scholarly journals PENENTUAN MUTU PEKTIN DARI LIMBAH KULIT PISANG DENGAN VARIASI VOLUME PELARUT ASAM SITRAT

Jurnal Kimia ◽  
2020 ◽  
pp. 169
Author(s):  
V. A. Devianti ◽  
L. Sa'diyah ◽  
A. R. Amalia

The need for pectin in Indonesia is inscreasing every year. Indonesia relies on pectin import to fulfill domestic pectin needs. So it is necessary to search for sources of raw materials that contain pectin, one of which is banana peel waste. Pectin in banana peels can be extracted using acid solvents. This study aims to determine the effect of the ratio of banana peel powder and solvents (1:40, 1:50, and 1:60) to the yield and quality of pectin extracted. The acid solvent used was 5% citric acid, and the extraction was conditioned at 90 °C for 120 minutes. Pectin which has been extracted from banana peels is in powdered form, brownish, and odorless. The results showed that the optimum solvent/solid ratio was 1:50 with a quantity of yield, equivalent weight, methoxyl content, galacturonic acid content, and esterification degree were 10,68%, 958 mg, 3,54%, 196% and 14,84% respecively. FTIR analysis indicated that pectin from banana peels extract had characteristic near to comercial pectin. Keyword: pectin extraction, ratio peel powder and solvents, citric acid volume Kebutuhan pektin di Indonesia cenderung meningkat di setiap tahun dan lebih mengandalkan pektin impor untuk memenuhi kebutuhan pektin dalam negeri. Oleh karena itu perlu dilakukan pencarian sumber bahan baku yang memiliki kandungan pektin, diantaranya adalah kulit pisang. Pektin dalam kulit pisang dapat diekstrak menggunakan pelarut asam. Penelitian ini bertujuan untuk mengetahui pengaruh volume asam yang ditambahkan pada serbuk kulit pisang raja nangka dengan rasio 1:40, 1:50, dan 1:60. Pelarut asam yang digunakan adalah asam sitrat 7% dengan suhu estraksi 90 °C dan lama waktu ekstraksi 120 menit. Pektin yang telah diekstrak dari kulit buah pisang ini berbentuk serbuk, berwarna kecoklatan, dan tidak berbau. Hasil penelitian menunjukkan bahwa rasio bahan/pelarut adalah 1:50 dengan hasil rendemen, berat ekivalen, kadar metoksil, kadar galakturonat, dan derajat esterifikasi berturut-turut adalah 10,68%, 958 mg, 3,54%, 196% dan 14,84%. Analisis dengan FTIR menunjukkan bahwa bilangan gelombang yang muncul pada pektin dari kulit pisang ini memiliki karakteristik yang sama dengan pektin komersial. Kata kunci: ekstraksi pektin, volume asam sitrat, rasio bahan dan pelarut

2020 ◽  
Vol 5 (86) ◽  
pp. 3-10
Author(s):  
V.G. Chernikov ◽  
◽  
R.A. Rostovtsev ◽  
N.A. Kudryavtsev ◽  
I.V. Uschapovsky ◽  
...  

The formation of fiber flax yield and quality parameters depends on many soil-climatic, breedinggenetic, as well as anthropogenic factors. The quality of flax fiber is a combination of a number of features and properties that depend on the varietal characteristics of plants, the conditions of their cultivation, technologies for harvesting and straw retting, as well as on the processing modes of raw materials. During plant vegetation (90-130 days) many factors such as soil conditions (pH 4.8-5.5, humus 1.8-2.5%, P2O5 and K2O – 150-200 and 100-200 mg/kg, respectively) and the area of plant nutrition (15-30 million seeds/ha), temperature regime (the sum of active temperatures 1000-1800ºC), water supplying (400-430 units of water mass to create 1 unit of dry matter) and insolation (the arrival of FAR during the growing season 20-25 kcal / cm²), contamination of weeds (more than 60 annual and perennial species) and pests (more than 200 types of fungal, bacterial and viral diseases), features of phytosanitary measures (more than 50 chemicals) and agrotechnologic manners (Federal Register of technologies for the production of crop products) have a great influence on the quality of flax raw materials and can be a limit factor. Environmentally hazardous pollution of air, water and soil - the main components for the production of fiber flax – strongly affects the yield and quality of flax products. The development of waste-free environmentally friendly technologies for the cultivation, harvesting and processing of flax is an urgent task of scientific support of the industry. The main environmental factors affecting the yield and quality of fiber flax are discussed in the article.


