scholarly journals Damage Evolution of Granodiorite after Heating and Cooling Treatments

Minerals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 779
Author(s):  
Mohamed Gomah ◽  
Guichen Li ◽  
Salah Bader ◽  
Mohamed Elkarmoty ◽  
Mohamed Ismael

The awareness of the impact of high temperatures on rock properties is essential to the design of deep geotechnical applications. The purpose of this research is to assess the influence of heating and cooling treatments on the physical and mechanical properties of Egyptian granodiorite as a degrading factor. The samples were heated to various temperatures (200, 400, 600, and 800 °C) and then cooled at different rates, either slowly cooled in the oven and air or quickly cooled in water. The porosity, water absorption, P-wave velocity, tensile strength, failure mode, and associated microstructural alterations due to thermal effect have been studied. The study revealed that the granodiorite has a slight drop in tensile strength, up to 400 °C, for slow cooling routes and that most of the physical attributes are comparable to natural rock. Despite this, granodiorite thermal deterioration is substantially higher for quick cooling than for slow cooling. Between 400:600 °C is ‘the transitional stage’, where the physical and mechanical characteristics degraded exponentially for all cooling pathways. Independent of the cooling method, the granodiorite showed a ductile failure mode associated with reduced peak tensile strengths. Additionally, the microstructure altered from predominantly intergranular cracking to more trans-granular cracking at 600 °C. The integrity of the granodiorite structure was compromised at 800 °C, the physical parameters deteriorated, and the rock tensile strength was negligible. In this research, the temperatures of 400, 600, and 800 °C were remarked to be typical of three divergent phases of granodiorite mechanical and physical properties evolution. Furthermore, 400 °C could be considered as the threshold limit for Egyptian granodiorite physical and mechanical properties for typical thermal underground applications.

2020 ◽  
Author(s):  
Jackie E. Kendrick ◽  
Lauren N. Schaefer ◽  
Jenny Schauroth ◽  
Andrew F. Bell ◽  
Oliver D. Lamb ◽  
...  

Abstract. Volcanoes represent one of the most critical geological settings for hazard modelling due to their propensity to both unpredictably erupt and collapse, even in times of quiescence. Volcanoes are heterogeneous at multiple scales, from porosity which is variably distributed and frequently anisotropic to strata that are laterally discontinuous and commonly pierced by fractures and faults. Due to variable and, at times, intense stress and strain conditions during and post-emplacement, volcanic rocks span an exceptionally wide range of physical and mechanical properties. Understanding the constituent materials' attributes is key to improving the interpretation of hazards posed by the diverse array of volcanic complexes. Here, we examine the spectrum of physical and mechanical properties presented by a single dome-forming eruption at a dacitic volcano, Mount Unzen (Japan) by testing a number of isotropic and anisotropic lavas in tension and compression and using monitored acoustic emission (AE) analysis. The lava dome was erupted as a series of 13 lobes between 1991–1995, and its ongoing instability means much of the volcano and its surroundings remain within an exclusion zone today. During a field campaign in 2015, we selected 4 representative blocks as the focus of this study. The core samples from each block span range in porosity from 9.14 to 42.81 %, and permeability ranges from 1.54 × 10−14 to 2.67 × 10−10 m2 (from 1065 measurements). For a given porosity, sample permeability varies by > 2 orders of magnitude is lower for macroscopically anisotropic samples than isotropic samples of similar porosity. An additional 379 permeability measurements on planar block surfaces ranged from 1.90 × 10−15 to 2.58 × 10−12 m2, with a single block having higher standard deviation and coefficient of variation than a single core. Permeability under confined conditions showed that the lowest permeability samples, whose porosity largely comprises microfractures, are most sensitive to effective pressure. The permeability measurements highlight the importance of both scale and confinement conditions in the description of permeability. The uniaxial compressive strength (UCS) ranges from 13.48 to 47.80 MPa, and tensile strength (UTS) using the Brazilian disc method ranges from 1.30 to 3.70 MPa, with crack-dominated lavas being weaker than vesicle-dominated materials of equivalent porosity. UCS is lower in saturated conditions, whilst the impact of saturation on UTS is variable. UCS is between 6.8 and 17.3 times higher than UTS, with anisotropic samples forming each end member. The Young's modulus of dry samples ranges from 4.49 to 21.59 GPa and is systematically reduced in water-saturated tests. The interrelation of porosity, UCS, UTS and Young's modulus was modelled with good replication of the data. Acceleration of monitored acoustic emission (AE) rates during deformation was assessed by fitting Poisson point process models in a Bayesian framework. An exponential acceleration model closely replicated the tensile strength tests, whilst compressive tests tended to have relatively high early rates of AEs, suggesting failure forecast may be more accurate in tensile regimes, though with shorter warning times. The Gutenberg-Richter b-value has a negative correlation with connected porosity for both UCS and UTS tests which we attribute to different stress intensities caused by differing pore networks. b-value is higher for UTS than UCS, and typically decreases (positive Δb) during tests, with the exception of cataclastic samples in compression. Δb correlates positively with connected porosity in compression, and negatively in tension. Δb using a fixed sampling length may be a more useful metric for monitoring changes in activity at volcanoes than b-value with an arbitrary starting point. Using coda wave interferometry (CWI) we identify velocity reductions during mechanical testing in compression and tension, the magnitude of which is greater in more porous samples in UTS but independent of porosity in UCS, and which scales to both b-value and Δb. Yet, saturation obscures velocity changes caused by evolving material properties, which could mask damage accrual or source migration in water-rich environments such as volcanoes. The results of this study highlight that heterogeneity and anisotropy within a single system not only add uncertainty but also have a defining role in the channelling of fluid flow and localisation of strain that dictate a volcano's hazards and the geophysical indicators we use to interpret them.


