scholarly journals Effect of Nucleant Particle Agglomeration on Grain Size

2022 ◽  
Author(s):  
Feng Gao ◽  
Zhongyun Fan
Keyword(s):  
Grain Size ◽  
Solid Particle ◽  
Practical Implication ◽  
Solid Particles ◽  
Grain Structure ◽  
Particle Agglomeration ◽  
Industrial Practice ◽  
Nucleant Particle ◽  
Free Zone ◽  
Solute Accumulation

AbstractSolute accumulation/depletion in the liquid around a growing solid particle during the solidification of metallic melts creates a constitutionally supercooled (CS) zone that has a significant effect on the final solidified grain structure. In this paper, we introduce two mechanisms related to the CS zone that affect grain size: one is the grain initiation free zone (GIFZ) that describes the inability of nucleant particles located in the CS zone for grain initiation and the other is re-melting (RM) of solid particles due to overlap of CS zones. Based on these two mechanisms, we have systematically analysed the effect of nucleant particle agglomeration on grain size. We found that nucleant particle agglomeration has a significant effect on grain size and is responsible for the discrepancy between theoretically predicted grain size and the experimental data. In addition, our numerical analysis suggests that under normal solidification conditions relevant to industrial practice solid particle re-melting has little effect on grain size and thus may be ignored during theoretical analysis. A practical implication from this work is that significant grain refinement can be achieved by dispersing the nucleant particles in the melt prior to solidification.

Structural and Electrical Characterization of Shaped Beam Laser Recrystallized Polysilicon on Amorphous Substrates

1981 ◽  
Vol 4 ◽  
Author(s):  
T. J. Stultz ◽  
J. F. Gibbons
Keyword(s):  
Grain Size ◽  
Electrical Characterization ◽  
Grain Structure ◽  
Electrical Characteristics ◽  
Shaped Beam ◽  
Beam Laser ◽  
Cw Laser ◽  
Amorphous Substrates ◽  
Circular Beam

ABSTRACTStructural and electrical characterization of laser recrystallized LPCVD silicon films on amorphous substrates using a shaped cw laser beam have been performed. In comparing the results to data obtained using a circular beam, it was found that a significant increase in grain size can be achieved and that the surface morphology of the shaped beam recrystallized material was much smoother. It was also found that whereas circular beam recrystallized material has a random grain structure, shaped beam material is highly oriented with a <100> texture. Finally the electrical characteristics of the recrystallized film were very good when measured in directions parallel to the grain boundaries.

Surface Modification and its Influence on the Microstructure and Creep Resistance of Nickel Based Superalloy René 77 / Modyfikacja Powierzchniowa Oraz Jej Wpływ Na Mikrostrukture I Wytrzymałosc Na Pełzanie Odlewów Z Nadstopu Niklu Ren´E 77

2013 ◽  
Vol 58 (1) ◽  
pp. 95-98 ◽  
Author(s):  
M. Zielinska ◽  
J. Sieniawski
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Surface Modification ◽  
Turbine Blades ◽  
Processing Parameters ◽  
Grain Structure ◽  
Creep Tests ◽  
Cobalt Aluminate ◽  
Nickel Based Superalloy ◽  
Average Grain Size

Superalloy René 77 is very wide used for turbine blades, turbine disks of aircraft engines which work up to 1050°C. These elements are generally produced by the investment casting method. Turbine blades produced by conventional precision casting methods have coarse and inhomogeneous grain structure. Such a material often does not fulfil basic requirements, which concern mechanical properties for the stuff used in aeronautical engineering. The incorporation of controlled grain size improved mechanical properties. This control of grain size in the casting operation was accomplished by the control of processing parameters such as casting temperature, mould preheating temperature, and the use of grain nucleates in the face of the mould. For nickel and cobalt based superalloys, it was found that cobalt aluminate (CoAl2O4) has the best nucleating effect. The objective of this work was to determine the influence of the inoculant’s content (cobalt aluminate) in the surface layer of the ceramic mould on the microstructure and mechanical properties at high temperature of nickel based superalloy René 77. For this purpose, the ceramic moulds were made with different concentration of cobalt aluminate in the primary slurry was from 0 to 10% mass. in zirconium flour. Stepped and cylindrical samples were casted for microstructure and mechanical examinations. The average grain size of the matrix ( phase), was determined on the stepped samples. The influence of surface modification on the grain size of up to section thickness was considered. The microstructure investigations with the use of light microscopy and scanning electron microscopy (SEM) enable to examine the influence of the surface modification on the morphology of ’ phase and carbides precipitations. Verification of the influence of CoAl2O4 on the mechanical properties of castings were investigated on the basis of results obtained form creep tests.

