scholarly journals INCREASING THE DEGREE OF EXTRACTION OF ORGANIC IMPURITIES OF RECTIFIED ALCOHOL

2021 ◽  
Vol 43 (1) ◽  
pp. 68-74
Author(s):  
Y. V. Bulii ◽  
O. M. Obodovych ◽  
V. V. Sydorenko
Keyword(s):  
Research Methods ◽  
Ethyl Alcohol ◽  
Esterification Reaction ◽  
Technological Parameters ◽  
Organic Impurities ◽  
Physico Chemical ◽  
Mass Transfer Equipment ◽  
Rectification Unit ◽  
Degree Of Extraction

Obtaining high quality rectified ethyl alcohol is a priority for the further development of the alcohol industry. The solution to this urgent problem is possible under the condition of deeper extraction and concentration of volatile alcohol impurities on the plates of the column equipment of the Distillation/Rectification Unit. In the columns of the Distillation/Rectification Unit simultaneously with the release of volatile alcohol impurities due to the esterification reaction is the formation of organic compounds that degrade its quality and reduce the yield of the final product. Thus, during the interaction of alcohols, acids, and aldehydes, the breakdown products of amino acids, sulfur compounds, and other components of the brew in the fermentation column are the formation of esters, aldehydes, and acetals of organic acids. The aim of the work was to determine the optimal technological modes of distillation of alcohol-containing intermediate products and by-products of the distillation/rectification process in the accelerating column, epuration of wash distillate in the epuration column, the concentration of rectified alcohol in the alcohol column, and its repeated epuration in the column of final clearance, under which the content of organic impurities in rectified ethyl alcohol would be the lowest. Materials and methods.  Research methods were analytical, chemical, physico-chemical with the use of instruments and research methods used in the production of rectified ethyl alcohol. The concentration of volatile alcohol impurities was determined on a gas chromatograph with a column of HP FFAP 50 m × 0.32 m. It is determined that to increase the degree of extraction of organic impurities it is necessary to ensure the concentration of ethyl alcohol in the column bottom of the accelerating column, which does not exceed 4% vol.; pasteurization zone in the rectification column increase to 10 plates, reduce the concentration of ethanol in the epurate to 22-29% by hydroselection of impurities; for hydroselection in the epuration column use free of impurities bottom products of the accelerating column. To improve the quality of rectified alcohol and reduce energy consumption by extending the contact time on the plates of steam and liquid, a promising direction is the use of mass transfer equipment of cyclic mode. The proposed measures require constant monitoring of technological parameters and provide for the operation of technological equipment in an automated mode.

scholarly journals INNOVATIVE METHODS OF JOINT PROCESSING OF HEAD AND FUSEL FRACTION IN RECTIFIED ALCOHOL END BIOETHANOL PRODUCTION

2021 ◽  
Vol 43 (4) ◽  
pp. 43-50
Author(s):  
Y.V. Bulii ◽  
I.I. Yuryk ◽  
O.M. Obodovych ◽  
V.V. Sydorenko
Keyword(s):  
Ethyl Alcohol ◽  
Complete Removal ◽  
Energy Prices ◽  
Technological Parameters ◽  
Cyclic Action ◽  
Joint Processing ◽  
Innovative Methods ◽  
Column Method ◽  
Degree Of Extraction

With rising energy prices, the development and implementation of innovative energy-saving technologies is a priority in the production of rectified alcohol and bioethanol.  By-products of distillation are the head fraction of ethyl alcohol, fusel oil, and fusel alcohol. Existing methods of joint processing of the head and fusel fractions in one column do not provide effective removal together head and intermediate impurities, which adversely affects the quality of commercial alcohol. The aim of the work was to develop methods of joint processing of the head and fusel fractions in the column for the concentration of impurities of cyclic action, to determine the optimal technological parameters of the column, and to test the efficiency of innovative methods in production conditions: to determine the degree of extraction, the concentration of volatile impurities Three schemes of processing of the head and fusel fractions are given. The method I allowed to free the bottom products from the head and intermediate impurities of alcohol and use such a liquid for hydroselection in the epuration column. Method II allowed significantly improving the physicochemical parameters of the bottom water-alcohol products, improving the quality of rectified ethyl alcohol by more complete removal of volatile organic impurities from the zones of their maximum accumulation and reducing their content in the reflux entering the irrigation column. Method III allowed ensuring maximum removal of volatile head and intermediate impurities and reducing the loss of ethyl alcohol with the concentrate of impurities. The use of innovative methods allows for joint processing of the main and fusel fractions in the production of rectified alcohol and bioethanol, to increase the yield of marketable alcohol by 3.8%.

