Microstructures of AZ61 Magnesium Alloy Solidified via Ultrasonic Vibration Treatment

2013 ◽  
Vol 750-752 ◽  
pp. 691-695 ◽  
Author(s):  
Jun Ping Yao ◽  
Zhong Sun ◽  
Wen Yuan Long ◽  
Lei Zhang
Keyword(s):  
Grain Size ◽  
Magnesium Alloy ◽  
Cross Section ◽  
Ultrasonic Vibration ◽  
Entire Cross Section ◽  
Microstructural Refinement ◽  
Β Phase ◽  
Az61 Magnesium Alloy ◽  
Average Grain Size ◽  
Dendritic Shape

The effects of ultrasonic vibration (USV) on the solidified microstructure of AZ61 magnesium alloy were investigated. The experimental results show that the remarkable microstructural refinement is achieved when the USV was applied to the solidification of the AZ61 alloy. The average grain size is decreased from 263 μm without ultrasonic treatment to 98 μm with USV treatment. The microstructure evolution reveals that the primary α-Mg generates and grows in globular shape with USV, contrast with the dendritic shape without USV. The USV causes melt convection during solidification, which makes the temperature of the whole melt homogenized, and produces an undercooling zone in front of the liquid/solid interface, which makes the nucleation rate increased and big dendrites prohibited. In addition, the β-phase in the entire cross-section of the billet is significantly refined and also changed from continuous to discontinuous morphology. Spherical β-phase is formed during the solidification of billet treated with USV.

scholarly journals Experimental and Numerical Investigation of the ECAP Processed Copper: Microstructural Evolution, Crystallographic Texture and Hardness Homogeneity

Metals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 607
Author(s):  
A. I. Alateyah ◽  
Mohamed M. Z. Ahmed ◽  
Yasser Zedan ◽  
H. Abd El-Hafez ◽  
Majed O. Alawad ◽  
...  
Keyword(s):  
Grain Size ◽  
Equal Channel Angular Pressing ◽  
Cross Section ◽  
Room Temperature ◽  
Pure Copper ◽  
High Density ◽  
Ecap Processing ◽  
Heterogeneous Distribution ◽  
Angular Pressing ◽  
Average Grain Size

The current study presents a detailed investigation for the equal channel angular pressing of pure copper through two regimes. The first was equal channel angular pressing (ECAP) processing at room temperature and the second was ECAP processing at 200 °C for up to 4-passes of route Bc. The grain structure and texture was investigated using electron back scattering diffraction (EBSD) across the whole sample cross-section and also the hardness and the tensile properties. The microstructure obtained after 1-pass at room temperature revealed finer equiaxed grains of about 3.89 µm down to submicrons with a high density of twin compared to the starting material. Additionally, a notable increase in the low angle grain boundaries (LAGBs) density was observed. This microstructure was found to be homogenous through the sample cross section. Further straining up to 2-passes showed a significant reduction of the average grain size to 2.97 µm with observable heterogeneous distribution of grains size. On the other hand, increasing the strain up to 4-passes enhanced the homogeneity of grain size distribution. The texture after 4-passes resembled the simple shear texture with about 7 times random. Conducting the ECAP processing at 200 °C resulted in a severely deformed microstructure with the highest fraction of submicron grains and high density of substructures was also observed. ECAP processing through 4-passes at room temperature experienced a significant increase in both hardness and tensile strength up to 180% and 124%, respectively.

Microstructures and Mechanical Properties of AZ61 Mg Alloy Processed by Equal Channel Angular Pressing

2012 ◽  
Vol 468-471 ◽  
pp. 2124-2127 ◽  
Author(s):  
Shao Feng Zeng ◽  
Kai Huai Yang ◽  
Wen Zhe Chen
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Equal Channel Angular Pressing ◽  
Uniform Elongation ◽  
Considerable Decrease ◽  
Angular Pressing ◽  
Az61 Magnesium Alloy ◽  
Average Grain Size ◽  
Microstructures And Mechanical Properties ◽  
Bimodal Grain Size

Equal channel angular pressing (ECAP) was applied to a commercial AZ61 magnesium alloy for up to 8 passes at temperatures as low as 473K. Microstructures and mechanical properties of as-received and ECAP deformed samples were investigated. The microstructure was initially not uniform with a “bimodal” grain size distribution but became increasingly homogeneous with further ECAP passes and the average grain size was considerably reduced from over 26 μm to below 5 μm. The ultimate tensile strength (UTS) decreases clearly after one pass, but increases significantly up to two passes, and then continuously slowly decreases up to six passes, and again increases slightly up to eight passes. In contrast, the uniform elongation increased significantly up to 3 passes, followed by considerable decrease up to 8 passes. These observations may be attributed to combined effects of grain refinement and texture development.

