Tailoring Mechanical Properties of Extruded Ti-6Al-4V Alloy from the Blended Elemental Route via Microstructure Control

2018 ◽  
Vol 884 ◽  
pp. 36-42
Author(s):  
Carlos Romero ◽  
Fei Yang ◽  
Leandro Bolzoni
Keyword(s):  
Mechanical Properties ◽  
Solution Treatment ◽  
Lamellar Microstructure ◽  
Annealing Treatment ◽  
X Ray Diffraction ◽  
Primary Alpha ◽  
Β Phase ◽  
Different Temperatures ◽  
The One ◽  
Strength And Ductility

Vacuum-sintered billets of Ti-6Al-4V alloy from powder blend were extruded at two different temperatures: 1150 °C and 950 °C. The extruded material at 1150 °C was subjected to various heat treatments to obtain different microstructures: annealing in the β phase, β solution treatment and aging and α+β solution treatment and aging. The materials processed were characterised using scanning electron microscopy, X-ray diffraction and the mechanical properties were measured by tensile test. The microstructure of both extrusions are fairly similar, consisting of lamellar colonies, and the mechanical properties are also comparable, with yield strengths of about 1000 MPa, ultimate tensile strength of about 1100 MPa and elongation at fracture of 8-9%. The β annealing treatment, through coarsening the lamellar microstructure, reduces the strength of the alloy while keeping a high ductility. Both solution treatments and aging, which produces aged martensite and aged martensite and primary alpha, respectively, increases the strength and reduces the ductility. There is a trade-off between ductility and strength when it comes to tailoring the microstructure, and the as-extruded Ti-6Al-4V condition is the one with the best balance between strength and ductility.

Effect of Alloying and Thermal Processing on Mechanical Properties of TiAl Alloys

2016 ◽  
Vol 258 ◽  
pp. 501-505
Author(s):  
Alice Chlupová ◽  
Milan Heczko ◽  
Karel Obrtlík ◽  
Přemysl Beran ◽  
Tomáš Kruml
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Thermal Processing ◽  
Lamellar Microstructure ◽  
High Strength ◽  
Fatigue Behaviour ◽  
Tial Alloys ◽  
Working Temperature ◽  
Β Phase ◽  
Strength And Ductility

Two γ-based TiAl alloys with 7 at.% of Nb, alloyed with 2 at.% Mo and 0.5 at.% C, were studied. A heat treatment leading to very fine lamellar microstructure was applied on both alloys. Microstructure after the heat treatment was described and mechanical properties including fatigue behaviour were measured. The as-received material alloyed with C possesses high strength and very limited ductility, especially at RT. After application of selected heat treatment it becomes even more brittle; therefore, this process could be considered as not appropriate for this alloy. On the contrary, in the case of Mo alloyed material, both strength and ductility are improved by the heat treatment at RT and usual working temperature (~750 °C). Presence of the β phase is responsible for this effect. The selected heat treatment thus can be an alternative for this alloy to other thermomechanical treatments as high temperature forging.

CHARACTERIZATION OF HYDROXYAPATITE/TI6AL4V COMPOSITE POWDER UNDER VARIOUS SINTERING TEMPERATURE

2015 ◽  
Vol 75 (7) ◽  
Author(s):  
Amir Arifin ◽  
Abu Bakar Sulong ◽  
Norhamidi Muhamad ◽  
Junaidi Syarif
Keyword(s):  
Mechanical Properties ◽  
Composite Powder ◽  
Sintering Temperature ◽  
Physical And Mechanical Properties ◽  
Xrd Analysis ◽  
X Ray Diffraction ◽  
Different Temperatures ◽  
Two Phases ◽  
Work Interaction

Hydroxyapatite (HA) has been widely used in biomedical applications due to its excellent biocompatibility. However, Hydroxyapatite possesses poor mechanical properties and only tolerate limited loads for implants. Titanium is well-known materials applied in implant that has advantage in mechanical properties but poor in biocompatibility. The combination of the Titanium alloy and HA is expected to produce bio-implants with good in term of mechanical properties and biocompatabilty. In this work, interaction and mechanical properties of HA/Ti6Al4V was analyzed. The physical and mechanical properties of HA/Ti6Al4V composite powder obtained from compaction (powder metallurgy) of 60 wt.% Ti6Al4V and 40 wt.% HA and sintering at different temperatures in air were investigated in this study. Interactions of the mixed powders were investigated using X-ray diffraction. The hardness and density of the HA/Ti6Al4V composites were also measured. Based on the results of XRD analysis, the oxidation of Ti began at 700 °C. At 1000 °C, two phases were formed (i.e., TiO2 and CaTiO3). The results showed that the hardness HA/Ti6Al4V composites increased by 221.6% with increasing sintering temperature from 700oC to 1000oC. In contrast, the density of the composites decreased by 1.9% with increasing sintering temperature. 