scholarly journals Optimization of Chemical Composition of the Mould Powder for Casting Ø 170 mm Billets from C45 Steel

2016 ◽  
Vol 61 (4) ◽  
pp. 2083-2090 ◽  
Author(s):  
H. Kania ◽  
K. Nowacki
Keyword(s):  
Chemical Composition ◽  
Surface Quality ◽  
Chemical Properties ◽  
Medium Carbon Steel ◽  
Technological Parameters ◽  
Medium Carbon ◽  
Mould Wall ◽  
Physico Chemical ◽  
Mould Powder

Abstract Physico-chemical properties of mould powders and assumed casting parameters for the particular steel grade influence the way of lubricating the surface of the skin of concast billets formed in the mould, as well as heat transfer along its circumference. The paper presents research which main aim was to improve the surface quality of continuous casting round billets (Ø 170 mm) cast from C45 steel. Improvement of the surface quality can be obtained by designing the chemical composition of mould powder for local casting conditions and the technical and technological parameters of CC equipment. Based on the experimental casting from C45 medium carbon steel it was found that there are relationships between the physicochemical properties of mould powder and intensity of skin lubrication and heat transmission to the mould wall.

DECOLOURIZATION AND COD REMOVAL OF WASEWATER FROM ETHANOL PRODUCTION PROCESS FROM MOLASSES BY COAGULANTION USING INORGANIC ALUM

2010 ◽  
Vol 13 (3) ◽  
pp. 92-102
Author(s):  
Trung Duc Le
Keyword(s):  
Ethanol Production ◽  
Oxygen Demand ◽  
Cod Removal ◽  
Treated Wastewater ◽  
Treatment Processes ◽  
Physico Chemical ◽  
Biological Methods ◽  
Treatment Step ◽  
Main Material

The industrial production of ethanol by fermentation using molasses as main material that generates large quantity of wastewater. This wastewater contains high levels of colour and chemical oxygen demand (COD), that may causes serious environmental pollution. Most available treatment processes in Vietnam rely on biological methods, which often fail to treat waste water up to discharge standard. As always, it was reported that quality of treated wastewater could not meet Vietnameses discharge standard. So, it is necessary to improve the treatment efficiency of whole technological process and therefore, supplemental physico-chemical treatment step before biodegradation stage should be the appropriate choice. This study was carried out to assess the effect of coagulation process on decolourization and COD removal in molasses-based ethanol production wastewater using inorganic coaglutant under laboratory conditions. The experimental results showed that the reductions of COD and colour with the utilization of Al2(SO4)3 at pH 9.5 were 83% and 70%, respectively. Mixture FeSO4 – Al2(SO4)3 at pH 8.5 reduced 82% of colour and 70% of COD. With the addition of Polyacrylamide (PAM), the reduction efficiencies of colour, COD and turbidity by FeSO4 – Al2(SO4)3 were 87%, 73.1% and 94.1% correspondingly. It was indicated that PAM significantly reduced the turbidity of wastewater, however it virtually did not increase the efficiencies of colour and COD reduction. Furthermore, the coagulation processes using PAM usually produces a mount of sludge which is hard to be deposited.

Video Profile Sebagai Media Penunjang Promosi Pada Sdk Penabur Gading Serpong

CCIT Journal ◽  
2019 ◽  
Vol 12 (2) ◽  
pp. 149-157
Author(s):  
Dewi Immaniar Desrianti ◽  
Giandari Maulani ◽  
Dana Krisdiana
Keyword(s):  
Marketing Strategy ◽  
Research Methods ◽  
Needs Analysis ◽  
Media Production ◽  
Promotional Effort ◽  
The Public ◽  
Adobe Photoshop ◽  
Support Information

