Effect of Laser Scan Speed on Microstructure and Mircohardness on Titanium Clad Magnesium

2021 ◽  
pp. 75-84
Author(s):  
Kannan Ganesa Balamurugan ◽  
Muthukannan Duraiselvam
Keyword(s):  
Author(s):  
C.J. Stuart ◽  
B.E. Viani ◽  
J. Walker ◽  
T.H. Levesque

Many techniques of imaging used to characterize petroleum reservoir rocks are applied to dehydrated specimens. In order to directly study behavior of fines in reservoir rock at conditions similar to those found in-situ these materials need to be characterized in a fluid saturated state.Standard light microscopy can be used on wet specimens but depth of field and focus cannot be obtained; by using the Tandem Scanning Confocal Microscope (TSM) images can be produced from thin focused layers with high contrast and resolution. Optical sectioning and extended focus images are then produced with the microscope. The TSM uses reflected light, bulk specimens, and wet samples as opposed to thin section analysis used in standard light microscopy. The TSM also has additional advantages: the high scan speed, the ability to use a variety of light sources to produce real color images, and the simple, small size scanning system. The TSM has frame rates in excess of normal TV rates with many more lines of resolution. This is accomplished by incorporating a method of parallel image scanning and detection. The parallel scanning in the TSM is accomplished by means of multiple apertures in a disk which is positioned in the intermediate image plane of the objective lens. Thousands of apertures are distributed in an annulus, so that as the disk is spun, the specimen is illuminated simultaneously by a large number of scanning beams with uniform illumination. The high frame speeds greatly simplify the task of image recording since any of the normally used devices such as photographic cameras, normal or low light TV cameras, VCR or optical disks can be used without modification. Any frame store device compatible with a standard TV camera may be used to digitize TSM images.


Author(s):  
Dominique Carisetti ◽  
Nicolas Sarazin ◽  
Nathalie Labat ◽  
Nathalie Malbert ◽  
Arnaud Curutchet ◽  
...  

Abstract To improve the long-term stability of AlGaN/GaN HEMTs, the reduction of gate and drain leakage currents and electrical anomalies at pinch-off is required. As electron transport in these devices is both coupled with traps or surface states interactions and with polarization effects, the identification and localization of the preeminent leakage path is still challenging. This paper demonstrates that thermal laser stimulation (TLS) analysis (OBIRCh, TIVA, XIVA) performed on the die surface are efficient to localize leakage paths in GaN based HEMTs. The first part details specific parameters, such as laser scan speed, scan direction, wavelength, and laser power applied for leakage gate current paths identification. It compares results obtained with Visible_NIR electroluminescence analysis with the ones obtained by the TLS techniques on GaN HEMT structures. The second part describes some failure analysis case studies of AlGaN/GaN HEMT with field plate structure which were successful, thanks to the OBIRCh technique.


2021 ◽  
Vol 7 (2) ◽  
pp. 48
Author(s):  
Vittorio Scardaci ◽  
Giuseppe Compagnini

Laser scribing has been proposed as a fast and easy tool to reduce graphene oxide (GO) for a wide range of applications. Here, we investigate laser reduction of GO under a range of processing and material parameters, such as laser scan speed, number of laser passes, and material coverage. We use Raman spectroscopy for the characterization of the obtained materials. We demonstrate that laser scan speed is the most influential parameter, as a slower scan speed yields poor GO reduction. The number of laser passes is influential where the material coverage is higher, producing a significant improvement of GO reduction on a second pass. Material coverage is the least influential parameter, as it affects GO reduction only under restricted conditions.


2021 ◽  
Vol 4 (1) ◽  
Author(s):  
Ozan Aktas ◽  
Yuji Yamamoto ◽  
Mehmet Kaynak ◽  
Anna C. Peacock

AbstractAdvanced solid-state devices, including lasers and modulators, require semiconductor heterostructures for nanoscale engineering of the electronic bandgap and refractive index. However, existing epitaxial growth methods are limited to fabrication of vertical heterostructures grown layer by layer. Here, we report the use of finite-element-method-based phase-field modelling with thermocapillary convection to investigate laser inscription of in-plane heterostructures within silicon-germanium films. The modelling is supported by experimental work using epitaxially-grown Si0.5Ge0.5 layers. The phase-field simulations reveal that various in-plane heterostructures with single or periodic interfaces can be fabricated by controlling phase segregation through modulation of the scan speed, power, and beam position. Optical simulations are used to demonstrate the potential for two devices: graded-index waveguides with Ge-rich (>70%) cores, and waveguide Bragg gratings with nanoscale periods (100–500 nm). Periodic heterostructure formation via sub-millisecond modulation of the laser parameters opens a route for post-growth fabrication of in-plane quantum wells and superlattices in semiconductor alloy films.


Author(s):  
Massimiliano Bonesso ◽  
Pietro Rebesan ◽  
Claudio Gennari ◽  
Simone Mancin ◽  
Razvan Dima ◽  
...  

