Optimization of an improved aqueous method for the production of high quality white sesame oil and de-oiled meal

2020 ◽  
Vol 71 (2) ◽  
pp. 349
Author(s):  
M. Lv ◽  
W. Wu

Research into the production of white sesame oil by aqueous extraction has been promoted because of concerns about the environment, health, and cost. The advanced aqueous method using a 1.95:10 liquid-to-raw material ratio, which was finally developed in this study, recovered 96.06% white sesame oil and produced de-oiled meal with high quality (3.98% residual oil content). The acid value and peroxide value of the oil produced were quite low at 0.19 mg KOH/kg and < 3.25 mmol/kg, respectively, which were better than the values required by the Chinese national standard for first class edible sesame oils and oils produced by hexane extraction. No wastewater was discharged during the extraction of white sesame oils by an aqueous salt solution. The protein rich de-oiled meal may be a good material for making protein isolate with high purity (e.g. > 90%). It can also be a nutritious ingredient or raw material for producing many food products.

2019 ◽  
Vol 70 (3) ◽  
pp. 313 ◽  
Author(s):  
J. Tu ◽  
W. Wu

Concern for the environment, safety and costs has promoted the development of the method for extracting soybean oil by an aqueous process. An advanced aqueous extraction of soybean oil assisted by adding free oil was established in this study, which recovered 81% of the oil from soybeans with 20.73% crude oil content and produced a de-oiled residue with 4.7% residual oil. The acid or peroxide value of the recovered oil met the Chinese national standard for first class refined oil, which was lower than that produced by solvent extraction or high temperature pressing. No wastewater was produced during the aqueous extraction of oil. The removal of the oil by the addition of oil and a small amount of water generated a residue (solids) containing all the protein, which represents 2/3 of the revenue in the soybean process. The protein-rich residue can be further processed to produce a protein isolate with high purity (e.g. > 90%) by using a higher amount of water. It can also be used as a nutritious ingredient or raw material for the production of many food products, among other applications.


2014 ◽  
Vol 1015 ◽  
pp. 272-275
Author(s):  
Xiao Qiong Ren ◽  
Ya Nan Wu ◽  
Ying Li ◽  
Mo Han Lin ◽  
Feng Qing Zhao

Gypsum retarder is an important additive of building materials. Commercial gypsum retarders are mainly composed of four types: organic acids, phosphates, protein and composite retarder. Although the effects of organic acids and phosphates have better retarding performances, there is still obvious a shortcoming that the mechanical strength reduces largely with time going by. Protein based retarders prolong the setting time of hemihydrates with less strength loss and higher costs. The gypsum retarder from waste mycelium, a protein-rich raw material, solved the problem of the disposal of waste mycelium from anti-biotic plants, while producing high-quality retarder for gypsum, shows potential for future.


Author(s):  
Shuting Fu ◽  
Wenbiao Wu

The extraction of oil by a new aqueous method has been promoted because it is environmentally friendly, safe and economical of cost. A new aqueous method using 1.4:10.0 water-to-pecan kernel slurry ratio was developed, which recovered 97.73% of oils from the kernel containing 70.47% crude oil content. The method had a higher oil recovery as compared to enzyme-assisted extraction or solvent extraction or cold pressing in terms of producing oil for safe consumption. The method recovered oils with 0.47 mg KOH/g acid value and 0.34 mmol/kg peroxide value which were identical to that obtained by enzyme-assisted aqueous method and lower than that obtained by solvent extraction. The de-oiled pecan meal obtained by the new aqueous method only contained 5.14% residual oils, which was edible since no harmful chemical was added during oil extraction. No waste water was produced during the aqueous extraction of oils.


