scholarly journals Aluminum with dispersed nanoparticles by laser additive manufacturing

2019 ◽  
Vol 10 (1) ◽  
Author(s):  
Ting-Chiang Lin ◽  
Chezheng Cao ◽  
Maximilian Sokoluk ◽  
Lin Jiang ◽  
Xin Wang ◽  
...  
Keyword(s):  
Thermal Stability ◽  
Additive Manufacturing ◽  
Young’S Modulus ◽  
Young's Modulus ◽  
Pure Aluminum ◽  
Specific Yield ◽  
Ultrafine Grain ◽  
Layer By Layer ◽  
Laser Additive Manufacturing ◽  
Aluminum Powders

Abstract While laser-printed metals do not tend to match the mechanical properties and thermal stability of conventionally-processed metals, incorporating and dispersing nanoparticles in them should enhance their performance. However, this remains difficult to do during laser additive manufacturing. Here, we show that aluminum reinforced by nanoparticles can be deposited layer-by-layer via laser melting of nanocomposite powders, which enhance the laser absorption by almost one order of magnitude compared to pure aluminum powders. The laser printed nanocomposite delivers a yield strength of up to 1000 MPa, plasticity over 10%, and Young’s modulus of approximately 200 GPa, offering one of the highest specific Young’s modulus and specific yield strengths among structural metals, as well as an improved specific strength and thermal stability up to 400 °C compared to other aluminum-based materials. The improved performance is attributed to a high density of well-dispersed nanoparticles, strong interfacial bonding between nanoparticles and Al matrix, and ultrafine grain sizes.

scholarly journals Recent Studies and Developments in Titanium Biomaterials

2020 ◽  
Vol 321 ◽  
pp. 02004
Author(s):  
M. Ikedaa ◽  
M. Ueda ◽  
M. Ninomi
Keyword(s):  
Health Care ◽  
Additive Manufacturing ◽  
Titanium Alloys ◽  
Young’S Modulus ◽  
Young's Modulus ◽  
Layer By Layer ◽  
Metal Powders ◽  
Alloy Development ◽  
Dental Surgery ◽  
Artificial Bones

Titanium and its alloys have a high specific strength, excellent corrosion resistance, and good biocompatibility. Therefore, these alloys are adopted as raw materials for artificial bones and joints. Furthermore, these alloys are used as materials for dental surgery. In the development of alloy design, beta-type titanium alloys that possess a lower Young’s modulus than other types of titanium alloys, e.g., Ti-6Al-4V alpha-beta-type alloys, are being actively investigated worldwide. Based on these studies, titanium-niobium-tantalum and zirconium system alloys were developed. For example, Ti-29Nb-13Ta-4.6Zr alloy has a low Young’s modulus, excellent biocompatibility, and improved mechanical properties. Many researchers are actively investigating surface modifications and surface treatments. Additive manufacturing, namely 3D printing, wherein metal powders are piled up layer by layer to produce goods without a mold, has attracted attention in many fields, including manufacture of implants, especially porous structural implants with a low Young’s modulus. It is very important that titanium and its alloys be applied to health-care goods, e.g., wheelchairs and prostheses. Therefore, we herein consider four topics: alloy development, coating and surface modification, additive manufacturing, and health care applications.

Basis für den industriellen 3D-Druck in Stahl/Basics for industrial 3D printing for steel - Contribution to additive manufacturing of complex products in multi-variant and functional skeleton construction

2017 ◽  
Vol 107 (06) ◽  
pp. 415-419
Author(s):  
M. Hillebrecht ◽  
V. Uhlenwinkel ◽  
A. von Hehl ◽  
H. Zapf ◽  
B. Schob
Keyword(s):  
Additive Manufacturing ◽  
Functional Integration ◽  
Complex Geometries ◽  
Layer By Layer ◽  
Laser Additive Manufacturing ◽  
Complex Products ◽  
Metal Parts ◽  
Laser Joining ◽  
Automation Technology ◽  
Selection Of