Statistical Assessment of the Effects of Grain-Structure Representation and Micro-Properties on the Behavior of Bonded Block Models for Brittle Rock Damage Prediction

2021 ◽  
Vol 13 (14) ◽  
pp. 7889
Author(s):  
Carlos Efrain Contreras Inga ◽  
Gabriel Walton ◽  
Elizabeth Holley
Keyword(s):  
Grain Size ◽  
Grain Shape ◽  
Grain Structure ◽  
Minor Effect ◽  
Unique Contribution ◽  
Structure Generation ◽  
Structure Representation ◽  
The Real ◽  
Study Results ◽  
Block Models

The ability to predict the mechanical behavior of brittle rocks using bonded block models (BBM) depends on the accuracy of the geometrical representation of the grain-structure and the applied micro-properties. This paper evaluates the capabilities of BBMs for predictive purposes using an approach that employs published micro-properties in combination with a Voronoi BBM that properly approximates the real rock grain-structure. The Wausau granite, with Unconfined Compressive Strength (UCS) of 226 MPa and average grain diameter of 2 mm, is used to evaluate the effectiveness of the predictive approach. Four published sets of micro-properties calibrated for granites with similar mineralogy to the Wausau granite are used for the assessment. The effect of grain-structure representation in Voronoi BBMs is analyzed, considering grain shape, grain size and mineral arrangement. A unique contribution of this work is the explicit consideration of the effect of stochastic grain-structure generation on the obtained results. The study results show that the macro-properties of a rock can be closely replicated using the proposed approach. When using this approach, the micro-properties have a greater impact on the realism of the predictions than the specific grain-structure representation. The grain shape and grain size representations have a minor effect on the predictions for cases that do not deviate substantially from the real average grain geometry. However, the stochastic effect introduced by the use of randomly-generated Voronoi grain-structures can be significant, and this effect should be considered in future studies.

Simulation of Impaction Between Liquid Droplet and Solid Particles Based on SPH Method

2014 ◽  
Author(s):  
Shuai Meng ◽  
Qian Wang ◽  
Rui Yang
Keyword(s):  
Surface Tension ◽  
Solid Particle ◽  
Liquid Droplet ◽  
Particle Interaction ◽  
Solid Particles ◽  
Seed Particle ◽  
Liquid Droplets ◽  
Particle Hydrodynamics ◽  
Smoothed Particle ◽  
Spray Granulation

The phenomenon of impaction between liquid droplets and solid particles is involved in many scientific problems and engineering applications, such as impaction between sprayed droplet and solid particles in limestone injection desulfurization system and the collision between a droplet of the liquid to be granulated and a seed particle in fluidized bed spray granulation process. There are a lot of factors affected this phenomenon: droplet and particle size, momentum of both liquid droplet and solid particles, materials, surface conditions of the solid particles and so on. However the experimental or numerical researches have been done mostly pay attention to Specific application or process, so the impaction phenomenon has not been through studied, for example how different factors affected the impaction process with its effect on different applications. This paper focuses on the basic issue of interaction between droplet and solid particles. Three main factors were considered: ratio of diameter between the droplet and solid particle, relative velocity and the surface tension (including the contact angle between droplet and solid particle). All the study is based on simulation using SPH (smoothed particle hydrodynamics) method, and the surface tension is simulated by particle-particle interaction.

Recrystallization and Grain Growth during Alloy 718 Processing

2007 ◽  
Vol 539-543 ◽  
pp. 3094-3099
Author(s):  
Nho Kwang Park ◽  
Jeoung Han Kim ◽  
Jong Taek Yeom
Keyword(s):  
Grain Size ◽  
Grain Growth ◽  
Heat Treatments ◽  
Grain Structure ◽  
Alloy 718 ◽  
Compression Tests ◽  
Δ Phase ◽  
Grain Boundary Characteristics ◽  
The Difference ◽  
Boundary Characteristics

