scholarly journals Kinetics of Oil Extraction from Candlenut (Aleurites moluccana)

2019 ◽  
Vol 12 ◽  
pp. 1-8
Author(s):  
Faiznur Mohd Fuad ◽  
Wan Abdul Azim Wan Azzuddin
Keyword(s):  
Solvent Extraction ◽  
Extraction Process ◽  
Oil Extraction ◽  
Extraction Time ◽  
Oil Yield ◽  
Model Parameters ◽  
Extraction Temperature ◽  
Logarithmic Model ◽  
Aleurites Moluccana ◽  
Kinetics Of

Oil from candlenut (Aleurites moluccana) was extracted using a solvent extraction technique. The influence of three parameters namely extraction time, extraction temperature as well as liquid to solid (L/S) ratio on the candlenut oil yield were studied to optimise the extraction conditions for achieving maximum oil yield. The maximum candlenut oil yield (35.67%) was achieved using methanol as a solvent at a temperature of 45oC for 80 min of extraction period. The optimum L/S ratio was 10ml/g. It was found that the candlenut oil yield increases with the increase of extraction time, extraction temperature and L/S ratio. Kinetics of solvent extraction of oil from candlenut was evaluated using Peleg’s model and Logarithmic model. The model parameters were calculated using the experimental data.  The kinetics of candlenut oil extraction conforms very well to the Peleg’s model with a high R2 value of 0.9927 and low MRPD value of 1.827%. However, the Logarithmic model can fairly describe the candlenut oil extraction process with the values of R2 and MRPD of 0.9653 and 4.352%, respectively.

A Study on the Investigation of Diffusion Coefficient for Oil Extraction from Terebinth (Pistacia terebinthus L.) Seeds

2020 ◽  
Vol 10 (2) ◽  
pp. 144-153
Author(s):  
Fatih Kaya ◽  
Ahmet Özer
Keyword(s):  
Particle Size ◽  
Diffusion Coefficients ◽  
Initial Conditions ◽  
Extraction Process ◽  
Oil Extraction ◽  
Extraction Yield ◽  
Extraction Time ◽  
Solvent Ratio ◽  
Extraction Temperature ◽  
Pistacia Terebinthus

Objective: In this study, the extraction of oil from Pistacia terebinthus L’s seeds grown in Elazig-TURKEY and called menengic in domestic region was investigated. Crude oil content of the seeds obtained from this region was determined as approximately 47% (w/w). Methods: Effects of the parameters such as extraction time, temperature, seeds/solvent ratio (dosage), the particle size of seeds and type of solvent were examined on the oil extraction yield. In this context, it has concluded that up to a certain point, the extraction time has increased the yield of oil extracted. But the extraction temperature showed activity as depending on the solvent type. Results: As expected, it has been observed that the yield of oil has decreased depending on the increase in particle size and dosage as well. The mathematical model obtained by solving Fick's second law under the appropriate boundary and initial conditions were used to calculate diffusion coefficients for the extraction process. Diffusion coefficients for the seeds with a particle size of 0.55 mm were found to be between 1.15x10-11 and 1.86x10-11 m2s-1. To compare the extraction yield of Pistacia terebinthus L’s seeds with that of sunflower at the same conditions, the diffusion coefficients of sunflower seeds were calculated in the range of 9.11x10-12 and 1.13x10-11 m2s-1. Conclusion: These figures show that the diffusion coefficients calculated for both oily seeds are nearly equivalent to each other. The fatty acid composition of extracted oil from Pistacia terebinthus L’s seeds was determined by GC-FID. The GC-FID results showed that oleic, linoleic (ω-6) and palmitic acid were main fatty acids in the oil obtained from menengic seeds.

scholarly journals Optimization of Essential Oil Extraction Process of White Pepper (Piper nigrum L.) Harvested in Phu Quoc Island, Kien Giang Province, Vietnam

2020 ◽  
Vol 32 (11) ◽  
pp. 2707-2712
Author(s):  
Thien Hien Tran ◽  
Thi Cam Quyen Ngo ◽  
Hoang Duy Ngo ◽  
Nguyen Huu Thuan Anh ◽  
Ton Nu Thuy An ◽  
...  
Keyword(s):  
Essential Oil ◽  
Extraction Process ◽  
Black Pepper ◽  
Oil Extraction ◽  
Extraction Time ◽  
Gas Chromatography Mass Spectrometry ◽  
Piper Nigrum ◽  
Extraction Temperature ◽  
Green Pepper ◽  
White Pepper

