Internal stress in titanium G4 before and after metal forming in increased temperature and shot-peening determinated by sin2ψ method

2020 ◽  
Vol 25 (1-2) ◽  
pp. 31-37
Author(s):  
Jerzy Jeleńkowski ◽  
Joanna Zdunek ◽  
Piotr Nawrocki ◽  
Grzegorz Mońka
Keyword(s):  
Shot Peening ◽  
Metal Forming ◽  
Source Material ◽  
Internal Stresses ◽  
Ray Method ◽  
X Ray ◽  
Plastic Processing ◽  
Before And After ◽  
Titanium Grade ◽  
Structure Diversity

The article presents the assessment of the macroscopic residual stresses in titanium, grade G4, determined by the sin2ψ X-ray method. The values of stresses measured in the source material and in samples of sub/microstructure obtained after plastic processing in the Gleeble plastometer at the temperature 875 K, optimized strain ε and strain velocity έ were compared. After shot peening, regardless of the structure diversity, the roughness of the polished surfaces of the samples sometimes increased even about 10 times. Small differences occurred in hardness, higher in the more plastic sub/microstructure, which was also reflected in the magnitude of internal stresses.

Identification and Analysis of Residual Stresses in the Axisymmetric Workpiece Existing before and after Machining

2016 ◽  
Vol 686 ◽  
pp. 33-38 ◽  
Author(s):  
Tadeusz Otko ◽  
Wojciech Zębala
Keyword(s):  
Point Of View ◽  
Internal Stresses ◽  
Entire Volume ◽  
Shape Accuracy ◽  
Workpiece Surface ◽  
Plastic Processing ◽  
Machining Allowance ◽  
Before And After ◽  
The Impact

Semi-manufactured parts dedicated for precise machining often have internal stresses which have remained after previous cutting and plastic processing. These stresses reside in a fixed state of balance over the entire volume of the workpiece. Removal of the machining allowance is associated with a change in the state of balance and deformation of the workpiece, which affect its dimensional and shape accuracy. The study, involving non-stress removal of precisely defined volume of the machining allowance and determination of the impact of this treatment on the deformation of the workpiece surface is presented. It is important from the point of view of dimensional tolerance of the axially symmetrical workpiece, finally processed by turning.

Influence of Ethanol as a Carburizing Agent on Carbon Surface Concentration and Microstructure of DIN 17NiCrMo7 Steel Gears

2015 ◽  
Author(s):  
Rogério Catalão ◽  
Omar Khayyam Ribas ◽  
José Rubens G. Carneiro ◽  
Érico Freitas ◽  
Larissa Vilela Costa ◽  
...  
Keyword(s):  
Shot Peening ◽  
Surface Concentration ◽  
Carbon Surface ◽  
Quantitative Chemical Analysis ◽  
X Ray Diffraction ◽  
Austenite Grain Size ◽  
X Ray ◽  
Transmission Electron ◽  
Before And After ◽  
The Impact

In the present work, the addition of ethanol to endothermic gas during the carburizing process of DIN 17NiCrMo7 steel gears was investigated with the objective of determining the impact on carbon surface concentration and microstructure. The materials were carburized at 870°C and 930°C, oil quenched, tempered and subsequently shot peened. Carburizing was carried out in a continuous industrial furnace for a total of 280 min. After quenching and tempering, the in-depth carbon concentrations were determined through quantitative chemical analysis and the resulting profiles were modeled in order to obtain carbon diffusivity constants. The amount of retained austenite and austenite grain size, determined by X-ray diffraction and optical microscopy, were found to increase with carburizing temperature. Residual stress profiles were also determined by X-ray diffraction before and after the shot-peening process. The microstructure of the specimens was further investigated by transmission electron microscopy, which revealed the presence of BCC martensite before and after shot-peening. The enrichment of the endothermic gas carrier with ethanol could be shown to be a viable option, allowing for surface concentrations of up to 0.8%C.

The alkali feldspars of the Ardara pluton, Donegal

1966 ◽  
Vol 35 (273) ◽  
pp. 693-703 ◽  
Author(s):  
A. Hall
Keyword(s):  
Structural State ◽  
Significant Variation ◽  
Reciprocal Lattice ◽  
Bulk Composition ◽  
Alkali Feldspar ◽  
Ray Method ◽  
X Ray ◽  
Before And After ◽  
Different Parts ◽  
Alkali Feldspars

