scholarly journals The influence of different sample preparation on mechanical properties of human iliotibial tract

2020 ◽  
Vol 10 (1) ◽  
Author(s):  
Benjamin Fischer ◽  
Sascha Kurz ◽  
Andreas Höch ◽  
Stefan Schleifenbaum

Abstract In the run-up to biomechanical testing, fresh human tissue samples are often frozen in order to inhibit initial decomposition processes and to achieve a temporal independence of tissue acquisition from biomechanical testing. The aim of this study was to compare the mechanical properties of fresh tissue samples of the human iliotibial tract (IT) to fresh-frozen samples taken from the same IT and those modified with different concentrations of Dimethylsulfoxide (DMSO) prior to freezing. All samples were partial plastinated and destructive tensile tests were conducted with a uniaxial tensile test setup. A plastination technique already established in the laboratory was modified to improve the clamping behaviour of the samples. Material failure was caused by a gradual rupture of the load-bearing collagen fibre bundles. Contrary to our expectations, no significant difference was found between the tensile strength of fresh and fresh frozen specimens. The addition of 1 wt% DMSO did not increase the tensile strength compared to fresh-frozen samples; an addition of 10 wt% DMSO even resulted in a decrease. Based on our findings, the use of simple fresh-frozen specimens to determine the tensile strength is viable; however fresh specimens should be used to generate a complete property profile.

2018 ◽  
Vol 913 ◽  
pp. 109-117 ◽  
Author(s):  
Qing Yun Zhao ◽  
Si Rui Cheng ◽  
Li Dong Wang ◽  
Li Min Dong ◽  
Feng Lei Liu

The effects of heat treatment on microstructure and mechanical properties of Ti-38644 alloy were investigated by scanning electron microscope (SEM) and transmission electron microscopy (TEM) as well as uniaxial tensile test. The results show that when the solution temperature is lower than 845°C, the microstructure of Ti-38644 alloy is equiaxed β phase with the grain size of 20μm, and the tensile strength is about 960MPa. As raising solution temperature to 860°C, the grain size of Ti-38644 alloy increases to 100μm and the tensile strength decreased to 870MPa. There are a large number of secondary α phase precipitated from the grain boundaries and within grain of β phase undergoing aging treatment. Secondary α phase coarsens with increasing the aging temperature, leading to the decrease of tensile strength. After solution treatment at 815°C for 1.5h, water quenching plus aging at 520°C for 10h, air cooling, Ti-38644 alloy shows a better mechanical property with the tensile strength 1330MPa, elongation and reduction of area 10% and 45% respectively.


Author(s):  
M. A. Malik ◽  
I. Salam ◽  
W. Muhammad

The extruded materials are extensively used in chemical, food and nuclear industry and generally offer a unique combination of strength and freedom with regard to design solutions. During extrusion, material flow occurs in the direction of applied force and as a result microstructure change. The process ultimately induces variation in the mechanical properties when tested along or across the extrusion direction. The uniaxial tensile test is a simple and versatile test to expose most of the mechanical properties of the materials required to ensure the reliability of the systems. In present study, the mechanical behavior of an Al-Mg-Si alloy extruded cylinder has been determined with the help of uniaxial tensile test in longitudinal and transverse orientations. The microstructural features revealed significant difference in two orientations and constituent particles were found aligned in the direction of extrusion. Tensile tests were conducted in displacement mode at different cross head speeds corresponding to strain rates ranging from 10−5 to 10−1 s−1. The tests were conducted at ambient temperature in air atmosphere. The data thus obtained include: yield strength, ultimate tensile strength, percent elongation and reduction of area. Comparing the trends of strength variation, the material shows higher yield strength in longitudinal orientation as compared to transverse orientation. A slight increase in the yield strength with increasing strain rate was found in both the orientations. The ultimate tensile strength in both the directions was found similar and there was no appreciable change with increasing strain rate. The elongation and reduction in area were found higher in the longitudinal orientation. The effect of strain rate on these properties was negligible up to maximum speed tested. In longitudinal orientation typical dimpled fracture was observed indicating deformation before failure. In transverse orientation shallow dimples were present. The present study revealed that the distribution of constituent particles in an extruded thick-walled cylinder has a pronounced effect on its mechanical behavior and fracture morphology.


Author(s):  
M. Carraturo ◽  
G. Alaimo ◽  
S. Marconi ◽  
E. Negrello ◽  
E. Sgambitterra ◽  
...  

AbstractAdditive manufacturing (AM), and in particular selective laser melting (SLM) technology, allows to produce structural components made of lattice structures. These kinds of structures have received a lot of research attention over recent years due to their capacity to generate easy-to-manufacture and lightweight components with enhanced mechanical properties. Despite a large amount of work available in the literature, the prediction of the mechanical behavior of lattice structures is still an open issue for researchers. Numerical simulations can help to better understand the mechanical behavior of such a kind of structure without undergoing long and expensive experimental campaigns. In this work, we compare numerical and experimental results of a uniaxial tensile test for stainless steel 316L octet-truss lattice specimen. Numerical simulations are based on both the nominal as-designed geometry and the as-build geometry obtained through the analysis of µ-CT images. We find that the use of the as-build geometry is fundamental for an accurate prediction of the mechanical behavior of lattice structures.


