Influence of Carbon Content in Cobalt-Based Superalloys on Mechanical and Wear Properties

2004 ◽  
Vol 126 (2) ◽  
pp. 204-212 ◽  
Author(s):  
Rong Liu ◽  
Matthew X. Yao ◽  
Xijia Wu
Keyword(s):  
Mechanical Properties ◽  
Wear Resistance ◽  
Carbon Content ◽  
X Ray Diffraction ◽  
Wear Properties ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Pin On Disc ◽  
Rotating Bending ◽  
The Impact

Two cobalt-based superalloys containing 1.6% and 2% carbon respectively were studied, with the emphasis on the influence of the carbon content on their microstructures, wear resistance, and mechanical properties. Phase formation and transformation in the microstructures were analyzed using metallographic, X-ray diffraction, and differential scanning calorimetry techniques. Wear resistance, tensile and fatigue behaviors of the alloys were investigated on a pin-on-disc tribometer, MTS machine and rotating-bending machine, respectively. It is found that the wear resistance was increased significantly with the carbon content. The mechanical properties of the alloys are also influenced by the carbon content, but the impact is not so significant as on the wear resistance. It was observed that the carbon content increased the yielding strength and fatigue strength, but decreased the fracture stress and fracture strain.

Studies on Mechanical Properties and Structure of LLDPE/Nano-Montmorillonite Composites

2012 ◽  
Vol 510 ◽  
pp. 579-584
Author(s):  
Yu Xin Liu ◽  
Qi Yang ◽  
Fang Yang ◽  
Yong Fei Zhu ◽  
Xian Zhong Mo
Keyword(s):  
Mechanical Properties ◽  
Mechanical Test ◽  
Linear Low Density Polyethylene ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
Melting Method ◽  
X Ray ◽  
Small Angle Light Scattering ◽  
The Impact ◽  
Scanning Electron

Linear low-density polyethylene (LLDPE)/nano-montmorillonite (nano-MMT) composites were prepared by melting method. Mechanical test, scanning electron microscope (SEM), X-ray diffraction (XRD), differential scanning calorimetry (DSC) and small angle light scattering (SALS) measurements were used to characterize the mechanical properties and structure of the LLDPE composite. The results indicated that the impact strength of LLDPE decreased with the increase of nano-MMT content. However, the tensile strength firstly increased and then decreased. The aggregation of nano-MMT in LLDPE happened at larger content. The spherulite size and crystallinity of LLDPE reduced with the addition of nano-MMT. Furthermore, it was found that the structure of the spherulite was destroyed by the nano-MMT. The microcrystal size of LLDPE also decreased with the increase of nano-MMT content.

scholarly journals Effects of Sintering Temperature on Densification, Microstructure and Mechanical Properties of Al-Based Alloy by High-Velocity Compaction

Metals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 218
Author(s):  
Xianjie Yuan ◽  
Xuanhui Qu ◽  
Haiqing Yin ◽  
Zaiqiang Feng ◽  
Mingqi Tang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
High Velocity ◽  
Sintered Density ◽  
Sintering Temperature ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Transmission Electron ◽  
High Velocity Compaction ◽  
Sintered Temperature

This present work investigates the effects of sintering temperature on densification, mechanical properties and microstructure of Al-based alloy pressed by high-velocity compaction. The green samples were heated under the flow of high pure (99.99 wt%) N2. The heating rate was 4 °C/min before 315 °C. For reducing the residual stress, the samples were isothermally held for one h. Then, the specimens were respectively heated at the rate of 10 °C/min to the temperature between 540 °C and 700 °C, held for one h, and then furnace-cooled to the room temperature. Results indicate that when the sintered temperature was 640 °C, both the sintered density and mechanical properties was optimum. Differential Scanning Calorimetry, X-ray diffraction of sintered samples, Scanning Electron Microscopy, Energy Dispersive Spectroscopy, and Transmission Electron Microscope were used to analyse the microstructure and phases.