2020 ◽  
Author(s):  
Li Yu ◽  
Hai-wang PENG ◽  
Yu Zhang ◽  
GuoWei Li

Abstract To study the influence of thermal shock caused by water cooling on the physical and mechanical properties of high-temperature granite, granite was subjected to an increasing number of high-temperature (300℃) water-cooling and thermal shock treatment cycles, and static mechanical experiments were carried out on the treated granite. The results support the following conclusions: (1) Thermal shock causes an increase in the number and size of the pores and cracks within the granite; thus, its volume expands, density decreases, water absorption rate increases, and P-wave velocity decreases. (2) With an increase in the number of thermal shocks, both the compressive strength and tensile strength of the granite decrease, and there is a linear relationship between the compressive strength and tensile strength. With the corresponding fitting formula, the change in the strength of the granite can be accurately predicted. (3) With an increase in the number of thermal shocks, the plasticity of the granite increases and its resistance to deformation weakens, which is manifested as a decrease in both the compressive modulus and tensile modulus of the granite. After 15 cycles of thermal shock, the compressive elastic modulus and tensile modulus of the granite decreased by 25.18% and 46.76%, respectively. (4) The m and s values of the damaged granite were calculated based on the Hoek-Brown empirical criterion, and it was found that both of these parameters decrease with the increase in the number of thermal shocks. The calculation results can provide a reference for engineering rock mass failure.Clinical trial registration


2016 ◽  
Vol 53 (3) ◽  
pp. 253-271 ◽  
Author(s):  
Hajar Yousefian ◽  
Denis Rodrigue

Nanocomposite foams based on Nylon 6 and nanocrystalline cellulose were prepared via extrusion and injection molding to study the effect of nanocrystalline cellulose concentration (0 to 5%), chemical foaming agent content (0, 1%, and 2%), and mold temperature (30℃ and 80℃) on the morphological, physical, and mechanical properties of the samples. Nanocrystalline cellulose content, especially between 1 and 3 wt%, was very effective in reducing the cell size and increasing the cell density of the foam structure. Nanocrystalline cellulose addition (0–5%) was found to increase density (4% for composites and 20% for foams), tensile strength (10% for composite and 13% for foams), tensile modulus (20% for composites and 34% for foams), and flexural modulus (37% for composites and 29% for foams), but decreased the impact strength (35–40% for composites and 20–40% for foams). Foaming agent addition (1%) was able to improve the specific tensile (10%) and flexural (12%) moduli, tensile strength (14%), elongation at break (6%), and impact strength (27%). Finally, higher mold temperature decreased skin thickness and, consequently, decreased the mechanical properties, mostly tensile strength of the foam samples (1% for composites and 18% for foams).