Materials ◽  
2021 ◽  
Vol 14 (14) ◽  
pp. 3969
Author(s):  
Shirui Zhang ◽  
Shili Qiu ◽  
Pengfei Kou ◽  
Shaojun Li ◽  
Ping Li ◽  
...  

Granite exhibits obvious meso-geometric heterogeneity. To study the influence of grain size and preferred grain orientation on the damage evolution and mechanical properties of granite, as well as to reveal the inner link between grain size‚ preferred orientation, uniaxial tensile strength (UTS) and damage evolution, a series of Brazilian splitting tests were carried out based on the combined finite-discrete element method (FDEM), grain-based model (GBM) and inverse Monte Carlo (IMC) algorithm. The main conclusions are as follows: (1) Mineral grain significantly influences the crack propagation paths, and the GBM can capture the location of fracture section more accurately than the conventional model. (2) Shear cracks occur near the loading area, while tensile and tensile-shear mixed cracks occur far from the loading area. The applied stress must overcome the tensile strength of the grain interface contacts. (3) The UTS and the ratio of the number of intergrain tensile cracks to the number of intragrain tensile cracks are negatively related to the grain size. (4) With the increase of the preferred grain orientation, the UTS presents a “V-shaped” characteristic distribution. (5) During the whole process of splitting simulation, shear microcracks play the dominant role in energy release; particularly, they occur in later stage. This novel framework, which can reveal the control mechanism of brittle rock heterogeneity on continuous-discontinuous trans-scale fracture process and microscopic rock behaviour, provides an effective technology and numerical analysis method for characterizing rock meso-structure. Accordingly, the research results can provide a useful reference for the prediction of heterogeneous rock mechanical properties and the stability control of engineering rock masses.


Metals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 1097
Author(s):  
Umer Masood Chaudry ◽  
Seung-Chang Han ◽  
Fathia Alkelae ◽  
Tea-Sung Jun

In the present study, the effect of post-weld heat treatment (PWHT) on the microstructure and mechanical properties of friction stir welded (FSW) DP780 steel sheets was investigated. FSW was carried out at a constant tool rotation speed of 400 rpm and different welding speeds (200 mm/min and 400 min/min). A defect free weld was witnessed for both of the welding conditions. The mutual effect of severe plastic deformation and frictional heat generation by pin rotation during the FSW process resulted in grain refinement due to dynamic recrystallization in the stir zone (SZ) and thermo-mechanically affected zone (TMAZ). Lower tensile elongation and higher yield and ultimate tensile strengths were recorded for welded-samples as compared to the base material (BM) DP780 steel. The joints were subsequently annealed at various temperatures at 450–650 °C for 1 h. At higher annealing temperature, the work hardening rate of joints gradually decreased and subsequently failed in the softened heat-affected zone (HAZ) during the uniaxial tensile test. Reduction in yield strength and tensile strength was found in all PWHT conditions, though improvement in elongation was achieved by annealing at 550 °C. The digital image correlation analysis showed that an inhomogeneous strain distribution occurred in the FSWed samples, and the strain was particularly highly localized in the advancing side of interface zone. The nanoindentation measurements covering the FSWed joint were consistent with an increase of the annealing temperature. The various grains size in the BM, TMAZ, and SZ is the main factor monitoring the hardness distribution in these zones and the observed discrepancies in mechanical properties.


Metals ◽  
2018 ◽  
Vol 8 (10) ◽  
pp. 790 ◽  
Author(s):  
Changping Tang ◽  
Kai Wu ◽  
Wenhui Liu ◽  
Di Feng ◽  
Xuezhao Wang ◽  
...  

The effects of Gd, Y content on the microstructure and mechanical properties of Mg-Gd-Y-Nd-Zr alloy were investigated using hardness measurements, X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive spectrometer (EDS), and uniaxial tensile testing. The results indicate that the alloys in as-cast condition mainly consist of α-Mg matrix and non-equilibrium eutectic Mg5.05RE (RE = Gd, Y, Nd). After solution treatment, the non-equilibrium eutectics dissolved into the matrix but some block shaped RE-rich particles were left at the grain boundaries and within grains. These particles are especially Y-rich and deteriorate the mechanical properties of the alloys. Both the compositions of the eutectic and the block shaped particle were independent of the total Gd, Y content of the alloys, but the number of the particles increases as the total Gd, Y content increases. The ultimate tensile strength increases as the total Gd, Y content decreases. A Mg-5.56Gd-3.38Y-1.11Nd-0.48Zr alloy with the highest ultimate tensile strength of 280 MPa and an elongation of 1.3% was fabricated. The high strength is attributed to the age hardening behavior and the decrease in block shaped particles.


