extraction system. On the other hand, the final aim of this work was to provide a scientific and quantitative basis for RSLDE. Therefore, the results obtained from stevia extracts using the corresponding mathematical model allowed hypothesizing the application of this model to the extraction processes of other vegetable matrices.

Sign in / Sign up

Export Citation Format

Share Document