Experimental investigation on fabrication and thermal-stamping of woven jute/polylactic acid biocomposites

2018 ◽  
Vol 53 (7) ◽  
pp. 851-861 ◽  
Author(s):  
Siqi Du ◽  
Xiongqi Peng ◽  
Hailin Gu

Jute woven fabrics in as-received and alkali-treated conditions were respectively combined with polylactic acid resin to fabricate completely biodegradable composites by compression molding in one step. Scanning electron microscopy and differential scanning calorimetry and tensile tests were conducted to estimate the surface morphology, thermal, and mechanical properties of jute fabrics and the composites manufactured. The formability of the composites was evaluated by a thermal-stamping experiment. The results demonstrate that alkali treatment removes the surface impurities of fabrics and refine the fiber structures, lifting the thermal property of composites. As for the mechanical properties, the strength of the fabrics and composites declines while the modulus increases after alkali treatment of fabrics. Although some defects occur, the thermal-stamping experiments confirm the possibility of shaping jute/polylactic acid composite into complicated geometries. And the formability of the composites is influenced by many factors including sample sizes, the holding time of temperature, layup sequence, and so on while the number of layer makes no obvious difference to it.

Materials ◽  
2020 ◽  
Vol 13 (5) ◽  
pp. 1242
Author(s):  
Olga Mysiukiewicz ◽  
Paulina Kosmela ◽  
Mateusz Barczewski ◽  
Aleksander Hejna

Investigations related to polymer/metal composites are often limited to the analysis of the electrical and thermal conductivity of the materials. The presented study aims to analyze the impact of aluminum (Al) filler content (from 1 to 20 wt%) on the rarely investigated properties of composites based on the high-density polyethylene (HDPE) matrix. The crystalline structure, rheological (melt flow index and oscillatory rheometry), thermal (differential scanning calorimetry), as well as static (tensile tests, hardness, rebound resilience) and dynamic (dynamical mechanical analysis) mechanical properties of composites were investigated. The incorporation of 1 and 2 wt% of aluminum filler resulted in small enhancements of mechanical properties, while loadings of 5 and 10 wt% provided materials with a similar performance to neat HDPE. Such results were supported by the lack of disturbances in the rheological behavior of composites. The presented results indicate that a significant content of aluminum filler may be introduced into the HDPE matrix without additional pre-treatment and does not cause the deterioration of composites’ performance, which should be considered beneficial when engineering PE/metal composites.


2015 ◽  
Vol 35 (4) ◽  
pp. 377-390 ◽  
Author(s):  
Andrzej Ambroziak

Abstract This article describes the laboratory tests necessary to identify the mechanical properties of the polyvinylidene fluoride (PVDF)-coated fabrics named Precontraint 1202S and Precontraint 1302S. First, a short survey of the literature concerning the description of coated woven fabrics is presented. Second, the material parameters for PVDF-coated fabrics are specified on the basis of biaxial tensile tests. A comparison of the 1:1 biaxial and the uniaxial tensile tests results is also given. Additionally, biaxial cyclic tests were performed to observe the change of immediate mechanical properties under cyclic load. The article is aimed as an introduction to a comprehensive investigation of the mechanical properties of coated fabrics.


2021 ◽  
Vol 36 (2) ◽  
pp. 137-143
Author(s):  
S. A. Awad

Abstract This paper aims to describe the thermal, mechanical, and surface properties of a PVA/HPP blend whereby the film was prepared using a solution casting method. The improvements in thermal and mechanical properties of HPP-based PVA composites were investigated. The characterization of pure PVA and PVA composite films included tensile tests, thermogravimetric analysis (TGA), and differential scanning calorimetry (DSC). The results of TGA and DSC indicated that the addition of HPP increased the thermal decomposition temperature of the composites. Mechanical properties are significantly improved in PVA/HPP composites. The thermal stability of the PVA composite increased with the increase of HPP filler content. The tensile strength increased from 15.74 ± 0.72 MPa to 27.54 ± 0.45 MPa and the Young’s modulus increased from 282.51 ± 20.56 MPa to 988.69 ± 42.64 MPa for the 12 wt% HPP doped sample. Dynamic mechanical analysis (DMA) revealed that at elevated temperatures, enhanced mechanical properties because of the presence of HPP was even more noticeable. Morphological observations displayed no signs of agglomeration of HPP fillers even in composites with high HPP loading.