In Alloy 718 ingot cogging process, dynamic and metadynamic recrystallizations, and static grain growth occur, and also the presence of δ phase plays a key role in controlling the grain size. In this study, the evolution of grain structure in VIM/VAR-processed Alloy 718 ingots during post-cogging heat treatments is dealt with. Compression tests were made on VIM/VAR-processed Alloy 718 ingot at temperatures between 900oC ~ 1150oC. Heat treatments were made on the compression-tested specimens, and the variation of grain size was evaluated. Constitutive equations for the grain growth are established to represent the evolution of microstructures. Special attention is paid to the evolution of grain structure under the condition of dynamic and metadynamic recrystallizations, and grain growth. The grain growth rate depends mainly on the presence of δ-phase below the δ-solvus temperature, and on the difference in the grain boundary characteristics above it.

A Model for the Effect of Velocity on Erosion of N80 Steel Tubing due to the Normal Impingement of Solid Particles

1992 ◽  
Vol 114 (1) ◽  
pp. 54-64 ◽  
Author(s):  
D. P. Chase ◽  
E. F. Rybicki ◽  
J. R. Shadley
Keyword(s):  
Solid Particle ◽  
Computational Study ◽  
Target Material ◽  
Target Surface ◽  
American Petroleum Institute ◽  
Solid Particles ◽  
Unknown Coefficient ◽  
Conservation Of Energy ◽  
Carrier Fluid ◽  
Erosion Behavior

As part of a combined experimental and computational study of erosion for gas and oil production conditions, a semi-empirical model has been developed to predict erosion ratio behaviors of metals due to solid particle impingement. One use of the model will be to reduce the total number of experiments needed to characterize erosion behavior. The model represents material property information associated with both the target material and the impinging particles, as well as impingement speed. Five different models are examined in terms of ability to predict erosion ratio behavior as a function of impingement speed. The model selected is based on a conservation of energy formulation and fracture mechanics considerations to predict the amount of material removed due to solid particle impingement. The resulting equation to predict the erosion ratio for a given particle size contains one unknown coefficient which is determined through comparison with experimental data. Illustrative examples are presented for data for two different sizes of glass bead solid particles in an oil carrier fluid impinging on an API (American Petroleum Institute) N80 grade steel target at an impingement angle 90 deg to the target surface. Using erosion data at one impingement speed to determine the unknown coefficient, the model was used to predict erosion behavior at a range of other speeds. Good agreement between the erosion ratio data and the values predicted by the model were found for two solid particle sizes. Recommendations for expanding the capabilities of the model are pointed out.

The Influence of Section Thickness on Microstructure of Elektron 21 and QE22 Magnesium Alloys

2012 ◽  
Vol 191 ◽  
pp. 145-150 ◽  
Author(s):  
Michał Stopyra ◽  
Robert Jarosz ◽  
Andrzej Kiełbus
Keyword(s):  
Solid Solution ◽  
Grain Size ◽  
Magnesium Alloys ◽  
Statistical Methods ◽  
Wall Thickness ◽  
Light Microscope ◽  
Volume Fraction ◽  
Grain Structure ◽  
Section Thickness ◽  
Gating System

The paper presents analysis of section thickness’ influence on microstructure of Elektron 21 and QE22 magnesium alloys in the form of a stepped casting test. Solid solution grain size and volume fraction of eutectic areas were measured using light microscope and sterological methods. The results showed the significant increase of grain size caused by wall thickness and its slight decrease connected with the distance beetwen analysed section and the gating system. This relationship was confirmed using statistical methods. QE22 alloy demonstrated finer grain structure than Elektron 21 alloy as well as lesser susceptibility of grain size to solidification conditions

Modeling of Dual-Phase Grain Structure in Ti-6Al-4V during Isothermal and Non-Isothermal Heat Treatment by Using Cellular Automata

2013 ◽  
Vol 753 ◽  
pp. 353-356
Author(s):  
Alfred Krumphals ◽  
Cecilia Poletti ◽  
Fernando Warchomicka ◽  
Martin Stockinger ◽  
Christof Sommitsch
Keyword(s):  
Heat Treatment ◽  
Grain Size ◽  
Cellular Automata ◽  
Isothermal Holding ◽  
Equilibrium Phase ◽  
Beta Phase ◽  
Grain Structure ◽  
Isothermal Heat Treatment ◽  
Dual Phase ◽  
Two Phase

