scholarly journals Modelling and Experimental Investigation on the Settling Rate of Kaolinite Particles in Non-Ideal Sedimentation Stage under Constant Gravity

Materials ◽  
2020 ◽  
Vol 13 (17) ◽  
pp. 3785
Author(s):  
Jianfu Wang ◽  
Xin Kang ◽  
Chunyin Peng
Keyword(s):  
Sedimentation Coefficient ◽  
Deposition Process ◽  
Soluble Starch ◽  
Aqueous System ◽  
Particle Sedimentation ◽  
Sedimentary Characteristics ◽  
Clay Concentration ◽  
Kaolinite Suspension ◽  
Time Required ◽  
Clay Suspensions

We compared the catalytic effects of two polymers (soluble starch and apple pectin) on the flocculation of kaolinite suspension. Moreover, the relationship between the zeta potential value and the time when kaolin particle sedimentation occurred was verified, and the mechanism of flocculation was analyzed. Additionally, a constitutive model was proposed to simulate the non-ideal sedimentation of clay particles in an aqueous system under constant gravity. This model not only considers the inhomogeneity of the solute but also simulates the change in clay concentration with time during the deposition process. This model proposes a decay constant (α) and sedimentation coefficient (s). The model can also be used to calculate the instantaneous sedimentation rate of the clay suspensions at any time and any depth for the settling cylinder. These sedimentary characteristics were simulated by adopting the established deposition model. The results show that the model is capable of predicting the time required for the complete sedimentation of particles in the aqueous system, suggesting the feasibility of engineering wastewater treatment, site dredging, etc.

scholarly journals Improvement of the Rheological and Filtration Properties of Drilling Mud Using the Syrian Clay

2020 ◽  
Vol 26 (5) ◽  
pp. 211-230
Author(s):  
Adnan Ibrahim Barodi
Keyword(s):  
Xanthan Gum ◽  
Drilling Fluid ◽  
Drilling Fluids ◽  
Drilling Mud ◽  
Clay Concentration ◽  
Fluid Properties ◽  
Drilling Operations ◽  
Solid Part ◽  
Time Required ◽  
Filtration Properties

Drilling fluid properties and formulation play a fundamental role in drilling operations. The Classical water-based muds prepared from only the Syrian clay and water without any additives((Organic and industrial polymers) are generally poor in performance. Moreover, The high quantity of Syrian clay (120 gr / l) used in preparing drilling fluids. It leads to a decrease in the drilling speed and thus an increase in the time required to complete the drilling of the well. As a result, the total cost of drilling the well increased, as a result of an increase in the concentration of the solid part in the drilling fluid. In this context, our study focuses on the investigation of the improvement in drilling mud   Prepared from the Syrian clay by reducing the clay concentration to (50 gr / L). And compensate for the remaining amount (70 gr / l) of clay by adding (natural and industrial polymers) The rheological properties and filtration are measured at different concentrations of polymers .. In light of the experiments, we determine the polymers' concentrations that gave good results in improving the flow properties and controlling the Filter. It is polymers that have given good results:، HEC، HEC and Xanthan Gum  PAC and HEC، CMCHV، PolyAcryl Amid ، Xanthan Gum .

scholarly journals Sediment Characteristics of Beachrock: A Baseline Investigation Based on Microbial Induced Carbonate Precipitation at Krakal-Sadranan Beach, Yogyakarta, Indonesia

2020 ◽  
Vol 10 (2) ◽  
pp. 520 ◽  
Author(s):  
Lutfian Rusdi Daryono ◽  
Kazunori Nakashima ◽  
Satoru Kawasaki ◽  
Anastasia Dewi Titisari ◽  
Didit Hadi Barianto
Keyword(s):  
Rare Earth ◽  
Rare Earth Elements ◽  
Deposition Process ◽  
The Novel ◽  
Bacterial Strains ◽  
Sedimentary Process ◽  
Sedimentary Characteristics ◽  
Heavy Rare Earth Elements ◽  
Light Rare Earth Elements ◽  
Ureolytic Bacteria

Isolation of ureolytic bacteria and geochemical analysis of beachrock from Krakal-Sadranan Beach (Yogyakarta, Indonesia) were conducted to determine natural sedimentary characteristics of the beachrock. The beachrock was also examined to determine the depositional conditions and distribution of rare earth elements. An increased concentration of total rare earth elements, both heavy rare earth elements (terbium, dysprosium, yttrium, holmium, erbium, thulium, ytterbium, and lutetium) and light rare earth elements (lanthanum, cesium, praseodymium, neodymium, samarium, europium, and gadolinium) signals that the beachrock deposition process happened under oxidative environmental conditions. This study proposes the novel use of ureolytic bacteria in a depositional environment for carbonate control of a sedimentary process for the development of artificial rock to mitigate coastal erosion. The resulting bacterial strains are highly homologous to the 16S rDNA nucleotide sequence of the species Oceanobacillus profundus, Vibrio maritimus, and Pseudoalteromonas tetradonis.