Mithilfe laserbasierter generativer Fertigungsverfahren (Laser Additive Manufacturing – LAM) ist es möglich, potentiell komplexe Bauteilgeometrien variantenreich herzustellen. Damit kann Gewicht eingespart werden und Funktionen sind integrierbar. In Kombination mit Automatisierungs- und innovativer Lasertechnik in der Schweiß- und Schneidapplikation lässt sich dieser Prozess wirtschaftlich nutzen. Durch pulverbettbasierte Lasergenerierverfahren können metallische Bauteile schichtweise aufgebaut werden, jedoch ist die Auswahl der Werkstoffe limitiert. Im Forschungsprojekt StaVari (Additive Fertigungsprozesse für komplexe Produkte in variantenreicher und hochfunktionaler Stahlbauweisen) vereinen sich die neuesten Erkenntnisse in Material-, Laser-, Füge- und Automatisierungstechnik, um modernen Anforderungen der Automobilbranche in der Massenfertigung sowie bei der Medizintechnik in der Kleinserie gerecht zu werden.   Laser Additive Manufacturing LAM has the potential to generate complex geometries. Through this weight reduction, functional integration and multi-variant production is possible. In combination with automation and innovative laser technology applicated in welding and cutting, this process can be used economically. With powderbed based laser additive manufacturing metal parts can be built up layer by layer. However selection of available metals is limited. In the project StaVari latest findings in material-, laser-, joining and automation technology are joint by qualified partners to meet modern automotive demands in mass production and medicine technology for small batch series.

Hybrid Nanocomposites of Poly(Lactic Acid)/Thermoplastic Polyurethane with Nanosilica/Montmorillonite

2019 ◽  
Vol 947 ◽  
pp. 77-81
Author(s):  
Natsuda Palawat ◽  
Phasawat Chaiwutthinan ◽  
Sarintorn Limpanart ◽  
Amnouy Larpkasemsuk ◽  
Anyaporn Boonmahitthisud
Keyword(s):  
Thermal Stability ◽  
Tensile Strength ◽  
Impact Strength ◽  
Young’S Modulus ◽  
Young's Modulus ◽  
Thermoplastic Polyurethane ◽  
Hybrid Nanocomposites ◽  
Poly Lactic Acid ◽  
Elongation At Break ◽  
Thermal Stability Of

The aim of this study is to improve the physical properties of poly(lactic acid) (PLA) by incorporating thermoplastic polyurethane (TPU), organo-montmorillonite (OMMT) and/or nanosilica (nSiO2). PLA was first melt mixed with five loadings of TPU (10–50 wt%) on a twin-screw extruder, followed by injection molding. The addition of TPU was found to increase the impact strength, elongation at break and thermal stability of the blends, but decrease the tensile strength and Young’s modulus. Based on a better combination of the mechanical properties, the 70/30 (w/w) PLA/TPU blend was selected for preparing both single and hybrid nanocomposites with a fix total nanofiller content of 5 parts per hundred of resin (phr), and the OMMT/nSiO2 weight ratios were 5/0, 2/3, 3/2 and 0/5 (phr/phr). The Young’s modulus and thermal stability of the nanocomposites were all higher than those of the neat 70/30 PLA/TPU blend, but at the expense of reducing the tensile strength, elongation at break and impact strength. However, all the nanocomposites exhibited higher impact strength and Young’s modulus than the neat PLA. Among the four nanocomposites, a single-filler nanocomposite containing 5 phr nSiO2 exhibited the highest impact strength and thermal stability, indicating that there was no synergistic effect of the two nanofillers on the investigated physical properties. However, the hybrid nanocomposite containing 2/3 (phr/phr) OMMT/nSiO2 possessed a compromise in the tensile properties.

The microstructure and mechanical properties of deposited-IN625 by laser additive manufacturing

2017 ◽  
Vol 23 (6) ◽  
pp. 1119-1129 ◽  
Author(s):  
Lanlan Qin ◽  
Changjun Chen ◽  
Min Zhang ◽  
Kai Yan ◽  
Guangping Cheng ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Thermal Stability ◽  
Additive Manufacturing ◽  
Dendritic Morphology ◽  
Laves Phase ◽  
Micro Hardness ◽  
Laser Additive Manufacturing ◽  
Content Type ◽  
Annealing Temperatures

Purpose Laser additive manufacturing (LAM) technology based on powder bed has been used to manufacture complex geometrical components. In this study, IN625 superalloys were fabricated by high-power fiber laser without cracks, bounding errors or porosity. Meanwhile, the objectives of this paper are to systemically investigate the microstructures, micro-hardness and the precipitated Laves phase of deposited-IN625 under different annealing temperatures. Design/methodology/approach The effects of annealing temperatures on the microstructure, micro-hardness and the precipitated Laves phase were studied by optical microscope (OM), scanning electron microscopy (SEM), X-ray diffraction (XRD), energy dispersive spectrometer (EDS), selected area electron diffraction (SAED), backscattered electron (BSE) imaging in the SEM and transmission electron microscopy (TEM), respectively. The thermal stability of the dendritic morphology about IN625 superalloys was investigated through annealing at temperatures range from 1,000°C to 1,200°C. Findings It is found that the microstructure of deposited-IN625 was typical dendrite structure. Besides, some Laves phase precipitated in the interdendritic region results in the segregation of niobium and molybdenum. The thermal stability indicate that the morphology of dendrite can be stable up to 1,000°C. With the annealing temperatures increasing from 1,000 to 1,200°C, the Laves phase partially dissolves into the γ-Ni matrix, and the morphology of the remaining Laves phase is changing from irregular shape to rod-like or block-like shape. Research limitations/implications The heat treatment used on the IN625 superalloys is helpful for knowing the evolution of microstructures and precipitated phases thermal stability and mechanical properties. Practical implications Due to the different kinds of application conditions, the original microstructure of the IN625 superalloys fabricated by LAM may not be ideal. So exploring the influence of annealing treatment on IN625 superalloys can bring theory basis and guidance for actual production. Originality/value This study continues valuing the fabrication of IN625 by LAM. It shows the effect of annealing temperatures on the shape, size and distribution of Laves phase and the microstructures of deposited-IN625 superalloys.