Geofluids ◽  
2021 ◽  
Vol 2021 ◽  
pp. 1-15
Author(s):  
Zhizhen Zhang ◽  
Yixin Niu ◽  
Xiaoji Shang ◽  
Peng Ye ◽  
Rui Zhou ◽  
...  

Both surface and underground rocks in nature often undergo repeated drying and wetting. The dry-wet cycle is a weathering effect that includes physical and chemical processes, which has varying degrees of degradation effects on the physical and mechanical properties of rocks. This paper analyzes and discusses this kind of rock degradation based on the existing literature data. First, the deterioration degree of various physical and mechanical properties (including density, P-wave velocity, porosity, static and dynamic compressive/tensile strength, and fracture toughness) is summarized as the number of dry-wet cycles increases. Secondly, the possible degradation mechanism of the dry-wet cycle is explained in terms of clay mineral swelling, solute migration, and microcrack evolution. Then, the damage constitutive model of the rock after cyclic dry-wet treatment is introduced. Finally, the issues that need to be studied in the future are put forward.


Solid Earth ◽  
2021 ◽  
Vol 12 (3) ◽  
pp. 633-664
Author(s):  
Jackie E. Kendrick ◽  
Lauren N. Schaefer ◽  
Jenny Schauroth ◽  
Andrew F. Bell ◽  
Oliver D. Lamb ◽  
...  

Abstract. Volcanoes represent one of the most critical geological settings for hazard modelling due to their propensity to both unpredictably erupt and collapse, even in times of quiescence. Volcanoes are heterogeneous at multiple scales, from porosity, which is variably distributed and frequently anisotropic, to strata, which are laterally discontinuous and commonly pierced by fractures and faults. Due to variable and, at times, intense stress and strain conditions during and following emplacement, volcanic rocks span an exceptionally wide range of physical and mechanical properties. Understanding the constituent materials' attributes is key to improving the interpretation of the hazards posed by the diverse array of volcanic complexes. Here, we examine the spectrum of physical and mechanical properties presented by a single dome-forming eruption at a dacitic volcano, Mount Unzen (Japan), by testing a number of isotropic and anisotropic lavas in tension and compression with acoustic emission (AE) monitoring. The lava dome erupted as a series of 13 lobes between 1991 and 1995, and its ongoing instability means that much of the volcano and its surroundings remain within an exclusion zone today. During a field campaign in 2015, we selected four representative blocks as the focus of this study. The core samples from each block span a range in total porosity from 9.14 % to 42.81 % and a range in permeability from 1.65×10-15 to 1.88×10-9 m2 (from 1065 measurements). For a given porosity, sample permeability varies by >2 orders of magnitude and is typically lower for macroscopically anisotropic samples than for isotropic samples of similar porosity. An additional 379 permeability measurements on planar surfaces of both an isotropic and anisotropic sample block showed consistent minimum, maximum, and average permeabilities, and comparable standard deviations to measurements on core and disc samples; this indicated a negligible impact of sample size on recorded permeability across the range of sample sizes and absolute permeabilities tested. Permeability measured under confined conditions showed that the lowest permeability samples, whose porosity largely comprises microfractures, are most sensitive to effective pressure and that anisotropy of permeability is enhanced by confinement. The permeability measurements highlight the importance of the measurement approach, scale, and confinement conditions in the description of permeability. The uniaxial compressive strength (UCS) ranges from 13.48 to 47.80 MPa, and tensile strength (UTS) using the Brazilian disc method ranges from 1.30 to 3.70 MPa, with crack-dominated lavas being weaker than vesicle-dominated materials of equivalent porosity. UCS is lower in saturated conditions, whereas the impact of saturation on UTS is variable. UCS is between 6.8 and 17.3 times higher than UTS, with anisotropic samples forming each endmember. The Young's modulus of dry samples ranges from 4.49 to 21.59 GPa and is systematically reduced in water-saturated tests. The interrelation of porosity, UCS, UTS, and Young's modulus was modelled with good replication of the data, and empirical relationships are provided. Acceleration of monitored acoustic emission (AE) rates during deformation was assessed by fitting Poisson point process models in a Bayesian framework. An exponential acceleration model closely replicated the tensile strength tests, whilst compressive tests tended to have relatively high early rates of AEs, suggesting failure forecast may be more accurate in tensile regimes, though with shorter warning times. The Gutenberg–Richter b value has a negative correlation with connected porosity for both UCS and UTS tests which we attribute to different stress intensities caused by differing pore networks. The b value is higher for UTS than UCS, and it typically decreases (positive Δb) during tests, with the exception of cataclastic samples in compression. Δb correlates positively with connected porosity in compression and correlates negatively in tension. Δb using a fixed sampling length may be a more useful metric for monitoring changes in activity at volcanoes than the b value with an arbitrary starting point. Using coda wave interferometry (CWI), we identify velocity reductions during mechanical testing in compression and tension, the magnitude of which is greater in more porous samples in UTS but independent of porosity in UCS and which scales to both b value and Δb. Yet, saturation obscures velocity changes caused by evolving material properties, which could mask damage accrual or source migration in water-rich seismogenic environments such as volcanoes. The results of this study highlight that heterogeneity and anisotropy within a single system not only add variability but also have a defining role in the channelling of fluid flow and localisation of strain that dictate a volcano's hazards and the geophysical indicators we use to interpret them.


