scholarly journals ANTHOCYANIN FROM BAUHINIA PURPUREA FLOWER: EXTRACTION, COLOR CHARACTERISTICS AND STABILITY

2021 ◽  
Vol 17 (1) ◽  
pp. 1
Author(s):  
Abdullah Muzi Marpaung ◽  
Darinda Pusha Djani ◽  
Della Rahmawati
Keyword(s):  
Heat Treatment ◽  
Extraction Temperature ◽  
Color Intensity ◽  
High Activation ◽  
Browning Index ◽  
Red Color ◽  
Food Applications ◽  
Bauhinia Purpurea ◽  
The Stability

The determination of the best temperature (45, 60, and 75°C ) and time (30, 75, and 120 minutes) to extract the anthocyanins from Bauhinia purpurea (BP) flower powder was studied.  The anthocyanin was extracted using 40 ml of 1 N HCl/g powder with continuous shaking. Based on the total monomeric anthocyanin (TMA), the best extraction temperature and time were 45°C and 30 minutes, respectively. The BP extract exhibited relatively high red color intensity (CI) at pH ≤ 3 and almost colorless at pH 4 – 6. Meanwhile, at pH ≥ 7,  the color was unsuitable for food applications due to the high browning index. Hence, the best performance of BP extract was at pH 3. At this pH, the stability of BP extract was relatively high with the t 1/2 of CI and TMA at 30°C was 70.30 and 72.89 days, respectively. Nevertheless, the extract was sensitive to heat as represented by the high activation energy (Ea). The Ea of CI and TMA was 64.50 kJ.mol-1 and 90.19 kJ.mol-1, respectively. The study showed the potential of BP extract as a red food colorant at pH 3 processed by relatively mild heat treatment. 

Effect of Heating Treatment of Fresh Rice Bran on Stabilization

2012 ◽  
Vol 602-604 ◽  
pp. 1200-1205
Author(s):  
Zhu Gong ◽  
Guo Ping Yu ◽  
Chao Ran Dou ◽  
Man Xu Xu
Keyword(s):  
Heat Treatment ◽  
Rice Bran ◽  
Peroxidase Activity ◽  
Direct Determination ◽  
Material Resources ◽  
Total Antioxidant ◽  
Heating Treatment ◽  
The Stability ◽  
First Time

In the research of rice bran stabilization, most of the literature only study the lipase which is explained by the changes in free fatty acids in the storage experiment or peroxidase activity. It leads results not comprehensive, extends the experiment time, increases the experimental difficulty and wastes of manpower and material resources. For the first time, the effect of heat treatment on fresh rice bran stability is examined in terms of direct determination of water content, lipase activity, peroxidase activity and total antioxidant capacity. The optimal condition is that 120 degrees for 22 min. The results show that the heat treatment can reduce the enzyme activity of rice bran to improve the stability of rice bran.

Determining the Norton’s Equivalent Model of Distribution System with Distributed Generation (DG) for Stability Analysis

2019 ◽  
Vol 12 (2) ◽  
pp. 190-198
Author(s):  
Sunny Katyara ◽  
Lukasz Staszewski ◽  
Faheem Akhtar Chachar
Keyword(s):  
Distributed Generation ◽  
Normal Condition ◽  
Distribution System ◽  
Distribution Networks ◽  
Equivalent Model ◽  
Stability Factor ◽  
Matlab Simulation ◽  
The Stability ◽  
Stability Issues

Background: Since the distribution networks are passive until Distributed Generation (DG) is not being installed into them, the stability issues occur in the distribution system after the integration of DG. Methods: In order to assure the simplicity during the calculations, many approximations have been proposed for finding the system’s parameters i.e. Voltage, active and reactive powers and load angle, more efficiently and accurately. This research presents an algorithm for finding the Norton’s equivalent model of distribution system with DG, considering from receiving end. Norton’s model of distribution system can be determined either from its complete configuration or through an algorithm using system’s voltage and current profiles. The algorithm involves the determination of derivative of apparent power against the current (dS/dIL) of the system. Results: This work also verifies the accuracy of proposed algorithm according to the relative variations in the phase angle of system’s impedance. This research also considers the varying states of distribution system due to switching in and out of DG and therefore Norton’s model needs to be updated accordingly. Conclusion: The efficacy of the proposed algorithm is verified through MATLAB simulation results under two scenarios, (i) normal condition and (ii) faulty condition. During normal condition, the stability factor near to 1 and change in dS/dIL was near to 0 while during fault condition, the stability factor was higher than 1 and the value of dS/dIL was away from 0.