Research on compatibility and surface of high impact bio-based polyamide

2021 ◽  
pp. 095400832110055
Author(s):  
Yang Wang ◽  
Yuhui Zhang ◽  
Yuhan Xu ◽  
Xiucai Liu ◽  
Weihong Guo
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Differential Scanning Calorimetry ◽  
Crystallization Behavior ◽  
High Impact ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Scanning Electron

The super-tough bio-based nylon was prepared by melt extrusion. In order to improve the compatibility between bio-based nylon and elastomer, the elastomer POE was grafted with maleic anhydride. Scanning Electron Microscopy (SEM) and Thermogravimetric Analysis (TGA) were used to study the compatibility and micro-distribution between super-tough bio-based nylon and toughened elastomers. The results of mechanical strength experiments show that the 20% content of POE-g-MAH has the best toughening effect. After toughening, the toughness of the super-tough nylon was significantly improved. The notched impact strength was 88 kJ/m2 increasing by 1700%, which was in line with the industrial super-tough nylon. X-ray Diffraction (XRD) and Differential Scanning Calorimetry (DSC) were used to study the crystallization behavior of bio-based PA56, and the effect of bio-based PA56 with high crystallinity on mechanical properties was analyzed from the microstructure.

Mechanical and Tribological Properties of W(100-x)%Cx% Coatings Deposited by DC Magnetron Sputtering

2015 ◽  
Vol 642 ◽  
pp. 184-189
Author(s):  
Yan Liang Su ◽  
Yueh Feng Lin
Keyword(s):  
Mechanical Properties ◽  
Wear Resistance ◽  
Magnetron Sputtering ◽  
X Ray Diffraction ◽  
Mechanical And Tribological Properties ◽  
Unbalanced Magnetron Sputtering ◽  
Unbalanced Magnetron ◽  
Pin On Disc ◽  
Dry Conditions ◽  
Coating Microstructure

W(100-x)%Cx% coatings with different tungsten and carbon contents were deposited by unbalanced magnetron sputtering. The microstructures and mechanical properties of the W(100-x)%C x% coatings was characterized by scanning electron microscope (SEM), X-ray diffraction (XRD), nanoindentation and adhesion testing techniques. The tribological performance of the coatings was investigated using a pin-on-disc trobometer under dry conditions. Experimental results indicated that coating microstructure, mechanical properties and wear resistance varied according to the tungsten and carbon contents of the coatings. The W72%C28% coating had the highest hardness/elastic modulus (H/E) ratio. In the ball-on-disc wear tests, it was found that the W72%C28% coating exhibited the best wear resistance.

Effects of Cooling Rate and Sn Addition on the Microstructure of Ti-Nb-Sn Alloys

2011 ◽  
Vol 172-174 ◽  
pp. 190-195 ◽  
Author(s):  
Giorgia T. Aleixo ◽  
Eder S.N. Lopes ◽  
Rodrigo Contieri ◽  
Alessandra Cremasco ◽  
Conrado Ramos Moreira Afonso ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Cooling Rate ◽  
Melting Furnace ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Β Phase ◽  
Arc Melting ◽  
Ti Alloys ◽  
Ω Phase

Ti-based alloys present unique properties and hence, are employed in several industrial segments. Among Ti alloys, β type alloys form one of the most versatile classes of materials in relation to processing, microstructure and mechanical properties. It is well known that heat treatment of Ti alloys plays an important role in determining their microstructure and mechanical behavior. The aim of this work is to analyze microstructure and phases formed during cooling of β Ti-Nb-Sn alloy through different cooling rates. Initially, samples of Ti-Nb-Sn system were prepared through arc melting furnace. After, they were subjected to continuous cooling experiments to evaluate conditions for obtaining metastable phases. Microstructure analysis, differential scanning calorimetry and X-ray diffraction were performed in order to evaluate phase transformations. Depending on the cooling rate and composition, α” martensite, ω phase and β phase were obtained. Elastic modulus has been found to decrease as the amount of Sn was increased.