Author(s):  
Pradeep Lall ◽  
Vikas Yadav ◽  
Jeff Suhling ◽  
David Locker

Electronics in automotive underhood and downhole drilling applications may be subjected to sustained operation at high temperature in addition to high strain-rate loads. SAC solders used for second level interconnects have been shown to experience degradation in high strain-rate mechanical properties under sustained exposure to high temperatures. Industry search for solutions for resisting the high-temperature degradation of SAC solders has focused on the addition of dopants to the alloy. In this study, a doped SAC solder called SAC-Q solder have been studied. The high strain rate mechanical properties of SAC-Q solder have been studied under elevated temperatures up to 200°C. Samples with thermal aging at 50°C for up to 6-months have been used for measurements in uniaxial tensile tests. Measurements for SAC-Q have been compared to SAC105 and SAC305 for identical test conditions and sample geometry. Data from the SAC-Q measurements has been fit to the Anand Viscoplasticity model. In order to assess the predictive power of the model, the computed Anand parameters have been used to simulate the uniaxial tensile test and the model predictions compared with experimental data. Model predictions show good correlation with experimental measurements. The presented approach extends the Anand Model to include thermal aging effects.


Author(s):  
R Pramod ◽  
N Siva Shanmugam ◽  
C K Krishnadasan ◽  
G Radhakrishnan ◽  
Manu Thomas

This work mainly focuses on designing a novel aluminum alloy 6061-T6 pressure vessel liner intended for use in launch vehicles. Fabrication of custom-made welding fixtures for the assembly of liner parts, namely two hemispherical domes and end boss, is illustrated. The parts of the liner are joined using the cold metal transfer welding process, and the welding trials are performed to arrive at an optimized parametric range. The metallurgical characterization of weld joint reveals the existence of dendritic structures (equiaxed and columnar). Microhardness of base and weld metal was 70 and 65 HV, respectively. The tensile strength of base and weld metal was 290 and 197 MPa, respectively, yielding a joint efficiency of 68%. Finite-element analysis of a uniaxial tensile test was performed to predict the tensile strength and location of the fracture in base and weld metal. The experimental and predicted tensile test results were found to be in good agreement.


2021 ◽  
Vol 23 (4) ◽  
pp. 140-154
Author(s):  
Tatiana Kalashnikova ◽  
◽  
Vladimir Beloborodov ◽  
Kseniya Osipovich ◽  
Andrey Vorontsov ◽  
...  

Introduction. Friction stir welding and processing are almost identical processes of severe plastic deformation at elevated temperatures. These technologies differ mainly in the purpose of its use: the formation of a hardened surface layer or producing a welded joint. However, it is known that both during welding and during processing of heavy gauge workpieces temperature gradients occur. As a result, the conditions of adhesive interaction, material plastic flow, and the formation of the stir zone change as compared to thin-sheet workpieces with fundamentally different heat dissipation rates. In this connection, the purpose of the work is to determine the regularities of the structure formation and stability of the mechanical properties in different directions in the material of 35-mm-thick aluminum-magnesium alloy samples produced by friction stir welding/processing. Research Methodology. The technique and modes of friction stir welding and processing of AA5056 alloy workpieces with a thickness of 35 mm are described. Data on the equipment used for mechanical tests and structural research are given. Results and discussion. The data obtained show the excess mechanical properties of the processing zone material over the base metal ones in all studied directions. Material structure heterogeneities after friction stir welding/processing of heavy gauge workpieces have no determining effect on the stir zone properties. At the same time, there is no clear correlation between the tensile strength values and the load application direction, nor is there any significant difference in mechanical properties depending on the location of the samples inside the stir zone. The average ultimate tensile strength values in the vertical, transverse, and longitudinal directions are 302, 295 and 303 MPa, respectively, with the yield strength values of 155, 153 and 152 MPa, and the relative elongation of 27.2, 27.5, 28.7 %.


2021 ◽  
Author(s):  
Budi Arifvianto ◽  
Teguh Nur Iman ◽  
Benidiktus Tulung Prayoga ◽  
Rini Dharmastiti ◽  
Urip Agus Salim ◽  
...  

Abstract Fused filament fabrication (FFF) has become one of the most popular, practical, and low-cost additive manufacturing techniques for fabricating geometrically-complex thermoplastic polyurethane (TPU) elastomer. However, there are still some uncertainties concerning the relationship between several operating parameters applied in this technique and the mechanical properties of the processed material. In this research, the influences of extruder temperature and raster orientation on the mechanical properties of the FFF-processed TPU elastomer were studied. A series of uniaxial tensile tests was carried out to determine tensile strength, strain, and elastic modulus of TPU elastomer that had been printed with various extruder temperatures, i.e., 190–230 °C, and raster angles, i.e., 0–90°. Thermal and chemical characterizations were also conducted to support the analysis in this research. The results obviously showed the ductile and elastic characteristics of the FFF-processed TPU, with specific tensile strength and strain that could reach up to 39 MPa and 600%, respectively. The failure mechanisms operating on the FFF-processed TPU and the result of stress analysis by using the developed Mohr’s circle are also discussed in this paper. In conclusion, the extrusion temperature of 200 °C and raster angle of 0° could be preferred to be applied in the FFF process to achieve high strength and ductile TPU elastomer.


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