Grain Refinement of Magnesium Alloy AZ31 under Torsion Extrusion with a Square-Hole Die

2010 ◽  
Vol 654-656 ◽  
pp. 711-714 ◽  
Author(s):  
Susumu Mizunuma ◽  
Takamichi Iizuka ◽  
Kazuhiro Mitsui ◽  
Hidehito Okumura ◽  
Masahide Kohzu
Keyword(s):  
Magnesium Alloy ◽  
Grain Refinement ◽  
Cross Section ◽  
Crystal Orientation ◽  
Electron Backscatter Diffraction ◽  
Entire Cross Section ◽  
Extrusion Axis ◽  
Alloy Az31 ◽  
Magnesium Alloy Az31 ◽  
Square Hole

Grain refinement and crystal orientation of magnesium alloy AZ31 under torsion extrusion with a square-hole die are investigated. The optimum temperature and ratio of the die rotation speed to the extrusion speed were clarified, resulting in uniformly distributed fine grains with sizes in the range 1- m over the entire cross section of the worked specimen. The crystal orientation of the specimen was determined by electron backscatter diffraction and compared with that of a conventionally extruded specimen. In the case of torsion extrusion, a very strong <0001> texture was observed along the extrusion axis, especially in the center region of the cross section. In contrast, the <0001> direction of many grains in the conventionally extruded specimen tended to be perpendicular to the extrusion axis.

Effects of Specimen Diameter on Microstructure and Microhardness of Hot Extruded AZ31B Magnesium Alloy

2014 ◽  
Vol 1004-1005 ◽  
pp. 158-162 ◽  
Author(s):  
Xiang Ting Hong ◽  
Fu Chen ◽  
Fei Chen ◽  
Wang Yu ◽  
Bo Rong Sang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Magnesium Alloy ◽  
Size Effects ◽  
Strain Distribution ◽  
Elevated Temperatures ◽  
Az31b Magnesium Alloy ◽  
Specimen Diameter ◽  
Average Grain Size ◽  
Micro Parts

Microstructures of metal micro parts after microforming at elevated temperatures must be evaluated due to mechanical properties depend on average grain size. In this work, the effects of specimen diameter on the microstructure and microhardness of a hot-extruded AZ31B magnesium alloy were studied. Obvious size effect on microstructure and microhardness of the alloy could be observed. The size effects could be explained by strain distribution and dislocation density differences between the two kinds of specimens.

Microstructure Prediction by Finite Element Analysis during Hot Rolling of Magnesium Alloy Sheets

2015 ◽  
Vol 661 ◽  
pp. 105-112
Author(s):  
Yeong Maw Hwang ◽  
Tso Lun Yeh
Keyword(s):  
Grain Size ◽  
Magnesium Alloy ◽  
Optimal Conditions ◽  
Compression Tests ◽  
Element Analysis ◽  
Grain Sizes ◽  
Average Grain Size ◽  
Microstructure Prediction ◽  
Alloy Microstructure ◽  
The Relationship

Material’s plastic deformation by hot forming processes can be used to make the materials generate dynamic recrystallization (DRX) and fine grains and accordingly products with more excellent mechanical properties, such as higher strength and larger elongation can be obtained. In this study, compression tests and water quenching are conducted to obtain the flow stress of the materials and the grain size after DRX. Through the regression analysis, prediction equations for the magnesium alloy microstructure were established. Simulations with different rolling parameters are conducted to find out the relationship between the DRX fractions or grain sizes of the rolled products and the rolling parameters. The simulation results show that rolling temperature of 400°C and thickness reduction of 50% are the optimal conditions. An average grain size of 0.204μm-0.206μm in the microstructure is obtained and the strength and formability of ZK60 magnesium alloys can be improved.

Effect of CO2 Laser Surface Melting on the Microstructure of AZ91D Magnesium Alloy

2011 ◽  
Vol 464 ◽  
pp. 461-464
Author(s):  
Ju Fang Chen ◽  
Xing Cheng Li ◽  
Jiang Tao Wang ◽  
Wei Ning Lei
Keyword(s):  
Grain Size ◽  
Magnesium Alloy ◽  
Continuous Wave ◽  
Surface Melting ◽  
Laser Surface ◽  
Laser Surface Melting ◽  
Micro Hardness ◽  
Az91d Magnesium Alloy ◽  
Average Grain Size ◽  
Melted Layer

In the present study, the effect of laser surface melting (LSM) on microstructure of AZ91D magnesium alloy was investigated with a 2kW continuous wave CO2 laser. The results indicate that both the substrate and laser melted layer mainly consisted of α-Mg and β-Mg17Al12, the amount of β-phase in laser melted layer was decreased as compared to that of the substrate. The microstructure of the laser surface melted zone consists of fine dendrites with an average grain size of less than 10m, the grain size was reduced by a factor of more than 10 times as compared to that of the substrate. The micro-hardness of the melted layer was increased to 70–85HV as compared to that of the substrate (about 53HV). Because of the grain refinement, the enhancement of the hard phase β-Mg17Al12, and the solid solution hardening of alloy elements, the micro-hardness and strength of the laser melted layer was increased significantly.