Effect of Varying Wt% of TiC on Mechanical and Wear Properties of RZ5-TiC In-Situ Composite

2018 ◽  
Vol 8 (2) ◽  
pp. 45-56 ◽  
Author(s):  
Deepak Mehra ◽  
M.M. Mahapatra ◽  
S. P. Harsha
Keyword(s):  
Wear Resistance ◽  
Wear Behavior ◽  
Wear Test ◽  
X Ray Diffraction ◽  
Wear Properties ◽  
X Ray ◽  
Tic Particle ◽  
Mechanical And Microstructural Properties ◽  
Sliding Distance

The purpose of this article is to enhance the mechanical properties and wear resistance of the RZ5 alloy used in the aerospace application by adding TiC particles. The present study discusses processing of in-situ RZ5-TiC composite fabricated by self-propagating high temperature (S.H.S.) method and its wear behavior. The effects of TiC particle on mechanical and microstructural properties of the composite are studied. The wear test is performed by varying the sliding distance and applied load. The composite is characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDS). The results exhibited the properties like strength and hardness of RZ5-10wt%TiC composite has been increased considerably, while grain size is decreased as compared to the RZ5 alloy. The fractography indicated mixed mode (quasi-cleavage and ductile feature) failure of the composites. The wear results showed improvement in wear resistance of the composite. The FESEM showed dominate wear mechanisms are abrasion, ploughing grooves.

Structure and properties of poly(3-hydroxybutyrate-co-3-hydroxyhexanoate)/poly(L-lactic acid) quasi core/sheath melt-electrospun microfibers

2018 ◽  
Vol 89 (9) ◽  
pp. 1770-1781 ◽  
Author(s):  
Huaizhong Xu ◽  
Benedict Bauer ◽  
Masaki Yamamoto ◽  
Hideki Yamane
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Lactic Acid ◽  
Tensile Tests ◽  
Processing Parameters ◽  
Structure And Properties ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Diffraction Patterns

A facile route was proposed to fabricate core–sheath microfibers, and the relationships among processing parameters, crystalline structures and the mechanical properties were investigated. The compression molded poly(3-hydroxybutyrate-co-3-hydroxyhexanoate) (PHBH)/poly(L-lactic acid) (PLLA) strip enhanced the spinnability of PHBH and the mechanical properties of PLLA as well. The core–sheath ratio of the fibers was determined by the prefab strip, while the PLLA sheath component did not completely cover the PHBH core component due to the weak interfacial tension between the melts of PHBH and PLLA. A rotational target was applied to collect aligned fibers, which were further drawn in a water bath. The tensile strength and the modulus of as-spun and drawn fibers increased with increasing the take-up velocities. When the take-up velocity was above 500 m/min, the jet became unstable and started to break up at the tip of the Taylor cone, decreasing the mechanical properties of the fibers. The drawing process facilitated the crystallization of PLLA and PHBH, and the tensile strength and the modulus increased linearly with the increasing the draw ratio. The crystal information displayed from wide-angle X-ray diffraction patterns and differential scanning calorimetry heating curves supported the results of the tensile tests.

scholarly journals Investigation of Crystalline and Tensile Properties of Carbon Nanotube-Filled Polyamide-12 Fibers Melt-Spun by Industry-Related Processes

2012 ◽  
Vol 7 (3) ◽  
pp. 155892501200700 ◽  
Author(s):  
Sanjukta Chatterjee ◽  
Felix A. Reifler ◽  
Bryan T. Chu ◽  
Rudolf Hufenus
Keyword(s):  
Mechanical Properties ◽  
Melt Spinning ◽  
Polymer Fibers ◽  
High Tensile Strength ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Polyamide 12 ◽  
Industrial Standards ◽  
Crystalline Domains

This paper addresses the influence of carbon nanotubes (CNT) on the structure and mechanical properties of high tensile strength thermoplastic polymer fibers. Polyamide (PA) fibers with different draw ratios, with and without CNTs as fillers, and having mechanical properties close to industrial standards were spun in a pilot melt spinning plant. The morphology of the fibers was investigated using optical microscopy, nuclear magnetic resonance (NMR) and 2-D wide angle x-ray diffraction (WAXD). Differential scanning calorimetry (DSC) was carried out to get an estimate of the crystallinity. For a concise interpretation of the results of the tensile measurements performed on the fibers, a parameter was developed to account for the detrimental influence of polymer extrusion on their mechanical properties. The CNTs seemed to act as sites for the growth of un-oriented crystalline domains converted from oriented regions, without yielding a mechanical reinforcing effect.