Author(s):  
I. A. Ilina ◽  
I. A. Machneva ◽  
E. S. Bakun

  The article is devoted to the study of the chemical composition, physical and thermal-pfysical characteristics of damp apple pomaces and the identifying patterns of influence of drying temperature the functional composition and gel-forming ability of pectin. The research is aimed at obtaining initial data for the subsequent calculation of the main technological, hydro-mechanical, thermal, structural and economic characteristics of devices for drying the plant raw materials, ensuring the environmental safety and high quality of pectin-containing raw materials, the reducing heat and energy costs. As a result of the study of the thermal characteristics of apple pomaces, the critical points (temperature conductivity – 16.5 x 10-8 m2/s, thermal conductivity – 0.28 W/m K, heat capacity – 1627 j/(kg K)) at a humidity of 56 % are determined, which characterizing the transition from the extraction of weakly bound moisture to the extraction of moisture with strong bonds (colloidal, adsorption). It was found that the pomaces obtained from apples of late ripening have a higher content of solids (21-23 %), soluble pectin and protopectin (2.5-4.5 %). Dried pomaces obtained from apple varieties of late ripening contain up to 25 % pectin, which allow us to recommend them as a source of raw materials for the production of pectin. The optimum modes of preliminary washing of raw materials are offered, allowing to the remove the ballast substances as much as possible. It is established that when the drying temperature increases, the destructive processes are catalyzed: the strength of the pectin jelly and the uronide component and the degree of pectin esterification are reduced. The optimum drying temperature of damp apple pomaces is 80 0C, at which the quality of pectin extracted from the dried raw materials is maintained as much as possible. It is shown that the most effective for the pectin production is a fraction with a particle size of 3-5 mm, which allow us to extract up to 71 % of pectin from raw materials.


Foods ◽  
2021 ◽  
Vol 10 (3) ◽  
pp. 644
Author(s):  
Do-Yeong Kim ◽  
Boram Kim ◽  
Han-Seung Shin

The effect of cellulosic aerogel treatments used for adsorption of four polycyclic aromatic hydrocarbons (PAHs)—benzo[a]anthracene, chrysene, benzo[b]fluoranthene, and benzo[a]pyrene [BaP])—generated during the manufacture of sesame oil was evaluated. In this study, eulalia (Miscanthus sinensis var. purpurascens)-based cellulosic aerogel (adsorbent) was prepared and used high performance liquid chromatography with fluorescence detection for determination of PAHs in sesame oil. In addition, changes in the sesame oil quality parameters (acid value, peroxide value, color, and fatty acid composition) following cellulosic aerogel treatment were also evaluated. The four PAHs and their total levels decreased in sesame oil samples roasted under different conditions (p < 0.05) following treatment with cellulosic aerogel. In particular, highly carcinogenic BaP was not detected after treatment with cellulosic aerogel. Moreover, there were no noticeable quality changes in the quality parameters between treated and control samples. It was concluded that eulalia-based cellulosic aerogel proved suitable for the reduction of PAHs from sesame oil and can be used as an eco-friendly adsorbent.


Author(s):  
Zhou J ◽  
◽  
Dong Y ◽  
Ma Y ◽  
Zhang T ◽  
...  

Graphene Quantum Dots (GQDs) have been prepared by oxidationhydrothermal reaction, using ball-milling graphite as the starting materials. The prepared GQDs are endowed with excellent luminescence properties, with the optimum emission of 320nm. Blue photoluminescent emitted from the GQDs under ultraviolet light. The GQDs are ~3nm in width and 0.5~2 nm in thickness, revealed by high-resolution transmission electron microscopy and atomic force microscopy. In addition, Fourier transform infrared spectrum evidences the existence of carbonyl and hydroxyl groups, meaning GQDs can be dispersed in water easily and used in cellar imaging, and blue area inside L929 cells were clearly observed under the fluorescence microscope. Both low price of raw material and simple prepared method contribute to the high quality GQDs widespread application in future.


Catalysts ◽  
2018 ◽  
Vol 8 (11) ◽  
pp. 527 ◽  
Author(s):  
Gaojian Ma ◽  
Lingmei Dai ◽  
Dehua Liu ◽  
Wei Du

Acidic oil, which is easily obtained and with lower cost, is a potential raw material for biodiesel production. Apart from containing large quantity of FFAs (free fatty acids), acidic oil usually contains some amount of inorganic acid, glycerides and some other complex components, leading to complicated effect on lipase’s catalytic performance. Exploring the efficient process of converting acidic oil for biodiesel production is of great significance to promote the use of acidic oil. A two-step conversion process for acidic soybean oil was proposed in this paper, where sulfuric acid-mediated hydrolysis was adopted first, then the hydrolyzed free fatty acid, collected from the upper oil layer was further subject to the second-step esterification catalyzed by immobilized lipase Novozym435. Through this novel process, the negative effect caused by harmful impurities and by-product glycerol on lipase was eliminated. A fatty acid methyl ester (FAME) yield of 95% could be obtained with the acid value decreased to 4 mgKOH/g from 188 mgKOH/g. There was no obvious loss in lipase’s activity and a FAME yield of 90% could be maintained with the lipase being repeatedly used for 10 batches. This process was found to have a good applicability to different acidic oils, indicating it has great prospect for converting low quality oil sources for biodiesel preparation.


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