The determination of clay in heavy soils

1921 ◽  
Vol 11 (3) ◽  
pp. 293-303 ◽  
Author(s):  
A. F. Joseph ◽  
F. J. Martin
Keyword(s):  
Sodium Carbonate ◽  
Acid Treatment ◽  
Sedimentation Method ◽  
Centrifugal Process ◽  
American Method ◽  
Time Required ◽  
Clay Suspensions

1. The Sudan method for clay determination worked out by Dr Beam in 1911 has been critically examined and compared with the methods in general use in England and America.2. The essential points of the method lie in (a) the use of sodium carbonate instead of ammonia as the deflocculating agent, and (b) the use of a camel-hair brush for puddling the clay. It differs from the English (and resembles the American) method in that no preliminary acid treatment is used, the height of the sedimentation column is 10 cms. and the time of subsidence 8 hours.3. It can be applied to a sedimentation or centrifugal process: the results agree well with each other and with those obtained by the American method.4. When modified by inclusion of acid treatment, by increasing the time of sedimentation from 8 to 24 hours and reducing the height of the column to 8·6 cms., the results agree well with those obtained by the English method.5. Treatment with acid either in the preliminary operations or for deflocculating clay suspensions may lead to uncertainty in the results in some cases as it causes loss of “clay” by solution.6. The Sudan sedimentation method can be carried out in about one-eighth the time required for the English method, and the centrifugal in about one-third the time required for the American. For general use the sedimentation method is preferred as requiring less attention.

scholarly journals Development and operation of an automatic air pluviation system for physical modelling applications

2021 ◽  
pp. 1-41
Author(s):  
Jinbiao Wu ◽  
George Kouretzis ◽  
Jubert Pineda ◽  
Laxmi Suwal ◽  
Ross Gibson ◽  
...  
Keyword(s):  
Pressure Sensors ◽  
Earth Pressure ◽  
Physical Modelling ◽  
Deposition Process ◽  
Dense Sand ◽  
Cone Penetration Testing ◽  
Deposition Parameters ◽  
Tip Resistance ◽  
Time Required ◽  
Sand Beds

This paper presents an air pluviation system, developed to facilitate 1-g physical model tests in granular soils. The deposition process is fully automated and requires minimal input from the operator, thereby significantly reducing the time required to deposit large volume of granular material, improving the uniformity of the prepared specimens, and the reliability of test results. The components comprising the pluviation system have been calibrated to produce loose-to-very dense sand beds, of relative density that ranges between Dr=7% and Dr>100% of the maximum density achieved with the procedures described in the pertinent standards. The testing chamber where sand is deposited is instrumented with an array of pressure sensors, and the rig is equipped with a miniature Cone Penetration Testing (mini-CPT) device. Measurements from the earth pressure sensors and cone tip resistance profiles are used to evaluate how friction at the sand-chamber interfaces affects the distribution of geostatic stresses inside the chamber, the uniformity of sand beds, and boundary effects during deposition and during mini-CPT testing. The air pluviation system allows preparing layered sand profiles by adjusting the deposition parameters on the fly, and this feature is demonstrated via the analysis of mini-CPT tests performed in layered sand beds.

The Critical Point Drying Method Applied to Scanning Electron Microscopy of L-929 Cells

1970 ◽  
Vol 28 ◽  
pp. 278-279
Author(s):  
Charles TurnbiLL ◽  
Delbert E. Philpott
Keyword(s):  
Electron Microscopy ◽  
Carbon Dioxide ◽  
Surface Tension ◽  
Critical Point ◽  
Freeze Drying ◽  
Attractive Alternative ◽  
Crystal Formation ◽  
Critical Point Drying ◽  
Time Required ◽  
Scanning Electron

The advent of the scanning electron microscope (SCEM) has renewed interest in preparing specimens by avoiding the forces of surface tension. The present method of freeze drying by Boyde and Barger (1969) and Small and Marszalek (1969) does prevent surface tension but ice crystal formation and time required for pumping out the specimen to dryness has discouraged us. We believe an attractive alternative to freeze drying is the critical point method originated by Anderson (1951; for electron microscopy. He avoided surface tension effects during drying by first exchanging the specimen water with alcohol, amy L acetate and then with carbon dioxide. He then selected a specific temperature (36.5°C) and pressure (72 Atm.) at which carbon dioxide would pass from the liquid to the gaseous phase without the effect of surface tension This combination of temperature and, pressure is known as the "critical point" of the Liquid.