Vietnam is a leading producer and exporter of products harvested from plants of the family Piperaceae such as green pepper, black pepper, red pepper and white pepper. In this study, an attempt is made to examine the essential oil extraction process with the material of white pepper grown and harvested in Phu Quoc island, Vietnam. To maximize essential oil production, three factors consisting the ratio of materials and solvents, extraction time and extraction temperature were selected and optimized. The surface response methodology optimization resulted the highest yield of 3.6%, achieved at the ratio of material and water ratio of 1:20 g/g, extraction time of 96 min and at 130 ºC. A high F values, low P values (< 0.0001), the determination coefficient (R2 = 0.9993) and a non-significant lack of fit suggested a strong correlation between actual and predicted values of the responses. The essential oil obtained was determined for chemical composition by gas chromatography-mass spectrometry (GC-MS) method. The GC-MS results showed that major constituents existing in the oil sample were limonene, 3-carene, sabinene, β-pinene, α-pinene and α-phellandrene, accounting for 27.059, 23.345, 17.903, 9.996, 5.167 and 4.588%, respectively.

scholarly journals Solvent Extraction of Jatropha Oil for Biodiesel Production: Effects of Solvent-to-Solid Ratio, Particle Size, Type of Solvent, Extraction Time, and Temperature on Oil Yield

2021 ◽  
Vol 2021 ◽  
pp. 1-8
Author(s):  
Justin W. Ntalikwa
Keyword(s):  
Particle Size ◽  
Solvent Extraction ◽  
Oil Recovery ◽  
Quality Parameters ◽  
Biodiesel Production ◽  
Extraction Time ◽  
Oil Yield ◽  
Extraction Temperature ◽  
Jatropha Oil ◽  
Solid Ratio

The aim of this study was to examine the effects of solvent-to-solid ratio, particle size, extraction time, and temperature on the extraction of Jatropha oil using three organic solvents, i.e., n-hexane, petroleum ether, and ethanol. The Soxhlet extraction method was used, and the parameters were varied in the following ranges: extraction temperature of 24–80°C, extraction time of 2 to 8 h, solvent-to-solid ratio of 4 : 1 to 7 : 1, and particle size of 0.5–0.8 mm. After obtaining optimal conditions, a large volume of Jatropha oil was prepared, purified, and subjected to analysis of quality parameters. It was found that the oil content of the Jatropha curcas L. seeds used was 48.2 ± 0.12% w/w. The highest oil yield of 47.5 ± 0.11% w/w corresponding to an oil recovery of 98.6 ± 0.3% w/w was obtained with n-hexane under the following conditions: solvent-to-solid ratio of 6 : 1, particle size of 0.5–0.8 mm, extraction time of 7 h, and extraction temperature of 68°C. This was followed by that of petroleum ether (46.2 ± 0.15% w/w) and lastly by ethanol (43 ± 0.18% w/w). The quality parameters of the oil extracted compared favorably well with most of the values reported in the literature, suggesting that the oil was of good quality for biodiesel production. Environmental and safety concerns over the use of hexane pose a great challenge. Thus, ethanol, which is environmentally benign, is recommended for application. The conditions for ethanol extraction that gave high oil yield were as follows: extraction temperature of 70°C, extraction time of 7 h, solvent-to-solid ratio of 6 : 1, particle size of 0.5–0.8 mm, and oil yield of 43 ± 0.18% w/w corresponding to an oil recovery of 89.2 ± 0.4% w/w.

scholarly journals Proses Ekstraksi Minyak Alga Chlorella.sp menggunakan Metode Sokhletasi

2020 ◽  
Vol 5 (1) ◽  
pp. 12
Author(s):  
Yustia Wulandari Mirzayanti ◽  
Dian Yanuarita Purwaningsih ◽  
Siti Nur Faida ◽  
Nurza Istifara
Keyword(s):  
Fatty Acids ◽  
Linoleic Acid ◽  
Solvent Extraction ◽  
Oil Content ◽  
Extraction Process ◽  
Oil Extraction ◽  
Reproductive Rate ◽  
Acid Number ◽  
Extraction Time ◽  
Algae Oil