Synthesis and solvatochromic studies of 2- amino-3-phenolazo1-(4-sulfophenyl)-3-methyi-5-pyrozolone and use it for the determination of trace amount of Nickel (II) in blood samples

2016 ◽  
Vol 5 (10) ◽  
pp. 4920
Author(s):  
Amar M. Ali ◽  
Hussain. J. Mohammed*
Keyword(s):  
Stability Constant ◽  
Trace Amount ◽  
Benzenesulfonic Acid ◽  
Determination Method ◽  
Blood Samples ◽  
Determination Of Nickel ◽  
Normal Human ◽  
The Stability ◽  
Normal Human Blood

A new, simple, sensitive and rapid spectrophotometric method is proposed for the determination of trace amount of Nickel (II). The method is based on the formation of a 1:2 complex with 4-(4-((2-hydroxy-6-nitrophenyl) diazenyl) -3-methyl-5-oxo-2, 5-dihydro-1H-pyrazol-1-yl) benzenesulfonic acid (2-ANASP) as a new reagent is developed. The complex has a maximum absorption at 516 nm and εmax of 1. 84 X 105 L. mol-1. cm-1. A linear correlation (0. 25 – 4. 0μg. ml-1) was found between absorbance at λmax and concentration. The accuracy and reproducibility of the determination method for various known amounts of Nickel (II) were tested. The results obtained are both precise (RSD was 1. 2 %) and accurate (relative error was 0. 787 %). The effect of diverse ions on the determination of Nickel (II) to investigate the selectivity of the method were also studied. The stability constant of the product was 0. 399 X 106 L. mol-1. The proposed method was successfully applied to the analysis of diabetes blood and normal human blood. 

Enzymatic colorimetry of lecithin and sphingomyelin in aqueous solution.

1983 ◽  
Vol 29 (8) ◽  
pp. 1513-1517 ◽  
Author(s):  
M W McGowan ◽  
J D Artiss ◽  
B Zak
Keyword(s):  
Aqueous Solution ◽  
Hydrogen Peroxide ◽  
Amniotic Fluid ◽  
Enzymatic Reaction ◽  
Detergent Solution ◽  
Enzymatic Determination ◽  
Red Color ◽  
Hydrolysis Of ◽  
Zwitterionic Detergent

Abstract A procedure for the enzymatic determination of lecithin and sphingomyelin in aqueous solution is described. The phospholipids are first dissolved in chloroform:methanol (2:1 by vol), the solvent is evaporated, and the residue is redissolved in an aqueous zwitterionic detergent solution. The enzymatic reaction sequences of both assays involve hydrolysis of the phospholipids to produce choline, which is then oxidized to betaine, thus generating hydrogen peroxide. The hydrogen peroxide is subsequently utilized in the enzymatic coupling of 4-aminoantipyrine and sodium 2-hydroxy-3,5-dichlorobenzenesulfonate, an intensely red color being formed. The presence of a non-reacting phospholipid enhances the hydrolysis of the reacting phospholipid. Thus we added lecithin to the sphingomyelin standards and sphingomyelin to the lecithin standards. This precise procedure may be applicable to determination of lecithin and sphingomyelin in amniotic fluid.

scholarly journals Determination of Objective Weights Using a New Method Based on the Removal Effects of Criteria (MEREC)

Symmetry ◽  
2021 ◽  
Vol 13 (4) ◽  
pp. 525 ◽  
Author(s):  
Mehdi Keshavarz-Ghorabaee ◽  
Maghsoud Amiri ◽  
Edmundas Kazimieras Zavadskas ◽  
Zenonas Turskis ◽  
Jurgita Antucheviciene
Keyword(s):  
Essential Elements ◽  
New Method ◽  
Multi Criteria Decision Making ◽  
Analysis Of Means ◽  
Simulation Based ◽  
Criteria Weights ◽  
The Stability ◽  
Computational Analyses ◽  
Weighting Methods

The weights of criteria in multi-criteria decision-making (MCDM) problems are essential elements that can significantly affect the results. Accordingly, researchers developed and presented several methods to determine criteria weights. Weighting methods could be objective, subjective, and integrated. This study introduces a new method, called MEREC (MEthod based on the Removal Effects of Criteria), to determine criteria’ objective weights. This method uses a novel idea for weighting criteria. After systematically introducing the method, we present some computational analyses to confirm the efficiency of the MEREC. Firstly, an illustrative example demonstrates the procedure of the MEREC for calculation of the weights of criteria. Secondly, a comparative analysis is presented through an example for validation of the introduced method’s results. Additionally, we perform a simulation-based analysis to verify the reliability of MEREC and the stability of its results. The data of the MCDM problems generated for making this analysis follow a prevalent symmetric distribution (normal distribution). We compare the results of the MEREC with some other objective weighting methods in this analysis, and the analysis of means (ANOM) for variances shows the stability of its results. The conducted analyses demonstrate that the MEREC is efficient to determine objective weights of criteria.