Author(s):  
Hatun Barut ◽  
Sait Aykanat ◽  
Ali Alpaslan Ezici ◽  
Uğur Sevilmiş

This research was conducted during 2016-2017 awheat growing season to investigate the effects of different rates of seed coating of an organic acid mixture (citric acid, glutamate, and proline) on yield and quality of wheat. The field experiments were established in Dogankent and Haciali locations of Eastern Mediterranean Agricultural Research Institute in Turkey. Study was carried out with randomised complete block design with 4 replications and Ceyhan-99 bread wheat variety was used as seed material. Before seeding, wheat seeds were coated with organic acid mixture product (0.75% citric acid, 0.25% glutamate, 0.25% proline, 2% Zn and 96.75 water), in three different doses (500 ml ton-1, 1 l ton-1, 1.5 l ton-1) to compare with control (uncoated). There were statistically significant differences at 5% level in 1000 grain weight and grain yield values in Dogankent location and 1000 grain weight, grain yield and number of spikes in Hacialilocation. Highest yield values were obtained from 500 ml t-1 application dose for both locations. With 500 ml t-1 application dose at Dogankent location, grain yield was 11.9 t ha-1 which was 8.97% higher over control. In Hacali location, 500 ml t-1 application dose was increased yield by 15.96% compared to control which resulted with 10.5 t ha-1 grain yield. No statistically significant difference was observed in quality characteristics (protein, gluten, hardiness and sedimentation) in trials.


2021 ◽  
Vol 9 (1) ◽  
pp. 21
Author(s):  
Andry Tahina Rabeharitsara ◽  
Ratsimba Marie Hanitriniaina ◽  
Rakotomalala Alain Fabrice ◽  
Rakotosaona Rijalalaina ◽  
Nambinina Richard Randriana

2021 ◽  
Vol 937 (2) ◽  
pp. 022138
Author(s):  
I Kreshchenok ◽  
E Lesik (Aistova) ◽  
A Toushkin ◽  
A Toushkina

Abstract Currently, despite of the active development of agriculture and the cultivation of many species, the use of wild food plants is relevant. Ferns also belong to such plants. Eight species of edible ferns grow in the Amur Region, of which 6 species are widespread and form large thickets. The population of the Amur Region uses 4 species for food, the most common is Pteridium japonicum, rarely –Athyrium sinense, Athyrium monomachii, Dryopteris expansa. The literature data on bracken harvesting on the territory of the Amur Region from 1970 to 2019 are presented. It was revealed that the collection takes place spontaneously and unsystematically. Irrational harvesting of raw materials leads to a decrease in yield and quality of harvested products. To restore bracken thickets after collecting, a recovery period of 4-8 years is required. Schemes for the use of fern populations are proposed, taking into account the period of their recovery. For a reasonable recommendation for the use of Athyrium sinense, Athyrium monomachii, Dryopteris expansa, Onoclea interrupta, Diplazium sibiricum in food, it is necessary to conduct research on their chemical composition, nutritional value, methods of preparation and storage.