 Chlorella.sp is a type of green algae and has no flagella. One of the advantages of algae Chlorella.sp is that it has a high reproductive rate. Chlorella.sp algae is one of the algae that has oil content from its body mass. This study aims to determine the effect of the amount of solvent, extraction time on the Chlorella.sp algae oil extraction process using methanol solvent through the sokhletation method. Also, knowing the composition of fatty acids and acid numbers from algae oil Chlorella.sp. The ratio of Chlorella.sp algae: the amount of methanol solvent used are 1: 6; 1: 9 and 1:12 gr/ml. Then for the extraction time variation are 4; 4,5; 5; 5.5 and 6 hours. Chlorella.sp algae oil extraction process using sokhletation method is carried out at 70oC. The best results through the% yield and number parameters obtained by 17.98% Chlorella.sp algae oil yield ratio of 1:12 and the extraction time for 5.5 hours. Chlorella.sp algae oil has an acid number of 3.14 mg NaOH/g. Based on the results of the GC-MS test it is known that Chlorella.sp algae are dominated by linoleic acid by 55.01%area. ABSTRAKChlorella.sp merupakan jenis alga berwarna hijau dan tidak memiliki flagella. Salah satu kelebihan dari alga Chlorella.sp yaitu memiliki tingkat reproduksi yang tinggi. Alga Chlorella.sp merupakan salah satu alga yang memiliki kandungan minyak dari massa tubuhnya. Penelitian ini bertujuan untuk mengetahui pengaruh jumlah pelarut, waktu ekstraksi pada proses ekstraksi minyak alga Chlorella.sp menggunakan pelarut methanol melalui metode sokhletasi. Selain itu, mengetahui komposisi asam lemak dan bilangan asam dari minyak alga Chlorella.sp. Variasi rasio perbandingan antara alga Chlorella.sp : jumlah pelarut metanol yang digunakan yaitu 1:6; 1:9 dan 1:12 gr/ml. kemudian untuk variasi waktu ekstraksi adalah 4; 4,5; 5; 5,5 dan 6 jam. Proses ekstraksi minyak alga Chlorella.sp menggunakan metode sokhletasi dilakukan pada temperatur 70oC. Hasil terbaik melalui parameter %yield dan bilangan diperoleh sebesar 17,98% yield minyak alga Chlorella.sp dengan ratio perbandingan 1:12 dan waktu ekatraksi selama 5,5 jam. Minyak alga Chlorella.sp memiliki bilangan asam sebesar 3,14 mgNaOH/g. Berdasarkan hasil uji GC-MS diketahui bahwa untuk alga jenis Chlorella.sp didominasi oleh asam linoleat sebesar 55,01%area.

scholarly journals Green Solvent Improving Mechanical Disruption of Palm Kernel Oil Extraction

2020 ◽  
Author(s):  
Eko K. Sitepu ◽  
Andy Chandra ◽  
Emma F. Zaidar ◽  
Annur Vika ◽  
Firman Sebayang ◽  
...  
Keyword(s):  
Ethyl Acetate ◽  
Palm Kernel ◽  
Extraction Process ◽  
Extraction Methods ◽  
Oil Extraction ◽  
Extraction Time ◽  
Oil Yield ◽  
Green Solvents ◽  
Palm Kernel Oil ◽  
Kernel Oil

Abstract Even though the mechanical extraction process offers a simple and environmentally friendly process, the recovery of oil is relatively low. Thermal pre-treating the oilseed increases the oil yield but produces unwanted oil colour. A new method which combines grinding and extraction using green solvents was developed to extract palm kernel oil. The performance of six different green solvents such as water, ethanol, isopropyl alcohol, dimethyl carbonate, ethyl acetate, and d-limonene in extraction palm kernel oil was determined using a controllable blender extractor (CBE), new extraction equipment modified from a household blender appliance. Further, ethyl acetate, which produced the maximum oil yield, was used to study the effect of the operating parameters of the CBE. The oil yield of 34.2 ± 0.02% was obtained in the extraction condition of the ratio of palm kernel to ethyl acetate of 1:7, rotational speed of 5000 rpm and 10 minutes extraction time. Compared to other green extraction methods, the CBE-intensified palm kernel oil extraction could save >70% energy consumption. In terms of extraction time, the CBE-intensified could extract palm kernel oil faster than existing extraction methods.

Effect of Particle Size on the Oil Yield and Catechin Compound Using Accelerated Solvent Extraction

2013 ◽  
Vol 60 (1) ◽  
Author(s):  
Mohd Azizi Che Yunus ◽  
Manzurudin Hasan ◽  
Norasikin Othman ◽  
Siti Hamidah Mohd-Setapar ◽  
Liza Md.-Salleh ◽  
...  
Keyword(s):  
Particle Size ◽  
Solvent Extraction ◽  
Accelerated Solvent Extraction ◽  
Extraction Time ◽  
Oil Yield ◽  
Particle Sizes ◽  
Experimental Range ◽  
Areca Catechu ◽  
Effect Of Particle Size ◽  
Extraction Cycle