Reaction couples of ceramic thin films prepared by CVD

1988 ◽  
Vol 46 ◽  
pp. 798-799
Author(s):  
D.W. Susnitzky ◽  
S.R. Summerfelt ◽  
C.B. Carter
Keyword(s):  
Thin Film ◽  
Vapor Deposition ◽  
Chemical Vapor ◽  
Deposition Process ◽  
Solid State Reactions ◽  
Spatial Distributions ◽  
Diffusion Couples ◽  
Kinetics Studies ◽  
Ceramic Thin Films ◽  
Initial Stage

Solid-state reactions have traditionally been studied in the form of diffusion couples. This ‘bulk’ approach has been modified, for the specific case of the reaction between NiO and Al2O3, by growing NiAl2O4 (spinel) from electron-transparent Al2O3 TEM foils which had been exposed to NiO vapor at 1415°C. This latter ‘thin-film’ approach has been used to characterize the initial stage of spinel formation and to produce clean phase boundaries since further TEM preparation is not required after the reaction is completed. The present study demonstrates that chemical-vapor deposition (CVD) can be used to deposit NiO particles, with controlled size and spatial distributions, onto Al2O3 TEM specimens. Chemical reactions do not occur during the deposition process, since CVD is a relatively low-temperature technique, and thus the NiO-Al2O3 interface can be characterized. Moreover, a series of annealing treatments can be performed on the same sample which allows both Ni0-NiAl2O4 and NiAl2O4-Al2O3 interfaces to be characterized and which therefore makes this technique amenable to kinetics studies of thin-film reactions.

Search mode for rapid detection of virus particles

1991 ◽  
Vol 49 ◽  
pp. 286-287
Author(s):  
O. E. Bradfute
Keyword(s):  
Electron Microscopy ◽  
Rapid Detection ◽  
Plant Virus ◽  
Low Dose ◽  
Search Mode ◽  
Virus Diseases ◽  
Virus Particles ◽  
Focus Image ◽  
Time Required ◽  
Rapid Switching

Electron microscopy is frequently used in preliminary diagnosis of plant virus diseases by surveying negatively stained preparations of crude extracts of leaf samples. A major limitation of this method is the time required to survey grids when the concentration of virus particles (VPs) is low. A rapid survey of grids for VPs is reported here; the method employs a low magnification, out-of-focus Search Mode similar to that used for low dose electron microscopy of radiation sensitive specimens. A higher magnification, in-focus Confirm Mode is used to photograph or confirm the detection of VPs. Setting up the Search Mode by obtaining an out-of-focus image of the specimen in diffraction (K. H. Downing and W. Chiu, private communications) and pre-aligning the image in Search Mode with the image in Confirm Mode facilitates rapid switching between Modes.

Observations on the growth of barium bismuth oxide thin films

1992 ◽  
Vol 50 (1) ◽  
pp. 76-77
Author(s):  
M G. Norton ◽  
E.S. Hellman ◽  
E.H. Hartford ◽  
C.B. Carter
Keyword(s):  
Substrate Temperature ◽  
Deposition Process ◽  
Nucleation Layer ◽  
Second Stage ◽  
Device Applications ◽  
High Transition ◽  
Substrate Temperatures ◽  
Oriented Material ◽  
Barium Bismuth ◽  
Superconductor Device

The bismuthates (for example, Ba1-xKxBiO3) represent a class of high transition temperature superconductors. The lack of anisotropy and the long coherence length of the bismuthates makes them technologically interesting for superconductor device applications. To obtain (100) oriented Ba1-xKxBiO3 films on (100) oriented MgO, a two-stage deposition process is utilized. In the first stage the films are nucleated at higher substrate temperatures, without the potassium. This process appears to facilitate the formation of the perovskite (100) orientation on (100) MgO. This nucleation layer is typically between 10 and 50 nm thick. In the second stage, the substrate temperature is reduced and the Ba1-xKxBiO3 is grown. Continued growth of (100) oriented material is possible at the lower substrate temperature.

Investigation of ultra-thin films of YBa2Cu3O7−δ grown on MgO

1990 ◽  
Vol 48 (4) ◽  
pp. 6-7
Author(s):  
S.K. Streiffer ◽  
C.B. Eom ◽  
J.C. Bravman ◽  
T.H. Geballet
Keyword(s):  
Thin Films ◽  
Room Temperature ◽  
Deposition Process ◽  
Nucleation And Growth ◽  
Multilayer Structures ◽  
Rf Power ◽  
Oxygen Loss ◽  
Transmission Electron ◽  
Single Target ◽  
Mtorr Argon

The study of very thin (<15 nm) YBa2Cu3O7−δ (YBCO) films is necessary both for investigating the nucleation and growth of films of this material and for achieving a better understanding of multilayer structures incorporating such thin YBCO regions. We have used transmission electron microscopy to examine ultra-thin films grown on MgO substrates by single-target, off-axis magnetron sputtering; details of the deposition process have been reported elsewhere. Briefly, polished MgO substrates were attached to a block placed at 90° to the sputtering target and heated to 650 °C. The sputtering was performed in 10 mtorr oxygen and 40 mtorr argon with an rf power of 125 watts. After deposition, the chamber was vented to 500 torr oxygen and allowed to cool to room temperature. Because of YBCO’s susceptibility to environmental degradation and oxygen loss, the technique of Xi, et al. was followed and a protective overlayer of amorphous YBCO was deposited on the just-grown films.

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