2016 ◽  
Vol 30 (2) ◽  
pp. 174-195 ◽  
Author(s):  
Rungsima Chollakup ◽  
Haroutioun Askanian ◽  
Florence Delor-Jestin

In the furniture, automotive and contruction industries, there is increased demand for cost-effective and lightweight biocomposites. The objective of this work was to develop new natural fibre-based composites with specific properties. Palm and pineapple leaf fibres were chosen in association with polypropylene (PP). The first step was to investigate the effect of these natural fibres as reinforcement for PP. The evolution of chemical structure and crystallinity was proposed with infrared spectroscopy measurements and differential scanning calorimetry thermograms, respectively. The assessments of mechanical properties with tensile tests and melt viscoelastic behaviour were also investigated. The study enabled to distinguish the influence of fibre content. The second step in our work was to assess the composite durability after ultraviolet exposure or thermal ageing. The oxidation level was calculated. The long-term evolution of thermal and mechanical properties was also proposed. As a result, the PP/pineapple leaf composite revealed a promising biocomposite.


2002 ◽  
Vol 753 ◽  
Author(s):  
Masahiro Tsuji ◽  
Hideki Hosoda ◽  
Kenji Wakashima ◽  
Yoko Yamabe-Mitarai

ABSTRACTEffects of ruthenium (Ru) substitution on constituent phases, phase transformation temperatures and mechanical properties were investigated for Ti-Ni shape memory alloys. Ti50Ni50-XRuX alloys with Ru contents (X) from 0mol% (binary TiNi) to 50mol% (binary TiRu) were systematically prepared by Ar arc-melting followed by hot-forging at temperatures from 1173K to 1673K depending on chemical composition. Phase stability was assessed by DSC (differential scanning calorimetry), XRD (X-ray diffractometry) and TEM (transmission electron microscopy). Mechanical properties were investigated using hardness and tensile tests at room temperature. With increasing Ru content, it was found that the lattice parameter of B2 phase increases, the martensitic transformation temperature slightly decreases, and the melting temperature increases monotonously. Besides, R-phase appears for Ti-Ni alloys containing 3mol% and 20mol%Ru but no diffusionless phase transformation is seen in Ti-Ni alloy containing 5mol%Ru. Vickers hardness shows the maximum at an intermediate composition (HV1030 at 30mol%Ru); this suggests that large solid solution hardening is caused by Ru substitution for the Ni-sites in TiNi.


2016 ◽  
Vol 682 ◽  
pp. 245-251 ◽  
Author(s):  
Grzegorz Włoch ◽  
Tomasz Skrzekut ◽  
Jakub Sobota ◽  
Antoni Woźnicki ◽  
Justyna Cisoń

Mixed and preliminarily consolidated powders of aluminium and nickel (90 mass % Al and 10 mass % Ni) were hot extruded. As results the rod, 8 mm in diameter, was obtained. As-extruded material was subjected to the microstructural investigations using scanning electron microscopy (SEM/EDS) and X-ray analysis (XRD). The differential scanning calorimetry (DSC) and thermo-mechanical analysis (TMA) were also performed. The mechanical properties of as extruded material were determined by the tensile test and Vickers hardness measurements. In order to evaluate the thermal stability of PM alloy, samples were annealed at the temperature of 475 and 550 °C. After annealing Vickers hardness measurements and tensile tests were carried out. The plastic consolidation of powders during extrusion was found to be very effective, because no pores or voids were observed in the examined material. The detailed microstructural investigations and XRD analyses did not reveal the presence of the intermetallic phases in the as-extruded material. During annealing, the Al3Ni intermetallic compound was formed as the result of chemical reaction between the alloy components. The hardness of the alloy after annealing at the temperature of 475°C was found to be comparable to the hardness in as-extruded state. Annealing of the material at the temperature of 550°C results in hardness decreasing by about 50%, as the consequence of porosity formation and Al3Ni cracking.