Influence of Heat Treatment on Microstrudture and Mechanical Properties of AZ31B Magnesium Alloy Prepared by Solid-State Recycling

2012 ◽  
Vol 271-272 ◽  
pp. 17-20
Author(s):  
Shu Yan Wu ◽  
Ze Sheng Ji ◽  
Chun Ying Tian ◽  
Ming Zhong Wu
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Solid State ◽  
Magnesium Alloy ◽  
Static Recrystallization ◽  
Annealing Treatment ◽  
Az31b Magnesium Alloy ◽  
Heat Treated ◽  
Elongation To Failure ◽  
Strength And Ductility

This work is to study the influence of heat treatment on microstrudture and mechanical properties of AZ31B magnesium alloy prepared by solid -state recycling. AZ31B magnesium alloy chips were recycled by hot extruding. Three different heat treatments were conducted for recycled alloy. Mechanical properties and microstructure of the recycled specimen and heat treated specimen were investigated. 300°C×2h annealing specimen exhibits finer grain due to static recrystallization, and microstructure of 400°C×2h annealing specimen becomes more coarse. 300°C×2h annealing treatment improves obviously strength and ductility of recycled alloy. Ultimate tensile strength of alloy decreases and elongation to failure increases after 400°C×2h annealing. Grain size, dislocation density and bonding of chips have an effect on the elongation of recycled materials. 190°C×8h ageing has no influence on microstructure and mechanical properties of recycled alloy.

Effects of Cooling Rate and Sn Addition on the Microstructure of Ti-Nb-Sn Alloys

2011 ◽  
Vol 172-174 ◽  
pp. 190-195 ◽  
Author(s):  
Giorgia T. Aleixo ◽  
Eder S.N. Lopes ◽  
Rodrigo Contieri ◽  
Alessandra Cremasco ◽  
Conrado Ramos Moreira Afonso ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Cooling Rate ◽  
Melting Furnace ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Β Phase ◽  
Arc Melting ◽  
Ti Alloys ◽  
Ω Phase

Ti-based alloys present unique properties and hence, are employed in several industrial segments. Among Ti alloys, β type alloys form one of the most versatile classes of materials in relation to processing, microstructure and mechanical properties. It is well known that heat treatment of Ti alloys plays an important role in determining their microstructure and mechanical behavior. The aim of this work is to analyze microstructure and phases formed during cooling of β Ti-Nb-Sn alloy through different cooling rates. Initially, samples of Ti-Nb-Sn system were prepared through arc melting furnace. After, they were subjected to continuous cooling experiments to evaluate conditions for obtaining metastable phases. Microstructure analysis, differential scanning calorimetry and X-ray diffraction were performed in order to evaluate phase transformations. Depending on the cooling rate and composition, α” martensite, ω phase and β phase were obtained. Elastic modulus has been found to decrease as the amount of Sn was increased.

scholarly journals Influence of Temperature on Mechanical Properties of P(BAMO-r-THF) Elastomer

Polymers ◽  
2020 ◽  
Vol 12 (11) ◽  
pp. 2507
Author(s):  
Jinxian Zhai ◽  
Hanpeng Zhao ◽  
Xiaoyan Guo ◽  
Xiaodong Li ◽  
Tinglu Song
Keyword(s):  
Mechanical Properties ◽  
X Ray Diffraction ◽  
Polymeric Chains ◽  
Different Temperatures ◽  
Influence Of Temperature On ◽  
Strain Induced Crystallization ◽  
Thermal Histories ◽  
Static Conditions ◽  
The Relationship ◽  
Induced Crystallization

