scholarly journals Durability Improvement of Concentrated Polymer Brushes by Multiscale Texturing

Author(s):  
Seiya Watanabe ◽  
Eri Kodama ◽  
Chiharu Tadokoro ◽  
Keita Sakakibara ◽  
Ken Nakano ◽  
...  

Abstract Concentrated polymer brushes (CPBs) are promising soft-material coatings for improving tribological properties under severe sliding conditions, even in the macroscopic scale. Therefore, they are expected to be applied to mechanical sliding components. However, the durability of CPBs has remained challenging for industrial applications. Previous studies revealed that applying a groove texture to the CPB substrate is effective in improving the durability of CPBs. In order to achieve further improvement of durability of CPBs, we attempted to apply the periodical structure, which is a microfabricated structure corresponding to a surface roughness 0.02 μm, whereas the groove texture applied in previous studies has widths and depths in micrometres. In this study, the effect of the nano-periodic structure in addition to the groove texture applied to the CPB substrate on the durability of CPB is investigated. The results demonstrate a significant improvement in the durability of CPBs by up to 90% compared with non-textured CPB when an appropriate nano-periodic structure is applied (i.e. a nano-periodic structure oriented parallel to the groove texture).

Author(s):  
Florian Kuisat ◽  
Fernando Lasagni ◽  
Andrés Fabián Lasagni

AbstractIt is well known that the surface topography of a part can affect its mechanical performance, which is typical in additive manufacturing. In this context, we report about the surface modification of additive manufactured components made of Titanium 64 (Ti64) and Scalmalloy®, using a pulsed laser, with the aim of reducing their surface roughness. In our experiments, a nanosecond-pulsed infrared laser source with variable pulse durations between 8 and 200 ns was applied. The impact of varying a large number of parameters on the surface quality of the smoothed areas was investigated. The results demonstrated a reduction of surface roughness Sa by more than 80% for Titanium 64 and by 65% for Scalmalloy® samples. This allows to extend the applicability of additive manufactured components beyond the current state of the art and break new ground for the application in various industrial applications such as in aerospace.


Author(s):  
Gabriele Piscopo ◽  
Alessandro Salmi ◽  
Eleonora Atzeni

AbstractThe production of large components is one of the most powerful applications of laser powder-directed energy deposition (LP-DED) processes. High productivity could be achieved, when focusing on industrial applications, by selecting the proper process parameters. However, it is of crucial importance to understand the strategies that are necessary to increase productivity while maintaining the overall part quality and minimizing the need for post-processing. In this paper, an analysis of the dimensional deviations, surface roughness and subsurface residual stresses of samples produced by LP-DED is described as a function of the applied energy input. The aim of this work is to analyze the effects of high-productivity process parameters on the surface quality and the mechanical characteristics of the samples. The obtained results show that the analyzed process parameters affect the dimensional deviations and the residual stresses, but have a very little influence on surface roughness, which is instead dominated by the presence of unmelted particles.


2014 ◽  
Vol 2014 ◽  
pp. 1-7 ◽  
Author(s):  
Jinlong Jiang ◽  
Qiong Wang ◽  
Yubao Wang ◽  
Zhang Xia ◽  
Hua Yang ◽  
...  

The titanium- and silicon-codoped a-C:H films were prepared at different applied bias voltage by magnetron sputtering TiSi target in argon and methane mixture atmosphere. The influence of the applied bias voltage on the composition, surface morphology, structure, and mechanical properties of the films was investigated by XPS, AFM, Raman, FTIR spectroscopy, and nanoindenter. The tribological properties of the films were characterized on an UMT-2MT tribometer. The results demonstrated that the film became smoother and denser with increasing the applied bias voltage up to −200 V, whereas surface roughness increased due to the enhancement of ion bombardment as the applied bias voltage further increased. The sp3carbon fraction in the films monotonously decreased with increasing the applied bias voltage. The film exhibited moderate hardness and the superior tribological properties at the applied bias voltage of −100 V. The tribological behaviors are correlated to the H/E or H3/E2ratio of the films.