2020 ◽  
Vol 9 (1) ◽  
pp. 125-130
Author(s):  
Maya Sarah ◽  
Hisham Hisham ◽  
Mushila Rizki ◽  
Ricka Erwinda

Investigation on microwave technique to extract pectin from cocoa pod husk in this study carries out using citric acid and hydrochloric acid (HCl). Extraction proceeds at various microwave powers (180, 300, 450, 600 Watt) and irradiation periods (10, 15, 20, 25, 30 minutes). This study observed effect of power and time to yield and quality of pectin.  Yield of pectin increased at elevated power and time either with citric acid or HCl solvent. Overall pectin quality in this study meet the IPPA quality factor exclude water content which relatively higher. MAE treatment with citric acid using microwave power of 300 Watt for 30 minutes resulted yield of 42% and high pectin quality as compare to MAE treatment with HCl. The best pectin product in this study has moisture content of 8%, ash content of 10%, equivalent weight of 714.29 mg, methoxyl content of 4.8% and galacturonate level of 43%. ©2020. CBIORE-IJRED. All rights reserved


2021 ◽  
Vol 15 (1) ◽  
pp. 61-73
Author(s):  
Serhiy Pyshyev ◽  
◽  
Denis Miroshnichenko ◽  
Ivan Malik ◽  
Aquilino Bautista Contreras ◽  
...  

The use of charcoal (CC) for various industries was analysed; the modern ideas about the factors influencing the process of obtaining CC were considered. The effect of raw materials nature (wood or agricultural wastes) and their characteristics (size, physical properties, chemical composition), as well as carbonization temperature, heating rate, oxygen level and pressure on the yield and quality of CC was described. The existing technologies for charcoal production were analyzed; they were classified according to the type of heating initiation and temperature maintenance during the carbonization process. The Lambiotte, DPC and Carbonex technologies were considered.


2017 ◽  
Vol 15 (2) ◽  
Author(s):  
Feri Manoi

Utilization of medicinal plants both for health and treatment increased at this time. Number of Traditional Medicine Industry (IOT), Small Industries Traditional Medicine (IKOT) and Industrial Appliances (PIRT) is increasing. Thus the demand for raw materials is increasing, one of which is tempuyung. Good quality raw material in the form of crude drugs and extracts need to be considered as related to the efficacy and quality of products for further processing. The study aims to determine the effect size and the old material extraction to the yield and quality of the extract. Activity consists of two sub-activities (1). How to drying (a) the sun covered with black cloth, (b) the sun combination of tools, and (c) drier. Sub-activities (2) extraction technique which consists of two factors: the fineness of materials (20,40 and 60 mesh) and the second factor is the length of the extraction (2, 4, and 6 hours). The study design using factorial completely randomized design with three replications. Parameter observations consisted of yield bulbs, phytochemical screening, quality characteristics, extract yield, and quality extracts. The results showed levels of water extract Sonchus arvensis L. greater than the levels of alcohol cider. Quality simplicia Sonchus arvensis L. dried using a dryer is not different from the quality of the dried under the sun. Fineness of materials and time of extraction affects the yield of the extract Sonchus arvensis L Keywords: Subtlety material, extraction, quality


Author(s):  
José Efraín Ramiírez-Benítez ◽  
Yulisa Yanilka Alcantara-Marte ◽  
Gerson Neftalí Arias Lara ◽  
Nelson Darling Velázquez Vizcaíno ◽  
Yanilka Yulisa Alcantara-Marte

Objective: To evaluate the effect of the pH and extraction temperature on the pectin yield from mango (Mangifera indica) peel, cultivar Banilejo, and its physicochemical properties. Design/methodology/approach: Pectin extraction was done by acid hydrolysis, using hydrochloric acid and ethyl alcohol to precipitate and purify. A randomized design with a factorial arrangement was used, evaluating the effect of pH (1.5, 2.0, and 2.5) and temperature (70, 80, and 90 ºC) on the yield and quality of pectin. Quality was determined by measuring pH, viscosity and moisture content, ash, methoxyls, and esterification degree. Their means were compared using Tukey's test at 95 % confidence. Results: The best results were obtained at pH 2.0 and 80 ºC, reporting an 18.159 % yield, 6.766 % moisture, 2.630 % ash, 0.085 Pa.s of viscosity, 26.307 % methoxyl, and 64.753 % esterification. Study limitations/implications: The different treatment combinations demonstrate that pH, ash, methoxyl content, and esterification degree vary as a function of the assessed pH and extraction temperatures; while viscosity, moisture and yield were not influenced by these variables. Findings/conclusions: It is concluded that mango peel is a viable source to obtain quality pectin.


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