Effect of Grain Size on Microstructure and Aging Behavior in AM60 Magnesium Alloy

2011 ◽  
Vol 409 ◽  
pp. 373-378
Author(s):  
H. Takano ◽  
Mitsuaki Furui ◽  
Susumu Ikeno ◽  
Tomoyasu Yamaguchi ◽  
Seiji Saikawa
Keyword(s):  
Grain Size ◽  
Magnesium Alloy ◽  
Grain Boundary ◽  
Eutectic Reaction ◽  
Age Hardening ◽  
Peak Hardness ◽  
Aging Behavior ◽  
Continuous Precipitation ◽  
Hardening Behavior ◽  
Average Grain Size

Our recent studies showed that continuous and cellular precipitates are covered with the whole of crystal grain in age hardable AM60 magnesium alloy cast into permanent molds, which have the average grain size of 75-85μm. Also, continuous precipitation is generated nearby grain boundary in the same alloys cast into sand molds, which have the average grain size of 138-147μm. It’s thought that permanent mold castings have the age hardening behavior of intragranular precipitation participation type that is influenced by continuous precipitates. It’s also thought that sand mold castings have the age hardening behavior of grain boundary participation type that is influenced by cellular precipitates. In this study, AM60 magnesium alloy with larger grain size was used to detect the grain size dependence of microstructure and aging behavior. In the microstructure of as-cast condition, the larger the grain size, it was shown that the none-equilibrium crystallized β phase with eutectic reaction during the solidification between liquidus and solidus temperatures becomes large-size. In the age hardening curves, the peak hardness values become higher with decreasing of grain size.

Effect of Bi on Microstructure and Mechanical Properties of Extruded AZ80-2Sn Magnesium Alloy

2018 ◽  
Vol 37 (1) ◽  
pp. 97-103 ◽  
Author(s):  
Hansong Xue ◽  
Xinyu Li ◽  
Weina Zhang ◽  
Zhihui Xing ◽  
Jinsong Rao ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Tensile Strength ◽  
Magnesium Alloy ◽  
Ultimate Tensile Strength ◽  
Yield Strength ◽  
Microstructure And Mechanical Properties ◽  
Average Grain Size

AbstractThe effects of Bi on the microstructure and mechanical properties of AZ80-2Sn alloy were investigated. The results show that the addition of Bi within the as-cast AZ80-2Sn alloy promotes the formation of Mg3Bi2 phase, which can refine the grains and make the eutectic phases discontinuous. The addition of 0.5 % Bi within the as-extruded AZ80-2Sn alloy, the average grain size decreases to 12 μm and the fine granular Mg17Al12 and Mg3Bi2 phases are dispersed in the α-Mg matrix. With an increase in Bi content, the Mg17Al12 and Mg3Bi2 phases become coarsened and the grain size increases. The as-extruded AZ80-2Sn-0.5 %Bi alloy has the optimal properties, and the ultimate tensile strength, yield strength and elongation are 379.6 MPa, 247.1 MPa and 14.8 %, respectively.

Effect of Ultrasonic Treatment on the Grain Refinement and Mechanical Properties of AZ91 Magnesium Alloy

2012 ◽  
Vol 710 ◽  
pp. 463-468 ◽  
Author(s):  
Pramod Bhingole ◽  
Gajanan Chaudhari
Keyword(s):  
Mechanical Properties ◽  
Magnesium Alloy ◽  
Ultrasonic Vibration ◽  
Ultrasonic Treatment ◽  
High Intensity ◽  
Intermetallic Phase ◽  
Ultrasonic Vibrations ◽  
Az91 Magnesium Alloy ◽  
Average Grain Size ◽  
Az91 Magnesium

The present study examines the microstructural evolution and mechanical properties of AZ91 magnesium alloy solidified under high intensity ultrasonic treatment (UST). High intensity ultrasonic vibrations were introduced isothermally below the liquidus temperature into the solidifying AZ91 alloy for the refinement of primary α-Mg grains and β-Mg17Al12intermetallic phase.Various microstructures were produced using different intensity of ultrasonic vibration at a constant temperature and fixed duration of UST. Without any ultrasonic treatment, the structure contains dendrites of primary α-Mg phase which are coarser and non-uniform in size. Nearly uniform, equiaxed grains with continuous and uniform network of intermetallic phase segregated along the grain boundaries were obtained in alloy subjected to high intensity ultrasonic vibration. The average grain size in this case decreased drastically from 300 μm for (without UST) to 17 μm (with UST at intensity of 4 kW/cm2). Vickers hardness also increased steadily with increase in ultrasonic intensity. The mechanisms for microstructural refinement are discussed and it is concluded that the fine uniform grain structure achieved under ultrasonic vibrations is attributed to the cavitation and the acoustic flow induced by ultrasonic vibrations.

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