Kajian ini bertujuan untuk mengkaji kesan saiz zarah ke atas pengekstrakan sebatian catechin daripada biji Areca catechu L. dengan menggunakan Pengekstrakan Pelarut Terpecut (PPT). Saiz zarah biji Areca catechu dipelbagaikan dari 75 μm sehingga 500 μm. Pengekstrakan telah dijalankan padaparameter tetap iaitu suhu (140oC), tekanan (1500 psi), masa (10 minit), isipadu semburan (60%) dan satu kitaran pengekstrakan, masing-masing. Hasil minyak peratusan yang lebih tinggi adalah 300 mg minyak / gram sampel (30.00% pati minyak) ditemui pada 125 μm. Walaubagaimanapun, kandungan catechin dalam pati minyak hanya 0.0375 mg catechin / gram sampel. Saiz zarah yang terbaik dalam julat uji kaji ini telah dikenal pasti pada 500 μm yang memberikan kandungan catechin yang tinggi iaitu 0.0515 mg catechin / gram sampel dari 247.5 mg minyak / gram sampel (24.75% pati minyak). Kata kunci: Saiz zarah; catechin; LC-MS-TOF; pengekstrakan pelarut terpecut The purpose of this work is to investigate the effects of particle size on the extraction of catechincompound from Areca catechu L. seeds by using Accelerated Solvent Extraction (ASE). The particle sizes of Areca catechu L. seeds are varied from 75 µm until 500 µm. The extraction is conducted at fixed parameters which are temperature (140oC), pressure (1500 psi), extraction time (10 minutes), flush volume (60%) and the static cycle is done for 1 extraction cycle respectively. Higher percentage oil yield of 300mg oil/gram of sample (30.00% oil yield) is found at 125 µm. However, the amount of catechin in oil yields is only 0.0375 mg of catechin/gram of sample. The best of particle size within the experimental range has been identified at 500 µm which gives a high content of catechin with 0.0515 mg Catechin/gram of sample from 247.5 mg oil/gram of sample (24.75% oil yield). Keywords: Particle size; catechin; LC-MS-TOF; accelerated solvent extraction

scholarly journals Central Composite Design, Kinetic Model, Thermodynamics, and Chemical Composition of Pomelo (Citrus Maxima (Burm.) Merr.) Essential Oil Extraction by Steam Distillation

Processes ◽  
2021 ◽  
Vol 9 (11) ◽  
pp. 2075
Author(s):  
Tan Phat Dao ◽  
Thanh Viet Nguyen ◽  
Thi Yen Nhi Tran ◽  
Xuan Tien Le ◽  
Ton Nu Thuy An ◽  
...  
Keyword(s):  
Activation Energy ◽  
Kinetic Model ◽  
Essential Oil ◽  
Rate Constant ◽  
Flow Rate ◽  
Steam Distillation ◽  
Extraction Process ◽  
Oil Extraction ◽  
Extraction Time ◽  
Pomelo Peel

Pomelo peel-derived essential oils have been gaining popularity due to greater demand for stress relief therapy or hair care therapy. In this study, we first performed optimization of parameters in the pomelo essential oil extraction process on a pilot scale to gain better insights for application in larger scale production. Then extraction kinetics, activation energy, thermodynamics, and essential oil quality during the extraction process were investigated during the steam distillation process. Three experimental conditions including material mass, steam flow rate, and extraction time were taken into consideration in response surface methodology (RSM) optimization. The optimal conditions were found as follows: sample weight of 422 g for one distillation batch, steam flow rate of 2.16 mL/min and extraction time of 106 min with the coefficient of determination R2 of 0.9812. The nonlinear kinetics demonstrated the compatibility of the kinetic model with simultaneous washing and unhindered diffusion with a washing rate constant of 0.1515 min−1 and a diffusion rate constant of 0.0236 min−1. The activation energy of the washing and diffusion process was 167.43 kJ.mol−1 and 96.25 kJ.mol−1, respectively. The thermodynamic value obtained at the ΔG° value was −35.02 kJ.mol−1. The quality of pomelo peel essential oil obtained by steam distillation was characterized by its high limonene content (96.996%), determined by GC-MS.

scholarly journals Ultrasound-Assisted Deep Eutectic Solvent Extraction of Anthocyanins from Blueberry Wine Residues: Optimization, Identification, and HepG2 Antitumor Activity

Molecules ◽  
2020 ◽  
Vol 25 (22) ◽  
pp. 5456
Author(s):  
Hongkun Xue ◽  
Jiaqi Tan ◽  
Qian Li ◽  
Jintian Tang ◽  
Xu Cai
Keyword(s):  
Solvent Extraction ◽  
Antitumor Activity ◽  
Deep Eutectic Solvent ◽  
Extraction Process ◽  
Ultrasonic Power ◽  
Extraction Temperature ◽  
Brewing Process ◽  
Ultrasound Assisted ◽  
Optimum Extraction ◽  
Better Than