SummaryThe alkali feldspars in the Ardara pluton are microcline- and orthoclase-microperthites. Their compositions have been determined by the 20 X-ray method, both before and after homogenization. The bulk compositions are very rich in potassium as a result of postmagmatic recrystallization of the alkali feldspar. There is no significant variation in either the bulk composition or the composition of the potassic phase in different parts of the intrusion. The structural state of the feldspars has been studied by measurement of 2V and obliquity of the potassic phases, and the reciprocal lattice angles α* and γ* of the potassic and sodic phases in selected crystals. Most of the specimens contain near-maximum microcline, but there is a decrease in the obliquity of the potassic phase at the eastern end of the intrusion. This can be related to the subsequent intrusion of the Main Donegal Granite.

scholarly journals Influence of Sandblasting Process on Tribological Properties of Titanium Grade 4 in Artificial Saliva for Dentistry Applications

Materials ◽  
2021 ◽  
Vol 14 (24) ◽  
pp. 7536
Author(s):  
Patrycja Osak ◽  
Joanna Maszybrocka ◽  
Maciej Zubko ◽  
Jan Rak ◽  
Sylwia Bogunia ◽  
...  
Keyword(s):  
Residual Stress ◽  
Dental Implants ◽  
Artificial Saliva ◽  
Stress Test ◽  
Wear Test ◽  
Polished Surface ◽  
X Ray ◽  
Wear And Friction ◽  
Before And After ◽  
Titanium Grade

Titanium Grade 4 (Ti G4) is widely used in medicine for dental implants. The failure-free life of implants depends on their properties such as resistance to wear and friction processes. This paper presents an analysis of the influence of sandblasting on tribological wear of commercial dental implants made of TiG4 in artificial saliva. Tribological wear measurements were performed in a reciprocating motion in the ball-on-disc system. The scanning electron microscopy/energy-dispersive X-ray spectroscopy (SEM/EDS) method was used to characterize the surface of the implants before and after the tribological wear test. The microhardness of Ti G4 was measured before and after sandblasting by the Vickers method. The contact angle was determined by the method of sitting drop in air. The residual stress test using the X-Ray Diffraction (XRD) single-{hkl} sin2ψ method was carried out. The compressive residual stress of 324(7) MPa and surface hardening of Ti G4 was revealed after sandblasting with Al2O3 particles of 53–75 μm in diameter. It was found that sandblasting changes the surface wettability of Ti G4. The intermediate wettability of the mechanically polished surface and the hydrophobicity of the sandblasted surface was revealed. Sandblasting reduces the tribological wear and friction coefficient of Ti G4 surface in saliva. The three-body abrasion wear mechanism was proposed to explain the tribological wear of Ti G4 in saliva.

Phase Transformations in Ti-7w/oMo-3w/oMe Alloy

1974 ◽  
Vol 32 ◽  
pp. 514-515
Author(s):  
S. Fujishiro
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Transmission Electron Microscopy ◽  
Tensile Strength ◽  
Mechanical Processing ◽  
Ray Method ◽  
X Ray ◽  
Transmission Electron ◽  
Water Quench ◽  
Alpha Beta

The mechanical properties of three titanium alloys (Ti-7Mo-3Al, Ti-7Mo- 3Cu and Ti-7Mo-3Ta) were evaluated as function of: 1) Solutionizing in the beta field and aging, 2) Thermal Mechanical Processing in the beta field and aging, 3) Solutionizing in the alpha + beta field and aging. The samples were isothermally aged in the temperature range 300° to 700*C for 4 to 24 hours, followed by a water quench. Transmission electron microscopy and X-ray method were used to identify the phase formed. All three alloys solutionized at 1050°C (beta field) transformed to martensitic alpha (alpha prime) upon being water quenched. Despite this heavily strained alpha prime, which is characterized by microtwins the tensile strength of the as-quenched alloys is relatively low and the elongation is as high as 30%.

Evaluation of Freezing Methods by Low Temperature X-Ray Diffraction

1977 ◽  
Vol 35 ◽  
pp. 330-333
Author(s):  
T. Gulik-Krzywicki ◽  
M.J. Costello
Keyword(s):  
Biological Materials ◽  
Molecular Organization ◽  
X Ray Diffraction ◽  
Glass Capillary ◽  
X Ray ◽  
Rate Dependent ◽  
Before And After ◽  
Freeze Etching ◽  
Diffraction Patterns ◽  
Set Up

Freeze-etching electron microscopy is currently one of the best methods for studying molecular organization of biological materials. Its application, however, is still limited by our imprecise knowledge about the perturbations of the original organization which may occur during quenching and fracturing of the samples and during the replication of fractured surfaces. Although it is well known that the preservation of the molecular organization of biological materials is critically dependent on the rate of freezing of the samples, little information is presently available concerning the nature and the extent of freezing-rate dependent perturbations of the original organizations. In order to obtain this information, we have developed a method based on the comparison of x-ray diffraction patterns of samples before and after freezing, prior to fracturing and replication.Our experimental set-up is shown in Fig. 1. The sample to be quenched is placed on its holder which is then mounted on a small metal holder (O) fixed on a glass capillary (p), whose position is controlled by a micromanipulator.