Author(s):  
M.N. Obaid ◽  
S.H. Radhi

Purpose: The number of people suffering from Degenerative Disc Disease (DDD) is increasing. The disease causes heavy pain and restrict a number of day-to-day life activities. In extreme cases, the degraded disc is removed under total disc replacement which is usually made up of Ultra-High Molecular Weight Polyethylene (UHMWPE). The material has astounding biocompatible characteristics mechanical properties and wear resistance. However, these characteristics are insufficient in arthroplasty application. Therefore, research investigations are ongoing to improve tribological properties through reinforcement that may result in a composite material of UHMWPE. Thus the current study is aimed at reinforcing UHMWPE with short fibres of polyesters to enhance the tribological properties and surface characteristic so as to improve wear resistance and nourish the fibroblast cells on synthetic disc. Design/methodology/approach: The researcher prepared UHMWPE composite material, reinforced with different weight fractions of short polyester fibres (2, 4, 6, 8 and 10% following hot press method. Further pin-on-disc device was used to study the tribological properties (coefficient of friction and volume of wear). The study tested surface roughness and surface characteristics by atomic force microscopy (AFM) device, hardness by shore D device, contact angle to study the effect of polyester short fibres on wettability of UHMWPE surface and tested the thermal properties and crystalline degree using Differential Scanning Calorimetry measurement (DSC) device. Findings: The results infer that the wear resistance got improved when using 2% w.t polyester though it got decreased initially. However, the value was still more than neat UHMWPE. There was a decrease observed in coefficient of friction, but after 4 w.t% polyester, the coefficient of friction got increased due to increasing percentage of fibres which make it harder and stiff compared to UHMWPE. There was a decline observed in surface roughness due to alignment of the fibres with smooth surface. The contact angle got increased in a moderate range while the roughness enhanced the growth of fibroblast cell. The hardness of composite material got increased, because the fibres turned stiffer and harder than the matrix. DSC results infer the improvements in thermal stability due to high thermal properties of polyester fibres compared to UHMWPE. The degree of crystallinity got increased which in turn enhanced wear resistance, especially at 6 w.t % polyester fibres. There was a mild increase observed in density since the density of polyester is higher than polymer. Research limitations/implications: The major challenge was the dispersion of fibres. Uniform distribution of fibres within the matrix (UHMWPE) was achieved through two steps of mixing processes such as mechanical mixture and twin extruder. In future studies, fatigue tests must be conducted to study the behaviour of prepared composite materials under fatigue cycle. Practical implications: A significant objective is how to connect among different properties to obtain good improvement in tribological and surface properties so as to enhance wear resistance and growth of fibrolase cells. Originality/value: In this study, polymeric short fibres were used as reinforcement with polymeric matrix to enhance the wettability of fibres with matrix. In this way, the bonding among them got increased which supports the tribological, surface, and crystalline behaviour.


2017 ◽  
Vol 140 (3) ◽  
Author(s):  
Wei Pu ◽  
Dong Zhu ◽  
Jiaxu Wang

In this study, a modified mixed lubrication model is developed with consideration of machined surface roughness, arbitrary entraining velocity angle, starvation, and cavitation. Model validation is executed by means of comparison between the obtained numerical results and the available starved elastohydrodynamic lubrication (EHL) data found from some previous studies. A comprehensive analysis for the effect of inlet oil supply condition on starvation and cavitation, mixed EHL characteristics, friction and flash temperature in elliptical contacts is conducted in a wide range of operating conditions. In addition, the influence of roughness orientation on film thickness and friction is discussed under different starved lubrication conditions. Obtained results reveal that inlet starvation leads to an obvious reduction of average film thickness and an increase in interasperity cavitation area due to surface roughness, which results in significant increment of asperity contacts, friction, and flash temperature. Besides, the effect of entrainment angle on film thickness will be weakened if the two surfaces operate under starved lubrication condition. Furthermore, the results show that the transverse roughness may yield thicker EHL films and lower friction than the isotropic and longitudinal if starvation is taken into account. Therefore, the starved mixed EHL model can be considered as a useful engineering tool for industrial applications.