2000 ◽  
Vol 9 (3) ◽  
pp. 096369350000900 ◽  
Author(s):  
J.L. Billoet ◽  
A. Cherouat

The present study concerns the modelling of the behaviour of pre-impregnated woven fabric during the forming process. The mechanical approach is based on a mesostructural model. It allows us to take into account the mechanical properties of fibres and resin and the various dominating mode of deformation of woven fabrics during the forming process. Shear and tensile tests of composite fabric specimens are proposed and compared with the experimental results in order to demonstrate the efficiency of our approach. Different numerical simulations and experiments of shaping process have been carried out in order to validate the proposed computational formulation. The various forming parameters examined have included the initial shape of fabric, fibre orientations and viscosity of resin.


2018 ◽  
Vol 89 (9) ◽  
pp. 1770-1781 ◽  
Author(s):  
Huaizhong Xu ◽  
Benedict Bauer ◽  
Masaki Yamamoto ◽  
Hideki Yamane

A facile route was proposed to fabricate core–sheath microfibers, and the relationships among processing parameters, crystalline structures and the mechanical properties were investigated. The compression molded poly(3-hydroxybutyrate-co-3-hydroxyhexanoate) (PHBH)/poly(L-lactic acid) (PLLA) strip enhanced the spinnability of PHBH and the mechanical properties of PLLA as well. The core–sheath ratio of the fibers was determined by the prefab strip, while the PLLA sheath component did not completely cover the PHBH core component due to the weak interfacial tension between the melts of PHBH and PLLA. A rotational target was applied to collect aligned fibers, which were further drawn in a water bath. The tensile strength and the modulus of as-spun and drawn fibers increased with increasing the take-up velocities. When the take-up velocity was above 500 m/min, the jet became unstable and started to break up at the tip of the Taylor cone, decreasing the mechanical properties of the fibers. The drawing process facilitated the crystallization of PLLA and PHBH, and the tensile strength and the modulus increased linearly with the increasing the draw ratio. The crystal information displayed from wide-angle X-ray diffraction patterns and differential scanning calorimetry heating curves supported the results of the tensile tests.


2016 ◽  
Vol 47 (5) ◽  
pp. 640-655 ◽  
Author(s):  
Ammayappan Lakshmanan ◽  
Rakesh Kumar Ghosh ◽  
Swati Dasgupta ◽  
Sujay Chakraborty ◽  
Prasanta Kumar Ganguly

Jute fiber has poor compatibility with hydrophobic thermosetting polymeric resin for the development of a biocomposite. In this present study, plain weave jute fabric was treated with 1% sodium hydroxide (owf) in three different time (30, 60 and 90 minutes), temperature (30, 40 and 50℃) and material-to-liquor ratio (1:5, 1:10 and 1:15) as per orthogonal array and the treated jute fabrics were used for the preparation of the biocomposite sheet by hand laying-cum-compression moulding method. Developed biocomposite sheets were evaluated for their mechanical properties as per ASTM standards and results were analyzed by Taguchi model to optimize the sodium hydroxide treatment condition. Results inferred that jute fabric reinforcement treated with 1% sodium hydroxide at 50℃ for 60 minutes in 1:10 material-to-liquor ratio could be the optimum condition to develop the biocomposite sheet with higher mechanical properties than other conditions.


2019 ◽  
Vol 895 ◽  
pp. 15-20
Author(s):  
Raghavendra Subramanya ◽  
S.S. Prabhakara

Natural fibers, in particularly lignocellulosic fibers are attracting material scientists now days, due to their comparative advantages over synthetic fibers. Biodegradable composites reinforced with short banana fibre after alkali treatment along with cassava starch matrix were prepared using the hot compression method. The mechanical properties like tensile strength and impact strength were investigated. Mechanical properties of the composites made from alkali treated fibres were superior to the untreated fibres. SEM observations on the fracture surface of composites showed that the surface modification of the fibre occurred and improved fibre–matrix adhesion. Keywords: Surface modification; banana fiber; Biodegradable composites; Mechanical properties; Matrix.


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