scholarly journals Determination of Transverse Shear Stiffness of Sandwich Panels with a Corrugated Core by Numerical Homogenization

Materials ◽  
2021 ◽  
Vol 14 (8) ◽  
pp. 1976
Author(s):  
Tomasz Garbowski ◽  
Tomasz Gajewski
Keyword(s):  
Transverse Shear ◽  
Shear Stiffness ◽  
The Finite Element Method ◽  
Homogenization Procedure ◽  
Plate Structures ◽  
Corrugated Board ◽  
Energy Equivalence ◽  
The Stability ◽  
Global Stiffness Matrix

Knowing the material properties of individual layers of the corrugated plate structures and the geometry of its cross-section, the effective material parameters of the equivalent plate can be calculated. This can be problematic, especially if the transverse shear stiffness is also necessary for the correct description of the equivalent plate performance. In this work, the method proposed by Biancolini is extended to include the possibility of determining, apart from the tensile and flexural stiffnesses, also the transverse shear stiffness of the homogenized corrugated board. The method is based on the strain energy equivalence between the full numerical 3D model of the corrugated board and its Reissner-Mindlin flat plate representation. Shell finite elements were used in this study to accurately reflect the geometry of the corrugated board. In the method presented here, the finite element method is only used to compose the initial global stiffness matrix, which is then condensed and directly used in the homogenization procedure. The stability of the proposed method was tested for different variants of the selected representative volume elements. The obtained results are consistent with other technique already presented in the literature.

scholarly journals Charge Transfer Complexes of Ketotifen with 2,3-Dichloro-5,6-dicyano-p-benzoquinone and 7,7,8,8-Tetracyanoquodimethane: Spectroscopic Characterization Studies

Molecules ◽  
2021 ◽  
Vol 26 (7) ◽  
pp. 2039
Author(s):  
Gamal A. E. Mostafa ◽  
Ahmed Bakheit ◽  
Najla AlMasoud ◽  
Haitham AlRabiah
Keyword(s):  
Charge Transfer ◽  
Spectroscopic Characterization ◽  
Molar Ratio ◽  
Charge Transfer Complexes ◽  
Physical Parameters ◽  
Spectrophotometric Methods ◽  
Theoretical Approaches ◽  
The Stability ◽  
Ct Complexes

The reactions of ketotifen fumarate (KT) with 2,3-dichloro-5,6-dicyano-p-benzoquinone (DDQ) and 7,7,8,8-tetracyanoquinodimethane (TCNQ) as π acceptors to form charge transfer (CT) complexes were evaluated in this study. Experimental and theoretical approaches, including density function theory (DFT), were used to obtain the comprehensive, reliable, and accurate structure elucidation of the developed CT complexes. The CT complexes (KT-DDQ and KT-TCNQ) were monitored at 485 and 843 nm, respectively, and the calibration curve ranged from 10 to 100 ppm for KT-DDQ and 2.5 to 40 ppm for KT-TCNQ. The spectrophotometric methods were validated for the determination of KT, and the stability of the CT complexes was assessed by studying the corresponding spectroscopic physical parameters. The molar ratio of KT:DDQ and KT:TCNQ was estimated at 1:1 using Job’s method, which was compatible with the results obtained using the Benesi–Hildebrand equation. Using these complexes, the quantitative determination of KT in its dosage form was successful.

scholarly journals A thermo-mechanical machining method for improving the accuracy and stability of the geometric shape of long low-rigidity shafts

2021 ◽  
Author(s):  
Antoni Świć ◽  
Arkadiusz Gola ◽  
Łukasz Sobaszek ◽  
Natalia Šmidová
Keyword(s):  
Heat Treatment ◽  
Cross Section ◽  
Mechanical Treatment ◽  
Geometric Shape ◽  
Different Dimensions ◽  
Thermo Mechanical Treatment ◽  
Mechanical Machining ◽  
Simultaneous Heat ◽  
Accuracy And Stability

AbstractThe article presents a new thermo-mechanical machining method for the manufacture of long low-rigidity shafts which combines straightening and heat treatment operations. A fixture for thermo-mechanical treatment of long low-rigidity shafts was designed and used in tests which involved axial straightening of shafts combined with a quenching operation (performed to increase the corrosion resistance of the steel used as stock material). The study showed that an analysis of the initial deflections of semi-finished shafts of different dimensions and determination of the maximum corrective deflection in the device could be used as a basis for performing axial straightening of shaft workpieces with simultaneous heat treatment and correction of the initial deflection of the workpiece. The deflection is corrected by stretching the fibers of the stock material, at any cross-section of the shaft, up to the yield point and generating residual stresses symmetrical to the axis of the workpiece. These processes allow to increase the accuracy and stability of the geometric shape of the shaft.

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