In the titanium alloy Ti-6Al-4V the dual-phase grain structure, which forms during thermo-mechanical processing, is of high importance due to its effect on the mechanical properties. In general the most significant microstructural parameters are the amount of alpha and beta phase as well as their grain size. For this reason a new cellular automata method (CA) was developed to predict the evolving grain structure during isothermal and non-isothermal heat treatment. The probabilistic CA model is based on the diffusion controlled movement of grain and phase boundaries. During temperature changes an algorithm is adjusting alpha and beta phase fraction to maintain equilibrium phase values. Hence, the CA is capable to calculate grain coarsening as well as grain growth and shrinking in the two-phase area while heating and isothermal holding at forging temperature. The initial microstructure can be imported form virtual created microstructures, real micrographs and EBSD-images. The results are mean grain diameters, grain size distributions and virtually simulated microstructures which can be easily compared with real micrographs. The predicted microstructures are showing a good correlation to data in literature and experimental results.

Macro and Microstructural Effects of the Application of an Induced Axial Magnetic Field During the Deposition of Aluminum Weld Beads

2009 ◽  
Vol 1242 ◽  
Author(s):  
M. A. García ◽  
V. H. López M. ◽  
R. García H. ◽  
F. F. Curiel L. ◽  
R. R. Ambríz R.
Keyword(s):  
Magnetic Field ◽  
Grain Size ◽  
Magnetic Fields ◽  
Weld Metal ◽  
Size Distribution ◽  
Grain Size Distribution ◽  
Axial Magnetic Field ◽  
Grain Structure ◽  
Bead Geometry ◽  
External Power Source

ABSTRACTIn this work, aluminum weld beads were deposited on aluminum plates of commercial purity (12.7 mm thick), using an ER-5356 filler wire. The aim of the experiments was to assess the effects that yield the induction of an axial magnetic field (AMF) during the application of the weld beads using the direct current gas metal arc welding process (DC-GMAW). An external power source was use to induce magnetic fields between 0 to 28 mT. The effects of the magnetic fields were assessed in terms of the macrostructural features of the deposits, morphology of the grain structure, grain size and grain size distribution in the weld metal. Macrostructural characteristics of the weld beads revealed that increasing the intensity of the magnetic induction to produce a magnetic field above 14 mT, leads to a significant loss of feeding material and there is a tendency of the deposits to increase their width and reduce penetration. Perturbation of the weld pool induced by the application of the AMF noticeably modified the grain structure in the weld metal. In particular, for the intensities of 5 and 14 mT, columnar growth was essentially non-existent. Grain size distribution plots showed, generally speaking, that the use of magnetic fields is an efficient method to produce homogeneous grain structures within the weld metal. Finite element analysis was used to explain the weld bead geometry with the intensity of the magnetic field.

Modeling evaluation on solid-liquid mixing characteristics in a dislocated guide impeller stirred tank

2021 ◽  
Vol 0 (0) ◽  
Author(s):  
Deyin Gu ◽  
Fenghui Zhao ◽  
Xingmin Wang ◽  
Zuohua Liu
Keyword(s):  
Power Consumption ◽  
Solid Particle ◽  
Particle Diameter ◽  
Solid Particles ◽  
Stirred Tank ◽  
Mixing Process ◽  
Solid Holdup ◽  
Aperture Ratio ◽  
Liquid Mixing ◽  
Solid Liquid

Abstract The solid-liquid mixing characteristics in a stirred tank with pitched blade impellers, dislocated impellers, and dislocated guide impellers were investigated through using CFD simulation. The effects of impeller speed, impeller type, aperture ratio, aperture length, solid particle diameter and initial solid holdup on the homogeneity degree in the solid-liquid mixing process were investigated. As expected, the solid particle suspension quality was increased with an increase in impeller speed. The dislocated impeller could reduce the accumulation of solid particles and improve the cloud height compared with pitched blade impeller under the same power consumption. The dislocated guide impeller could enhance the solid particles suspension quality on the basis of dislocated impeller, and the optimum aperture ratio and aperture length of dislocated guide impeller were 12.25% and 7 mm, respectively, in the solid-liquid mixing process. Smaller solid particle diameter and lower initial solid holdup led to higher homogeneity degree of solid-liquid mixing system. The dislocated guide impeller could increase solid particle integrated velocity and enhance turbulent intensity of solid-liquid two-phase compared with pitched blade impeller and dislocated impeller under the same power consumption.

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