scholarly journals Effect of Halloysite Nanotube on Mechanical Properties, Thermal Stability and Morphology of Polypropylene and Polypropylene/Short Kenaf Fibers Hybrid Biocomposites

Materials ◽  
2020 ◽  
Vol 13 (19) ◽  
pp. 4459 ◽  
Author(s):  
Piotr Franciszczak ◽  
Iman Taraghi ◽  
Sandra Paszkiewicz ◽  
Maksymilian Burzyński ◽  
Agnieszka Meljon ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Thermal Stability ◽  
Young’S Modulus ◽  
Young's Modulus ◽  
Flexural Modulus ◽  
Kenaf Fiber ◽  
Halloysite Nanotube ◽  
Low Concentrations ◽  
Izod Impact ◽  
Kenaf Fibers

In this article, the effect of the addition of halloysite nanotube (HNT) on the mechanical and thermal stability of polypropylene (PP) and PP/kenaf fiber biocomposites has been investigated. Different volume contents of HNTs ranging from 1 to 10 vol.% were melt mixed with PP and PP/kenaf fibers. The volume content of kenaf fibers was kept constant at 30%. The morphology of HNTs within the PP matrix has been studied via scanning electron microscopy (SEM). The morphological results revealed that HNT was uniformly dispersed in the PP matrix already at a low concentration of 1 and 2 vol.%. The mechanical properties of the manufactured nanocomposites and hybrid biocomposites such as Young’s modulus, tensile strength, elongation at break, flexural modulus, flexural strength, and notched Izod strength have been measured. The results show that Young’s modulus and strengths have been improved along with the addition of low content of HNTs. Moreover, the gain of notched Izod impact strength obtained by the addition of short kenaf fibers was maintained in hybrids with low concentrations of HNTs. Finally, the thermogravimetric analysis shows that at 10% and 50% weight loss, the thermal degradation rate of the PP and PP/kenaf biocomposites decreased by the addition of HNTs.

scholarly journals Control of crystallographic orientation by metal additive manufacturing process of β-type Ti alloys based on the bone tissue anisotropy

2020 ◽  
Vol 321 ◽  
pp. 05002
Author(s):  
Takayoshi Nakano ◽  
Takuya Ishimoto ◽  
Aira Matsugaki ◽  
Koji Hagihara ◽  
Yuichiro Koizumi ◽  
...  
Keyword(s):  
Additive Manufacturing ◽  
Young’S Modulus ◽  
Bone Tissue ◽  
Young's Modulus ◽  
Stress Shielding ◽  
Scanning Strategy ◽  
Ti Alloys ◽  
Specific Direction ◽  
Tissue Anisotropy ◽  
Metal Additive

Variation in the scanning strategy for β-type Ti alloys during additive manufacturing (AM) enables the fabrication of a singlecrystal-like microstructure possessing a crystallographic texture, in which the low-Young’s modulus-<100> direction is aligned along a specific direction. Thus, metal biomaterial with low elasticity, comparable to the bone Young’s modulus, can be developed by AM, which will contribute to suppress the stress shielding of bone and prevent degradation of bone tissue anisotropy.

Ultrafine Wollastonite Reinforced Polypropylene/Ethylene Propylene Diene Rubber Thermoplastic Elastomers

2012 ◽  
Vol 488-489 ◽  
pp. 945-949 ◽  
Author(s):  
Saowaroj Chuayjuljit ◽  
Thatisorn Karnjanamayul
Keyword(s):  
Thermal Stability ◽  
Tensile Strength ◽  
Young’S Modulus ◽  
Young's Modulus ◽  
Thermoplastic Elastomers ◽  
Dependent Manner ◽  
Elongation At Break ◽  
Ethylene Propylene ◽  
Ethylene Propylene Diene Rubber ◽  
Diene Rubber