The tight competition between schools in the era of globalization today, requires that the school Ivory Serpong Sower SDK to do the marketing strategy as attractive as possible, in order to enhance the new prospective learner interests as well as improve the quality of and professionalism in the management of the school. It is a promotional effort is used to market products or services to the public, so that they are more familiar with or know the product or service being marketed. Current media information and promotions that use the SDK Sower Ivory Serpong still be printed in the form of banners, brochures and more, so there are still many who have not yet learned about SDK Sower Gading Serpong. The purpose of this research is to inform and promote school SDK Sower Ivory Serpong. Based on a needs analysis is required of media promotion in the form of a video profile, to support information and promotion more attractive and effective by using the software Adobe Premier and Adobe Photoshop. Research methods used namely collecting data through observation, interviews and literature studies, Media Production and concept i.e. preproduction, production and postproduction. Through the design of Video media Profile of this SDK Sower Ivory Serpong can better known to many people and attracting parents to enroll his son in schools � SDK Sower Ivory Serpong

Physico-Chemical Assessment of Groundwater Quality of Ahmednagar Industrial Area

2011 ◽  
Vol 4 (4) ◽  
pp. 228-230
Author(s):  
Patil S.S Patil S.S ◽  
◽  
Gandhe H.D Gandhe H.D ◽  
Ghorade I.B Ghorade I.B
Keyword(s):  
Groundwater Quality ◽  
Industrial Area ◽  
Physico Chemical ◽  
Chemical Assessment

Physico-Chemical Analysis of Groundwater and Effect of Climatic Change in Angul-Talcher Area

2018 ◽  
Vol 6 (12) ◽  
pp. 26
Author(s):  
Aliva Bera ◽  
D.P. Satapathy
Keyword(s):  
Water Resources ◽  
Linear Regression ◽  
Regression Model ◽  
Climatic Change ◽  
Linear Regression Model ◽  
Ann Model ◽  
Quality Of Water ◽  
Physico Chemical ◽  
Simulation Based

In this paper, the linear regression model using ANN and the linear regression model using MS Excel were developed to estimate the physico-chemical concentrations in groundwater using pH, EC, TDS, TH, HCO3 as input parameters and Ca, Mg and K as output parameters. A comparison was made which indicated that ANN model had the better ability to estimate the physic-chemical concentrations in groundwater. An analytical survey along with simulation based tests for finding the climatic change and its effect on agriculture and water bodies in Angul-Talcher area is done. The various seasonal parameters such as pH, BOD, COD, TDS,TSS along with heavy elements like Pb, Cd, Zn, Cu, Fe, Mn concentration in water resources has been analyzed. For past 30 years rainfall data has been analyzed and water quality index values has been studied to find normal and abnormal quality of water resources and matlab based simulation has been done for performance analysis. All results has been analyzed and it is found that the condition is stable. 

Physico-Chemical Aspects of the Influence of Raw Material Components on the Quality of Ceramic Brick

2019 ◽  
Vol 777 (12) ◽  
pp. 37-42
Author(s):  
G.Yu. SHAGIGALIN ◽  
◽  
P.A. FEDOROV ◽  
L.N. LOMAKINA ◽  
◽  
...  
Keyword(s):  
Raw Material ◽  
Ceramic Brick ◽  
Physico Chemical

QUALIDADE DAS ÁGUAS E NÍVEL TRÓFICO DA BACIA DO RIO PACIÊNCIA NA ILHA DO MARANHÃO, BRASIL

2019 ◽  
Vol 21 (2) ◽  
pp. 437-453
Author(s):  
Elna Lucilia Santos Corrêa ◽  
Karina Suzana Feitosa Pinheiro ◽  
Cláudio José Da Silva de Sousa ◽  
Luiz Jorge Bezerra da Silva Dias
Keyword(s):  
Water Quality ◽  
Trophic Status ◽  
The Body ◽  
Chemical Parameters ◽  
Public Supply ◽  
Physico Chemical ◽  
Great Availability ◽  
Del Rio ◽  
Fluvial Environments