2020 ◽  
Vol 14 (2) ◽  
pp. 6734-6742
Author(s):  
A. Syamsir ◽  
S. M. Mubin ◽  
N. M. Nor ◽  
V. Anggraini ◽  
S. Nagappan ◽  
...  

This study investigated the combine effect of 0.2 % drink cans and steel fibers with volume fractions of 0%, 0.5%, 1%, 1.5%, 2%, 2.5% and 3% to the mechanical properties and impact resistance of concrete. Hooked-end steel fiber with 30 mm and 0.75 mm length and diameter, respectively was selected for this study.  The drinks cans fiber were twisted manually in order to increase friction between fiber and concrete. The results of the experiment showed that the combination of steel fibers and drink cans fibers improved the strength performance of concrete, especially the compressive strength, flexural strength and indirect tensile strength. The results of the experiment showed that the combination of steel fibers and drink cans fibers improved the compressive strength, flexural strength and indirect tensile strength by 2.3, 7, and 2 times as compare to batch 1, respectively. Moreover, the impact resistance of fiber reinforced concrete has increase by 7 times as compared to non-fiber concretes. Moreover, the impact resistance of fiber reinforced concrete consistently gave better results as compared to non-fiber concretes. The fiber reinforced concrete turned more ductile as the dosage of fibers was increased and ductility started to decrease slightly after optimum fiber dosage was reached. It was found that concrete with combination of 2% steel and 0.2% drink cans fibers showed the highest compressive, split tensile, flexural as well as impact strength.    


Polymers ◽  
2021 ◽  
Vol 13 (14) ◽  
pp. 2359
Author(s):  
Harmaen Ahmad Saffian ◽  
Masayuki Yamaguchi ◽  
Hidayah Ariffin ◽  
Khalina Abdan ◽  
Nur Kartinee Kassim ◽  
...  

In this study, Kraft lignin was esterified with phthalic anhydride and was served as reinforcing filler for poly(butylene succinate) (PBS). Composites with different ratios of PBS, lignin (L), modified lignin (ML) and kenaf core fibers (KCF) were fabricated using a compounding method. The fabricated PBS composites and its counterparts were tested for thermal, physical and mechanical properties. Weight percent gain of 4.5% after lignin modification and the FTIR spectra has confirmed the occurrence of an esterification reaction. Better thermo-mechanical properties were observed in the PBS composites reinforced with modified lignin and KCF, as higher storage modulus and loss modulus were recorded using dynamic mechanical analysis. The density of the composites fabricated ranged from 1.26 to 1.43 g/cm3. Water absorption of the composites with the addition of modified lignin is higher than that of composites with unmodified lignin. Pure PBS exhibited the highest tensile strength of 18.62 MPa. Incorporation of lignin and KCF into PBS resulted in different extents of reduction in tensile strength (15.78 to 18.60 MPa). However, PBS composite reinforced with modified lignin exhibited better tensile and flexural strength compared to its unmodified lignin counterpart. PBS composite reinforced with 30 wt% ML and 20 wt% KCF had the highest Izod impact, as fibers could diverge the cracking propagation of the matrix. The thermal conductivity value of the composites ranged from 0.0903 to 0.0983 W/mK, showing great potential as a heat insulator.