Blueberry wine residues produced during the wine-brewing process contain abundant anthocyanins and other bioactive compounds. To extract anthocyanins from blueberry wine residues more efficiently, a novel procedure of ultrasound-assisted deep eutectic solvent extraction (UADESE) was proposed in this work. The extraction process was optimized by response surface methodology coupled with genetic algorithm. The optimum extraction parameters to achieve the highest yield of anthocyanins (9.32 ± 0.08 mg/g) from blueberry wine residues by UADESE were obtained at water content of 29%, ultrasonic power of 380 W, extraction temperature of 55 °C, and extraction time of 40 min. The AB-8 macroporous resin combined with Sephadex LH-20 techniques was used to purify the crude extract (CE) obtained under optimum extraction conditions and analyze the anthocyanins composition by HPLC-ESI-MS/MS. The cyanidin-3-rutinoside with purity of 92.81% was obtained. The HepG2 antitumor activity of CE was better than that of the purified anthocyanins component. Moreover, CE could increase the intracellular reactive oxygen species levels and the apoptosis, and arrest HepG2 cells in the S phases. These findings provided an effective and feasible method for anthocyanins extraction, and reduced the environmental burden of this waste.

scholarly journals Extraction Process of Polyphenols from Soybean (Glycine max L.) Sprouts: Optimization and Evaluation of Antioxidant Activity

Processes ◽  
2019 ◽  
Vol 7 (8) ◽  
pp. 489 ◽  
Author(s):  
Xuan Tien Le ◽  
Vo Luu Lan Vi ◽  
Tran Quoc Toan ◽  
Long Giang Bach ◽  
Tran Thanh Truc ◽  
...  
Keyword(s):  
Antioxidant Activity ◽  
Ethanol Concentration ◽  
Dry Weight ◽  
Extraction Process ◽  
Extraction Time ◽  
Extraction Temperature ◽  
Polyphenol Content ◽  
Experimental Conditions ◽  
Total Polyphenol ◽  
Total Polyphenol Content

This research aimed to optimize the total polyphenol content (TPC) extracted from soybean sprout powder under different experimental parameters, including ethanol concentration (60–100% v/v), extraction temperature (40–80 °C), extraction time (15–150 min), material:solvent ratio (1:4–1:10 g/mL), the number extraction cycles (1, 2 and 3 times), the age of sprout (0–7 days), and the used part of the sprout (cotyledon, hypocotyl, or radicle). The obtained results were used in response surface methodology, in combination with a central composite design, to model the total polyphenol content (TPC) with respect to three variables, including ethanol concentration, extraction temperature, and material:solvent ratio. The experimental conditions for optimal recovery of TPC consisted of ethanol concentration of 88% (v/v), extraction temperature of 59 °C, material:solvent ratio of 1:6.5 g/mL, extraction time of 60 min, and 2 cycles of maceration. In addition, for maximal TPC, the sprout should undergo the germination of 5 days and the radicle fraction should be used. Based on the suggested optimum conditions, the obtained and verified TPC was 19.801 mg genistein (GE)/g dry weight (d.w.). The obtained dried extract also exhibited low antioxidant activity.

scholarly journals Mechanical oil extraction of Nicotiana tabacum L. seeds: analysis of main extraction parameters on oil yield

2016 ◽  
Vol 47 (3) ◽  
pp. 142-147 ◽  
Author(s):  
Salvatore Faugno ◽  
Luisa Del Piano ◽  
Mariano Crimaldi ◽  
Gennaro Ricciardiello ◽  
Maura Sannino
Keyword(s):  
Seed Oil ◽  
Chemical Properties ◽  
Temperature Sensors ◽  
Oil Extraction ◽  
Screw Press ◽  
Edible Oil ◽  
Oil Yield ◽  
Extraction Temperature ◽  
Tobacco Seed ◽  
Nicotiana Tabacum L

The aim of this study is to find the best conditions of tobacco seed oil (TSO) press extraction, combining multiple extraction factors such as screw rotational speed, seeds preheating and extraction temperature, in order to have a higher oil yield. The extracted oil, having peculiar chemical properties, can be used for several purposes, also as edible oil. TSO was obtained using a mechanical screw press that has been assembled with a head press and with speed and temperature sensors mounted on the machine. Results show that the combination of high extraction temperature, slow rotational screw speed and seeds preheating has a significant effect on the oil yield. Extracting under such conditions, oil yield is 79.47±0.12 as % (w/w), which is 25% (w/w) more than the lowest yield among investigated condition.

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