Author(s):  
C-T Duong ◽  
J-S Nam ◽  
E-M Seo ◽  
B P Patro ◽  
J-D Chang ◽  
...  

The tribological properties of engineering and biological materials have been investigated at microscale levels through the calculation of the surface roughness and frictional coefficient using atomic force microscopy (AFM). Although a number of previous studies have reported the frictional coefficients of diverse bearing materials in total hip arthroplasty (THA), the relationship between the surface roughness and frictional coefficient of bearing materials of THA have not been reported, and furthermore, the tribological properties for different wear regions of a cobalt-chromium (Co—Cr) femoral head have not been well identified. Therefore, the objective of this study is to investigate the relationships between the surface roughness, frictional coefficient, and hardness for both the main-wear and the least-wear regions of a Co—Cr femoral head 10 years after THA. The average Vickers hardness of the Co—Cr femoral head was 380.7 ± 11.3 HV. With the scanned area of 25 μm×25 μm through AFM, the frictional coefficients of the main-wear and the least-wear regions were 0.229 ± 0.054 and 0.243 ± 0.059, respectively, and showed no statistical differences between these two regions ( p = 0.449). However, differences in the surface roughness ( Rq) between the main-wear region ( Rq = 96.5 ± 26.2 nm) and the least-wear region ( Rq = 17.7 ± 4.2 nm) were statistically significant ( p<0.0001). The results of the current study suggest that the frictional property of the Co—Cr femoral head is not significantly correlated with its surface roughness, and also provide guidelines for improving the surface characteristics of metallic implant materials.


1994 ◽  
Vol 367 ◽  
Author(s):  
T. Yoshinobu ◽  
A. Iwamoto ◽  
K. Sudoh ◽  
H. Iwasaki

AbstractThe scaling behavior of the surface roughness of a-and poly-Si deposited on Si was investigated by atomic force microscopy (AFM). The interface width W(L), defined as the rms roughness as a function of the linear size of the surface area, was calculated from various sizes of AFM images. W(L) increased as a power of L with the roughness exponent ∝ on shorter length scales, and saturated at a constant value of on a macroscopic scale. The value of roughness exponent a was 0.48 and 0.90 for a-and poly-Si, respectively, and σ was 1.5 and 13.6nm for 350nm-thick a-Si and 500nm-thick poly-Si, respectively. The AFM images were compared with the surfaces generated by simulation.


2020 ◽  
Vol 62 (12) ◽  
pp. 1243-1250
Author(s):  
Fahri Vatansever ◽  
Alpay Tamer Erturk ◽  
Erol Feyzullahoglu

Abstract In this study, the tribological properties of 7075 aluminum alloy produced by ultrasonic melt treatment (UST) are investigated. Tribological properties of untreated and ultrasonically treated samples under dry and lubricated sliding conditions were analyzed experimentally by the block on ring test method. Worn surfaces of untreated and ultrasonically treated samples were scanned by 3D optical profilometer and analyzed to search out wear characteristics in the material. Furthermore, microstructural examinations were conducted to investigate the beneficial effects of UST on the microstructural properties of the alloy using optical and scanning electron microscopy. According to the results obtained, UST refines the α-Al phase of the alloy and disperses precipitates to grain boundaries more uniformly. Also, hardness and density of the alloy increased through the effect of UST. Due to these favorable effects, the wear resistance of the alloy increased and the worn surfaces of the ultrasonically treated samples exhibited lower surface roughness according to 3D surface roughness measurements.


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