2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Longxiao Chen ◽  
Kesheng Li ◽  
Guilei Song ◽  
Deng Zhang ◽  
Chuanxiao Liu

AbstractRock deterioration under freeze–thaw cycles is a concern for in-service tunnel in cold regions. Previous studies focused on the change of rock mechanical properties under unidirectional stress, but the natural rock mass is under three dimensional stresses. This paper investigates influences of the number of freeze–thaw cycle on sandstone under low confining pressure. Twelve sandstone samples were tested subjected to triaxial compression. Additionally, the damage characteristics of sandstone internal microstructure were obtained by using acoustic emission (AE) and mercury intrusion porosimetry. Results indicated that the mechanical properties of sandstone were significantly reduced by freeze–thaw effect. Sandstone’ peak strength and elastic modulus were 7.28–37.96% and 6.38–40.87% less than for the control, respectively. The proportion of super-large pore and large pore in sandstone increased by 19.53–81.19%. We attributed the reduced sandstone’ mechanical properties to the degenerated sandstone microstructure, which, in turn, was associated with increased sandstone macropores. The macroscopic failure pattern of sandstone changed from splitting failure to shear failure with an increasing of freeze–thaw cycles. Moreover, the activity of AE signal increased at each stage, and the cumulative ringing count also showed upward trend with the increase of freeze–thaw number.


2012 ◽  
Vol 3 (1) ◽  
pp. 13-26
Author(s):  
Myrtha Karina ◽  
Lucia Indrarti ◽  
Rike Yudianti ◽  
Indriyati

The effect of castor oil on the physical and mechanical properties of bacterial cellulose is described. Bacterial cellulose (BC) was impregnated with 0.5–2% (w/v) castor oil (CO) in acetone–water, providing BCCO films. Scanning electron micrographs revealed that the castor oil penetrated the pores of the bacterial cellulose, resulting in a smoother morphology and enhanced hydrophilicity. Castor oil caused a slight change in crystallinity indices and resulted in reduced tensile strength and Young's modulus but increased elongation at break. A significant reduction in tensile strength and Young's modulus was achieved in BCCO films with 2% castor oil, and there was an improvement in elongation at break and hydrophilicity. Impregnation with castor oil, a biodegradable and safe plasticiser, resulted in less rigid and more ductile composites.


Materials ◽  
2020 ◽  
Vol 13 (12) ◽  
pp. 2865
Author(s):  
Md Jihad Miah ◽  
Md. Munir Hossain Patoary ◽  
Suvash Chandra Paul ◽  
Adewumi John Babafemi ◽  
Biranchi Panda

This paper investigates the possibility of utilizing steel slags produced in the steelmaking industry as an alternative to burnt clay brick aggregate (BA) in concrete. Within this context, physical, mechanical (i.e., compressive and splitting tensile strength), length change, and durability (porosity) tests were conducted on concrete made with nine different percentage replacements (0%, 10%, 20%, 30%, 40%, 50%, 60%, 80%, and 100% by volume of BA) of BA by induction of furnace steel slag aggregate (SSA). In addition, the chemical composition of aggregate through X-ray fluorescence (XRF) analysis and microstructural analysis through scanning electron microscopy (SEM) of aggregates and concrete were performed. The experimental results show that the physical and mechanical properties of concrete made with SSA were significantly higher than that of concrete made with BA. The compressive and tensile strength increased by 73% when SSA fully replaced BA. The expansion of concrete made with SSA was a bit higher than the concrete made with BA. Furthermore, a significant lower porosity was observed for concrete made with SSA than BA, which decreased by 40% for 100% SSA concrete than 100% BA concrete. The relation between compressive and tensile strength with the porosity of concrete mixes are in agreement with the relationships presented in the literature. This study demonstrates that SSA can be used as a full replacement of BA, which is economical, conserves the natural aggregate, and is sustainable building material since burning brick produces a lot of CO2.


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