Microstructural characterization and wear properties of ultra-dispersed nanodiamond (UDD) reinforced Al matrix composites fabricated by ball-milling and sintering

2011 ◽  
Vol 46 (13) ◽  
pp. 1521-1534 ◽  
Author(s):  
H Kaftelen ◽  
ML Öveçoğlu
Keyword(s):  
Wear Resistance ◽  
Ball Milling ◽  
Microstructural Characterization ◽  
Matrix Composites ◽  
X Ray Diffraction ◽  
Wear Properties ◽  
X Ray ◽  
Al Matrix Composites ◽  
Al Matrix Composite ◽  
Al Matrix

Elemental aluminum (Al) powders reinforced with 1–10 wt% of ultra-dispersed nanodiamond (UDD) powders were ball-milled in a SpexTM Mixer/Mill between 0 and 120 min followed by consolidation and sintering. X-ray diffraction analyses on the ball-milled powders revealed only α-Al peaks, whereas Al4C3 phase was identified along with α-Al in all sintered composites. Increasing the addition of nanodiamond to Al-matrix resulted in improved hardness of both ball-milled and sintered composites. The wear resistances of the Al-UDD composites were significantly improved with increasing UDD contents. Under similar load and sliding conditions, the wear resistance of Al matrix composite containing 10 wt% nanodiamond enhances about 40 times when compared with unreinforced aluminum.

Processing of Biodegradable Polymer Composite Using Soy Protein-Based Resin and Nanoclay

2016 ◽  
Author(s):  
Mohammad K. Hossain ◽  
Samira N. Shaily ◽  
Hadiya J. Harrigan ◽  
Terrie Mickens
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Optical Microscopy ◽  
Soy Protein ◽  
Poly Vinyl Alcohol ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Scanning Electron

A completely biodegradable composite was fabricated from an herbal polymer, soy protein concentrate (SPC) resin. Soy protein was modified by adding 30 wt% of glycerol and 5 wt% of poly vinyl alcohol (PVA) to enhance its mechanical as well as thermal property. 3%, 5%, 10%, and 20% nanoclay (NC) were infused into the system. To evaluate its mechanical properties, crystallinity, thermal properties, bonding interaction, and morphological evaluation, tensile, X-ray diffraction (XRD), thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), and Fourier transform infrared spectroscopy (FTIR) tests, and optical microscopy (OM) and scanning electron microscopy (SEM) evaluation were performed. Tensile tests showed that the addition of nanoclay improved the mechanical properties of the modified resin. Soy protein is hydrophilic due to the presence of amino acids that contain various polar groups such as amine, carboxyl, and hydroxyl. As a result, polar nanoclay particles that are exfoliated can be evenly dispersed in the SPC resin. From experimental results, it is clear that adding of nanoclay with SPC resin significantly increased the stiffness of the SPC resin. A combination of 5% clay, 30% glycerol, and 5% PVA with the modified SPC resulted in the maximum stress of 18 MPa and Young modulus of 958 MPa. The modified SPC showed a reduced failure strain as well. X-ray diffraction curves showed an improvement of crystallinity of the prepared resin with increasing amount of nanoclay. Interaction among soy, glycerol, PVA, and nanoclay was clearly demonstrated from the FTIR analysis. Optical microscopy (OM) and scanning electron microscopy (SEM) micrographs revealed rougher surface in the nanoclay infused SPC samples compared to that of the neat one. SEM evaluation revealed rougher fracture surface in the NC infused samples.

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