The relationship between temperature and the mechanical properties of an end cross-linked equal molar random copolyether elastomer of 3,3-bis(azidomethyl)oxetane and tetrahydrofuran (P(BAMO-r-THF)) was investigated. During this investigation, the performances of two P(BAMO-r-THF) elastomers with different thermal histories were compared at different temperatures. The elastomer as prepared at 20 °C (denoted as S0) exhibited semi-crystallization morphology. Wide angle X-ray diffraction analysis indicated that the crystal grains within elastomer S0 result from the crystallization of BAMO micro-blocks embedded in P(BAMO-r-THF) polymeric chains, and the crystallinity is temperature irreversible under static conditions. After undergoing a heating-cooling cycle, this elastomer became an amorphous elastomer (denoted as S1). Regarding mechanical properties, at 20 °C, break strains and stresses of 315 ± 22% and 0.46 ± 0.01 MPa were obtained for elastomer S0; corresponding values of 294 ± 6% and 0.32 ± 0.02 MPa were obtained for elastomer S1. At −40 °C, these strains and stresses simultaneously increased to 1085 ± 21% and 8.90 ± 0.72 MPa (S0) and 1181 ± 25% and 10.23 ± 0.44 MPa (S1), respectively, owing to the strain-induced crystallization of BAMO micro-blocks within the P(BAMO-r-THF) polymeric chains.

scholarly journals Microstructure Evolution and Mechanical Properties of AZ80 Mg Alloy during Annular Channel Angular Extrusion Process and Heat Treatment

Materials ◽  
2019 ◽  
Vol 12 (24) ◽  
pp. 4223 ◽  
Author(s):  
Xi Zhao ◽  
Shuchang Li ◽  
Fafa Yan ◽  
Zhimin Zhang ◽  
Yaojin Wu
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Microstructure Evolution ◽  
Solution Treatment ◽  
Aging Treatment ◽  
Annular Channel ◽  
Mg Alloy ◽  
Strengthening Effect ◽  
Β Phase ◽  
Angular Extrusion

Microstructure evolution and mechanical properties of AZ80 Mg alloy during annular channel angular extrusion (350 °C) and heat treatment with varying parameters were investigated, respectively. The results showed that dynamic recrystallization of Mg grains was developed and the dendritic eutectic β-Mg17Al12 phases formed during the solidification were broken into small β-phase particles after hot extrusion. Moreover, a weak texture with two dominant peaks formed owing to the significant grain refinement and the enhanced activation of pyramidal <c + a> slip at relative high temperature. The tension tests showed that both the yield strength and ultimate tensile strength of the extruded alloy were dramatically improved owing to the joint strengthening effect of fine grain and β-phase particles as compared with the homogenized sample. The solution treatment achieved the good plasticity of the alloy resulting from the dissolution of β-phases and the development of more equiaxed grains, while the direct-aging process led to poor alloy elongation as a result of residual eutectic β-phases. After solution and aging treatment, simultaneous bonding strength and plasticity of the alloy were achieved, as a consequence of dissolution of coarse eutectic β-phases and heterogeneous precipitation of a large quantity of newly formed β-phases with both the morphologies of continuous and discontinuous precipitates.

Microstructure, Texture and Mechanical Properties of Al Alloy A380 Prepared by Directional Solidification Method

2019 ◽  
Vol 287 ◽  
pp. 18-23
Author(s):  
Hemant Borkar ◽  
Salem Seifeddine ◽  
Anders E.W. Jarfors
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Directional Solidification ◽  
Solidification Rate ◽  
Al Alloy ◽  
Secondary Dendrite Arm Spacing ◽  
Β Phase ◽  
Cu Alloy ◽  
Eutectic Si ◽  
The One

The mechanical properties of Al-Si alloys are affected by several microstructural features such as secondary dendrite arm spacing (SDAS), size and shape of eutectic Si-particles, presence of intermetallics as well as by porosity. In the current study, Al-Si-Cu alloy A380 was prepared by a unique directional solidification method to produce samples with two different SDAS of 9 μm and 27 μm. The lower solidification rate resulted in larger SDAS, larger grain size, larger eutectic Si and larger intermetallics including Fe-rich β phase. The microstructure with higher solidification rate was found to be finer and more homogeneous with smaller eutectic Si and intermetallics. The specimen with larger SDAS exhibited stronger texture than the one with smaller SDAS. The specimen with smaller SDAS showed improved mechanical properties including YS, UTS and ductility.