The Precipitation of Si in AlCuSi Thin Films

1973 ◽  
Vol 31 ◽  
pp. 34-35 ◽  
Author(s):  
R. M. Anderson
Keyword(s):  
Electron Microscopy ◽  
Thin Films ◽  
Heat Treatment ◽  
Solid Solution ◽  
Integrated Circuit ◽  
Copper Film ◽  
Solution Concentration ◽  
X Ray ◽  
Silicon Thin Films ◽  
Before And After

Aluminum-copper-silicon thin films have been considered as an interconnection metallurgy for integrated circuit applications. Various schemes have been proposed to incorporate small percent-ages of silicon into films that typically contain two to five percent copper. We undertook a study of the total effect of silicon on the aluminum copper film as revealed by transmission electron microscopy, scanning electron microscopy, x-ray diffraction and ion microprobe techniques as a function of the various deposition methods.X-ray investigations noted a change in solid solution concentration as a function of Si content before and after heat-treatment. The amount of solid solution in the Al increased with heat-treatment for films with ≥2% silicon and decreased for films <2% silicon.

A New Polyethylene Corrosion Protecting Coating with Ion Selectivity

2011 ◽  
Vol 314-316 ◽  
pp. 273-278
Author(s):  
Yu Hua Dong ◽  
Ke Ren ◽  
Qiong Zhou
Keyword(s):  
Ion Selectivity ◽  
Nano Particles ◽  
Ammonium Bromide ◽  
Linear Low Density Polyethylene ◽  
X Ray Diffraction ◽  
Sulfosalicylic Acid ◽  
X Ray ◽  
Chemically Modified ◽  
Before And After ◽  
Industrial Standards

Linear low density polyethylene (LLDPE) was chemically modified with grafting maleic anhydride (MAH) monomer on its backbone by melting blending. Nano-particles SiO2 was modified by cationic surfactant hexadecyl trimethyl ammonium bromide (CTAB) and anionic surfactant sulfosalicylic acid (SSA) and added to PE coating respectively. Measurement of membrane potential showed that the coating containing modified SiO2 nano-particles had characteristic of ion selectivity. The properties of the different coatings were investigated according to relative industrial standards. Experimental results indicated that PE coating with ion selectivity had better performances, such as adhesion strength, cathodic disbonding and anti-corrosion, than those of coating without ion selectivity. Crystal structure of the coatings before and after alkali corrosion was characterized by Fourier transform infrared spectra (FTIR) and X-ray diffraction (XRD). Structure of the coating without ion selectivity was damaged by NaOH alkali solution, causing mechanical properties being decreased. And the structure of the ion selective coatings was not affected.

scholarly journals Synthesis of Novel Arginine-Based Flame Retardant and Its Application in Lyocell Fabric

Molecules ◽  
2021 ◽  
Vol 26 (12) ◽  
pp. 3588
Author(s):  
Jiayi Chen ◽  
Yansong Liu ◽  
Jiayue Zhang ◽  
Yuanlin Ren ◽  
Xiaohui Liu
Keyword(s):  
Fourier Transform ◽  
Heat Release ◽  
Flame Retardant ◽  
Photoelectron Spectroscopy ◽  
Fourier Transform Infrared ◽  
Ftir Analysis ◽  
Excellent Thermal Stability ◽  
X Ray ◽  
Cone Calorimeter Test ◽  
Before And After

Lyocell fabrics are widely applied in textiles, however, its high flammability increases the risk of fire. Therefore, to resolve the issue, a novel biomass-based flame retardant with phosphorus and nitrogen elements was designed and synthesized by the reaction of arginine with phosphoric acid and urea. It was then grafted onto the lyocell fabric by a dip-dry-cure technique to prepare durable flame-retardant lyocell fabric (FR-lyocell). X-ray photoelectron spectroscopy (XPS) and Fourier-transform infrared spectroscopy (FTIR) analysis demonstrated that the flame retardant was successfully introduced into the lyocell sample. Thermogravimetric (TG) and Raman analyses confirmed that the modified lyocell fabric featured excellent thermal stability and significantly increased char residue. Vertical combustion results indicated that FR-lyocell before and after washing formed a complete and dense char layer. Thermogravimetric Fourier-transform infrared (TG-FTIR) analysis suggested that incombustible substances (such as H2O and CO2) were produced and played a significant fire retarding role in the gas phase. The cone calorimeter test corroborated that the peak of heat release rate (PHRR) and total heat release (THR) declined by 89.4% and 56.4%, respectively. These results indicated that the flame retardancy of the lyocell fabric was observably ameliorated.

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