AbstractOne of the major benefits of the Laser Powder Bed Fusion (LPBF) technology is the possibility of fabrication of complex geometries and features in only one-step of production. In the case of heat exchangers in particular, this is very convenient for the fabrication of conformal cooling channels which can improve the performance of the heat transfer capability. Yet, obtaining dense copper parts printed via LPBF presents two major problems: the high reflectivity of 1 μm (the wavelength of commonly used laser sources) and the high thermal conductivity of copper that limits the maximum local temperature that can be attained. This leads to the formation of porous parts.In this contribution, the influence of the particle size distribution of the powder on the physical and mechanical properties of parts produced via LPBF is studied. Three copper powders lots with different particle size distributions are used in this study. The effect on densification from two laser scan parameters (scan speed and hatching distance) and the influence of contours scans on the lateral surface roughness is reported. Subsequently, samples manufactured with the optimal process parameters are tested for thermal and mechanical properties evaluation.


2019 ◽  
Vol 813 ◽  
pp. 159-164
Author(s):  
Carlos Alberto Souto ◽  
Gustavo Faria Melo da Silva ◽  
Laura Angelica Ardila Rodriguez ◽  
Aline C. de Oliveira ◽  
Kátia Regina Cardoso

Coatings with high entropy alloys of the AlCoCrFeNiV system were obtained by selective laser melting on low carbon steel substrates. The effect of the variation of the Fe and V contents as well as the laser processing parameters in the development of the coating were evaluated. The coatings were obtained from the simple powder mixtures of the high purity elemental components in a planetary ball mill. The coatings were obtained by using CO2 laser with a power of 100 W, diameter of 0.16 mm, and scan speed varying from 3 to 12 mm/s. Phase constituents, microstructure and hardness were investigated by XRD, SEM, and microhardness tester, respectively. Wear resistance measurements were carried out by the micro-abrasion method using ball-cratering tests. The coatings presented good adhesion to the substrate and high hardness, of the order of 480 to 650 HV. Most homogeneous coating with nominal composition was obtained by using the higher scan speed, 12 mm/s. Vanadium addition increased hardness and gave rise to a high entropy alloy coating composed by BCC solid solutions. Ball cratering tests conducted on HEA layer showing improvement of material wear resistance, when compared to base substrate, decreasing up to 88% its wear rate, from 1.91x10-6 mm3/Nmm to 0.23x10-6 mm3/Nmm.


2021 ◽  
Author(s):  
SeHyuk Park ◽  
Hamad Alnuaimi ◽  
Anna Hayes ◽  
Madison Sitkiewicz ◽  
Umar Amjad ◽  
...  

Abstract Guided acoustic wave based techniques have been found to be very effective for damage detection, and both quantitative and qualitative characterization of materials. In this research, guided acoustic wave techniques are used for porosity evaluation of additively manufactured materials. A metal 3D printer, Concept Laser Mlab 200 R Cusing™, is used to manufacture 316L additively manufactured (AM) stainless steel specimens. Two levels of porosity are investigated in this study, which was controlled by a suitable combination of scan speed and laser power. The sample with lower level of porosity is obtained with a low scanning speed. Lead Zirconate Titanate (PZT) transducers are used to generate guided acoustic waves. The signal is excited and propagated through the specimens in a single sided transmission mode setup. Signal processing of the recorded signals for damage analysis involves both linear and nonlinear analyses. Linear ultrasonic parameters such as the time-of-flight and magnitude of the propagating waves are recorded. The nonlinear ultrasonic parameter, the Sideband Peak Count Index (SPC-I) is obtained by a newly developed nonlinear analysis technique. Results obtained for both specimens are analyzed and compared using both linear and nonlinear ultrasonic techniques. Finally, the effectiveness of SPC-I technique in monitoring porosity levels in AM specimens is discussed.


Author(s):  
J. C. Heigel ◽  
B. M. Lane

This work presents high speed thermographic measurements of the melt pool length during single track laser scans on nickel alloy 625 substrates. Scans are made using a commercial laser powder bed fusion machine while measurements of the radiation from the surface are made using a high speed (1800 frames per second) infrared camera. The melt pool length measurement is based on the detection of the liquidus-solidus transition that is evident in the temperature profile. Seven different combinations of programmed laser power (49 W to 195 W) and scan speed (200 mm/s to 800 mm/s) are investigated and numerous replications using a variety of scan lengths (4 mm to 12 mm) are performed. Results show that the melt pool length reaches steady state within 2 mm of the start of each scan. Melt pool length increases with laser power, but its relationship with scan speed is less obvious because there is no significant difference between cases performed at the highest laser power of 195 W. Although keyholing appears to affect the anticipated trends in melt pool length, further research is required.


1992 ◽  
Vol 70 (6) ◽  
pp. 1833-1837 ◽  
Author(s):  
Yan Xiang ◽  
Gilles Villemure

The cyclic voltammograms of tris (2,2′-bipyridyl) iron(II) ([Fe(bpy)3]2+) adsorbed in clay-modified electrodes made from a range of different smectites were recorded. In all cases, at low scan speed (1 mV/s), the initial anodic peak current was much larger than the initial cathodic peak current. Partial reduction of the clay structural iron further increased the initial anodic to cathodic current ratio, suggesting that the discrepancy between the charge transferred in the anodic and cathodic scans was due to a slow electron transfer between the clay structural Fe(II) and the oxidized bipyridyl cations. However, no clear quantitative relation was found between the measured FeO contents of the different clays and the observed excess anodic currents. In fact, of all the clays tested only one, montmorillonite SWy-1, contained enough Fe(II) for it to account for all of the excess anodic charge transferred in the initial scan.


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