Effect of AlN on Microstructure and Mechanical Properties of Mg-Al-Zn Alloy

2011 ◽  
Vol 704-705 ◽  
pp. 1095-1099
Author(s):  
Peng Liu ◽  
Hao Ran Geng ◽  
Zhen Qing Wang ◽  
Jian Rong Zhu ◽  
Fu Sen Pan ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Tensile Strength ◽  
Tensile Testing ◽  
Cast Alloy ◽  
X Ray Diffraction ◽  
X Ray ◽  
Β Phase ◽  
Microstructure And Mechanical Properties ◽  
Zn Alloy

Effects of AlN addition on the microstructure and mechanical properties of as-cast Mg-Al-Zn magnesium alloy were investigated using optical microscopy (OM), scanning electron microscopy (SEM), X-ray diffraction (XRD) and tensile testing. Five different samples were made with different amounts of AlN(0wt%, 0.12wt%, 0.30wt%, 0.48wt%, 0. 60wt%). The results show that the phases of as-cast alloy are composed of α-Mg,β-Mg17Al12. The addition of AlN suppressed the precipitation of the β-phase. And, with the increase of AlN content, the microstructure of β-phase was changed from the reticulum to fine grains. When AlN content was up to 0.48wt% in the alloy, the β-phase became most uniform distribution. After adding 0.3wt% AlN to Al-Mg-Zn alloy, the average alloy grain size reduced from 102μm to 35μm ,the tensile strength of alloy was the highest. The average tensile strength increased from 139MPa to 169.91MPa, the hardness increased from 77.7HB to 98.4HB, but the elongation changes indistinctively. However, when more amount of AlN was added, the average alloy grain size did not reduce sequentially and increased to 50μm by adding 0.6wt% AlN and the β-phase became a little more. Keywords: Al-Mg-Zn alloy; AlN; β-Mg17Al12; Tensile strength

Effect of Forging Temperature on Microstructure and Tensile Properties in Fe3Al-Based Alloy

1994 ◽  
Vol 364 ◽  
Author(s):  
Y. Yang ◽  
W. Yan ◽  
J. N. Liu ◽  
S. Hanada
Keyword(s):  
Plastic Deformation ◽  
Low Temperature ◽  
Yield Strength ◽  
Grain Boundaries ◽  
Tensile Properties ◽  
Room Temperature ◽  
Annealing Treatment ◽  
Different Temperatures ◽  
Local Plastic Deformation ◽  
Strength And Ductility

AbstractForging processes at two different temperatures are performed to examine the relation between the microstructure and room temperature tensile properties in a Ce doped Fe3Al-based alloy. Results show that the microstructure and the ductility are sensitive to the forging temperature before annealing treatment. Higher yield strength and ductility can be obtained through forging at a relatively low temperature of 750°C followed by annealing at 800°C and 500°C. It is suggested that the formation of non-equilibrium grain boundaries and banded subgrains within carbide-free areas along grain boundaries enhances the local plastic deformation and results in the improvement of ductility. During the initial deformation at room temperature <111> slip is predominant for both microstructures.

Influence of Severe Plastic Deformation and Ageing on the Microstructure and Mechanical Properties of β-Alloy Ti-6.8Mo-4.5Fe-1.5Al

2010 ◽  
Vol 667-669 ◽  
pp. 731-736 ◽  
Author(s):  
Irina P. Semenova ◽  
Alexander Medvedev
Keyword(s):  
Mechanical Properties ◽  
Room Temperature ◽  
Solution Treatment ◽  
Secondary Phase ◽  
Initial Structure ◽  
Ecap Processing ◽  
Strength Enhancement ◽  
Angular Pressing ◽  
Solid Solution Treatment ◽  
Strength And Ductility

This work presents the possibility of strength enhancement in the -alloy Ti-6.8Mo-4.5Fe-1.5Al via equal channel angular pressing at room temperature without precipitation of a secondary -phase. Influence of the initial structure of the alloy and ageing temperature on the density of precipitations and dimensions of the secondary -phase is revealed. It has been stated that combination of the solid solution treatment with the subsequent ECAP processing and final ageing is an effective way to achieve superior strength and ductility.

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