O Brasil apresenta grande disponibilidade de água doce em seus mananciais. Fazendo parte desse recurso encontra-se, o rio Paciência, localizado na Ilha do Maranhão destacado pela sua importância local, principalmente por contribuir com suas águas para recarga dos mananciais subterrâneos, fonte de abastecimento público de vários bairros de São Luís, capital do estado. No entanto, este rio vem sofrendo comprometimento da qualidade de suas águas, consequência do processo de uso e ocupação dos espaços em sua bacia. Destacando-se como um dos principais problemas relacionados a qualidade de ambientes fluviais,  a eutrofização, que consiste no processo em que o corpo d’água adquire elevados níveis de nutrientes (fosfatos e nitratos), é um indicador determinante da qualidade da água. Neste sentido, o objetivo deste trabalho foi caracterizar a qualidade da água e do estado trófico na bacia hidrográfica do rio Paciência atráves dos parâmetros fisico-químico evidenciando os trechos mais comprometidos conforme os valores alcançados nas análises. Os resultados das análises foram comparados com a CONAMA No. 357/05 que indicaram uma situação preocupante quanto à qualidade da água no local de estudo.Palavras-chave: Qualidade de água; Eutrofização; Ilha do Maranhão. ABSTRACTThe Brazil has great availability of fresh water in its springs. Within these contexts, the Paciência River, located on the Island of Maranhão stands out for its local importance, mainly for contributing its waters to the recharge of the underground springs, source of public supply of several districts of São Luís, capital of the state. However, this river has been compromising the quality of its waters, a consequence of the process of use and occupation of the spaces in its basin. Highlighting as one of the main problems related to the quality of fluvial environments, eutrophication, which consists of the process in which the body of water acquires high levels of nutrients (phosphates and nitrates), is a determinant indicator of water quality. In this sense, the objective of this work was to characterize the water quality and trophic status in the Paciência river basin through the physico-chemical parameters, showing the most compromised stretches according to the values reached in the analyzes. The results of the analyzes were compared with CONAMA No. 357/05 which indicated a worrying situation regarding the quality of the water at the place of study.Keywords: Water quality; Eutrophication; Island of Maranhão. RESUMENBrasil tiene gran disponibilidad de agua dulce en sus manantiales. Parte de este recurso es el río Paciencia, ubicado en la isla de Maranhão, que destaca por su importancia local, principalmente porque contribuye con sus aguas a recargar las fuentes subterráneas, fuente de suministro público de varios barrios de São Luís, capital del estado. Sin embargo, este río se ha visto afectado por la calidad de sus aguas, como consecuencia del proceso de uso y ocupación de los espacios en su cuenca. Destacando como uno de los principales problemas relacionados con la calidad de los ambientes fluviales, la eutrofización, que consiste en el proceso en el que el cuerpo de agua adquiere altos niveles de nutrientes (fosfatos y nitratos), es un indicador determinante de la calidad del agua. En este sentido, el objetivo de este trabajo fue caracterizar la calidad del agua y el estado trófico en la cuenca del río Paciência a través de los parámetros fisicoquímicos, mostrando las secciones más comprometidas de acuerdo con los valores alcanzados en los análisis. Los resultados de los análisis se compararon con CONAMA N°. 357/05, que indicó una situación preocupante con respecto a la calidad del agua en el sitio de estudio.Palabras clave: Calidad del agua; Eutrofización, Isla Maranhão.

Phamacognostical and Pharmaceutical Evaluation of Chandrashakaladi Vataka - A herbal formulation

2016 ◽  
Vol 1 (3) ◽  
Author(s):  
Dr. Akash S Changole ◽  
Mandip Goyal ◽  
Harish CR
Keyword(s):  
Classical Method ◽  
Raw Materials ◽  
Herbal Medicines ◽  
Vital Role ◽  
Published Data ◽  
Herbal Formulation ◽  
Physico Chemical ◽  
Good Manufacturing Practices ◽  
Solvent Systems

Background: Quality control and the standardization of herbal medicines involve steps like standard source and quality of raw materials, good manufacturing practices and adequate analytical screening. These practices play a vital role in guaranting the quality and stability of herbal preparations. Chandrashakaladi Vataka is an Ayurvedic herbal formulation mentioned to be beneficial in Kushtha. Till date no published data is available on its analytical profile. Aim: To develop the Pharmacognostical and Phyto-chemical profile of Chandrashakaladi Vataka. Material and Methods: Chandrashakaladi Vataka was prepared as per classical method and analytical findings were recorded. Samples were subjected to organoleptic analysis, physico-chemical analysis and HPTLC examination by optimizing the solvent systems. Results and Conclusions: Pharmacognostical profile of Chandrashakaladi Vataka was established. Loss on drying, Ash value, Acid insoluble extract, Methanol soluble extract, Chandrashakaladi Vataka was found within prescribed limits. HPTLC profile of Chandrashakaladi Vataka revealed 12 spots at 254 nm and 13 spots at 366 nm.

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