In this study, tensile properties, thermal stability and morphology of polypropylene/ethylene propylene diene rubber/wollastonite (PP/EPDM/wollastonite) thermoplastic elastomer composites were tested and evaluated as a function of their compositions in comparison with PP/EPDM blends and native PP. PP was melt mixed with two loadings of EPDM (20 and 30% (w/w)) and for the composites each of these with three loadings of wollastonite (10, 20 and 30 parts by weight per hundred of the PP/EPDM resin) on a twin screw extruder and then injection molded. Both PP/EPDM blends provided a higher elongation at break but a lower tensile strength and Young’s modulus as compared with those of the neat PP. However, the addition of wollastonite microparticles (particle size of 1200 mesh) into the blends increased the Young’s modulus in a dose-dependent manner with increasing wollastonite loadings, whilst the tensile strength and elongation at break were decreased. Moreover, the thermal stability was improved by the presence of either EPDM or wollastonite in the PP matrix.

scholarly journals Ti–Zr–Si–Nb Nanocrystalline Alloys and Metallic Glasses: Assessment on the Structure, Thermal Stability, Corrosion and Mechanical Properties

Materials ◽  
2019 ◽  
Vol 12 (9) ◽  
pp. 1551
Author(s):  
Camelia Gabor ◽  
Daniel Cristea ◽  
Ioana-Laura Velicu ◽  
Tibor Bedo ◽  
Andrea Gatto ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Thermal Stability ◽  
Titanium Alloys ◽  
Young’S Modulus ◽  
Melt Spinning ◽  
Young's Modulus ◽  
Structural Features ◽  
Input Power ◽  
X Ray ◽  
Β Phase

The development of novel Ti-based amorphous or β-phase nanostructured metallic materials could have significant benefits for implant applications, due to improved corrosion and mechanical characteristics (lower Young’s modulus, better wear performance, improved fracture toughness) in comparison to the standardized α+β titanium alloys. Moreover, the devitrification phenomenon, occurring during heating, could contribute to lower input power during additive manufacturing technologies. Ti-based alloy ribbons were obtained by melt-spinning, considering the ultra-fast cooling rates this method can provide. The titanium alloys contain in various proportions Zr, Nb, and Si (Ti60Zr10Si15Nb15, Ti64Zr10Si15Nb11, Ti56Zr10Si15Nb19) in various proportions. These elements were chosen due to their reported biological safety, as in the case of Zr and Nb, and the metallic glass-forming ability and biocompatibility of Si. The morphology and chemical composition were analyzed by scanning electron microscopy and energy-dispersive X-ray spectroscopy, while the structural features (crystallinity, phase attribution after devitrification (after heat treatment)) were assessed by X-ray diffraction. Some of the mechanical properties (hardness, Young’s modulus) were assessed by instrumented indentation. The thermal stability and crystallization temperatures were measured by differential thermal analysis. High-intensity exothermal peaks were observed during heating of melt-spun ribbons. The corrosion behavior was assessed by electrocorrosion tests. The results show the potential of these alloys to be used as materials for biomedical applications.

High Strength Low Dielectric Constant Aromatic Thermosets

2005 ◽  
Vol 863 ◽  
Author(s):  
Yongqing Huang ◽  
James Economy
Keyword(s):  
Thermal Stability ◽  
Dielectric Constant ◽  
Young’S Modulus ◽  
Breakdown Strength ◽  
Young's Modulus ◽  
Chemical Vapor ◽  
High Strength ◽  
Low Dielectric Constant ◽  
Crosstalk Noise ◽  
Low Dielectric

AbstractContinuing miniaturization of microelectronic devices requires development of low dielectric constant materials to lower the RC delay, power dissipation and crosstalk noise. Although spin-on polymer dielectrics usually have better potential for extendibility to lower dielectric constant (k) values compared to chemical-vapor-deposited dielectrics, their low mechanical properties prevent them from being successfully integrated with copper metal lines.Recent evaluation of a new thermosetting oligomer shows high thermal stability, low moisture pick-up and low dielectric constant. Techniques to optimize the solubility and spin coating characteristics of the oligomer have been developed. The thermally cured polymer displayed a thermal stability up to 480°C in nitrogen and 400°C in air. The cured polymer displayed a dielectric constant of 2.7 at 1 MHz and a breakdown strength larger than 230 V/μm. Nanoindentation testing showed that it had an extraordinarily high Young's modulus of 16.8 GPa and a hardness of 3.5 GPa. By use of porogens, a dielectric constant as low as 1.85 was obtained while still maintaining an acceptable high Young's modulus of 7.7 GPa and hardness of 2.0 GPa. Nanoscratch testing indicated that this material had good adhesion to the Si substrate, and Ta which is a diffusion barrier for copper. These results appear unique compared to all commercially available low-k candidates.

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