scholarly journals Effect of the Particle Size of Al/Ni Multilayer Powder on the Exothermic Characterization

Materials ◽  
2020 ◽  
Vol 13 (19) ◽  
pp. 4394
Author(s):  
Shugo Miyake ◽  
Taisei Izumi ◽  
Rino Yamamoto

In this study, the exothermic temperature performance of various Al/Ni multilayer powders with particle sizes ranging from under 75 to over 850 µm, which generate enormous heat during self-propagating exothermic reactions, was determined using a high-speed sampling pyrometer. The Al/Ni multilayer powders were prepared by a cold-rolling and pulverizing method. The multilayer constitution of the Al/Ni multilayer powders was examined by observing the cross-section of the powders using scanning electron microscopy; the results indicate that the powders had similar lamellar structures regardless of the particle size. Exothermic reactions were carried out to measure the temperature changes during the experiment using a pyrometer. We found that the maximum temperature and the duration of the exothermic reaction increased with an increase in the particle size caused by the heat dissipation of the surface area of the Al/Ni multilayer powder. This indicates that the thermal characteristics of the exothermic reaction of the Al/Ni multilayer powder can be controlled by adjusting the particle size of the Al/Ni multilayer powder. Finally, we concluded that this controllability of the exothermic phenomenon can be applied as a local heating source in a wide range of fields.

2021 ◽  
Author(s):  
Fan Kai-Guo ◽  
Rongfei Xu ◽  
Ruoda Wang ◽  
Rui Gao

Abstract With the development of motorized spindle, the cooling effect and the distribution of cooling capacity become the crucial problem of cooling system. An optimization method for ThermoElectric-based Cooling System (TECS) is proposed based on the conservation of energy to distribute the cooling capacity. The main strategy of the proposed optimization method is to make the cold and heat input at different regions of the spindle sleeve equal in real-time through optimizing the contact area between the Heat Conduction Sleeve (HCS) and spindle sleeve. The numerical simulation and thermal characteristics experiments are carried to verify the effect of the proposed optimization method and the TECS. The simulation and experimental results show that the maximum temperature rise and thermal elongation of the TECS-based motorized spindle are reduced 56.7% and 58.6% compared with water-cooled motorized spindle, and the temperature distribution of the spindle sleeve is more uniform. It is meaningful to improve the accuracy of motorized spindle.


2019 ◽  
Vol 5 (2) ◽  
pp. 16-30
Author(s):  
Weili Li ◽  
Junci Cao ◽  
Dong Li ◽  
Zhigang Wu

Background: Aiming at the problems of high local temperature and uneven temperature distribution in asynchronous traction motor of high-speed Electric Multiple Unit (EMU) when it is running. Aim: In this paper, the influence of ventilation system with different structure on temperature distribution is studied. Methods: Taking 600kW asynchronous traction motor as an example, the electromagnetic-fluid-temperature analysis model of the traction motor is established, and the temperature values of different positions in the motor are obtained. The accuracy of the calculation results is verified by comparing with the actual measurement. On this basis, by adjusting the structure of stator and rotor axial ventilation holes, the relationship between temperature distribution and fluid flow state in motor is studied. In addition, the influence of fluid incidence angle on fluid velocity and heat dissipation performance of motor is also studied, and the ventilation structure scheme with relative balance of axial and circumferential temperature in motor is found out, which provides a reference strategy for the design of temperature rise of motor with forced ventilation structure. Results: The wind speed near the intake side of stator teeth and rotor teeth groove is less than that far from the intake side. The flow distribution trend of rotor vent is similar to that of stator vent, but the air in the groove is affected by centrifugal force of rotor rotation, which makes the wind speed difference on the intake side larger than that on the outlet side. The stator winding and rotor guide bar are affected by wind temperature to reach the maximum temperature at the end of the outlet respectively. The stator core is higher at the windward side and the leeward side than the other parts of the motor. The heat dissipation effect at both ends is good. The highest temperature of the stator core appears near the leeward side.


Author(s):  
E.D. Wolf

Most microelectronics devices and circuits operate faster, consume less power, execute more functions and cost less per circuit function when the feature-sizes internal to the devices and circuits are made smaller. This is part of the stimulus for the Very High-Speed Integrated Circuits (VHSIC) program. There is also a need for smaller, more sensitive sensors in a wide range of disciplines that includes electrochemistry, neurophysiology and ultra-high pressure solid state research. There is often fundamental new science (and sometimes new technology) to be revealed (and used) when a basic parameter such as size is extended to new dimensions, as is evident at the two extremes of smallness and largeness, high energy particle physics and cosmology, respectively. However, there is also a very important intermediate domain of size that spans from the diameter of a small cluster of atoms up to near one micrometer which may also have just as profound effects on society as “big” physics.


Author(s):  
C. J. Chan ◽  
K. R. Venkatachari ◽  
W. M. Kriven ◽  
J. F. Young

Dicalcium silicate (Ca2SiO4) is a major component of Portland cement. It has also been investigated as a potential transformation toughener alternative to zirconia. It has five polymorphs: α, α'H, α'L, β and γ. Of interest is the β-to-γ transformation on cooling at about 490°C. This transformation, accompanied by a 12% volume increase and a 4.6° unit cell shape change, is analogous to the tetragonal-to-monoclinic transformation in zirconia. Due to the processing methods used, previous studies into the particle size effect were limited by a wide range of particle size distribution. In an attempt to obtain a more uniform size, a fast quench rate involving a laser-melting/roller-quenching technique was investigated.The laser-melting/roller-quenching experiment used precompacted bars of stoichiometric γ-Ca2SiO4 powder, which were synthesized from AR grade CaCO3 and SiO2xH2O. The raw materials were mixed by conventional ceramic processing techniques, and sintered at 1450°C. The dusted γ-Ca2SiO4 powder was uniaxially pressed into 0.4 cm x 0.4 cm x 4 cm bars under 34 MPa and cold isostatically pressed under 172 MPa. The γ-Ca2SiO4 bars were melted by a 10 KW-CO2 laser.


2019 ◽  
Vol 56 (4) ◽  
pp. 750-758
Author(s):  
Nicolae Navodariu ◽  
Mihai Branzei ◽  
Robert Ciocoiu ◽  
Ion Ciuca ◽  
Razvan Coman ◽  
...  

Flame straightening is a technology process used to eliminate deformations. This method relies on local heating of the material to correct geometry or damaged parts. In the local automobile services its main use is for repairs of less critical deformed components. The maximum temperature and thermal gradient, heating time, cooling rate and number of heating cycles affect the mechanical properties since local heating can alter material microstructure. The aim of this research was to determine the mechanical characteristics of thin steel plates repaired by local heating associated with plastic deformation (similar to hot working) and cold straightening (similar to local cold working) for automotive side and door panels made of structural steel. Thin sheet plates, 0.9mm thickness, were deformed by impact and repaired by local heating using the flame and induction heating then plastically deformed while hot as well as straightened without heating. The heat repaired samples were studied by light microscopy to determine microstructure change and samples were tensile tested to determine their mechanical characteristics. Local excessive grain growth generates anisotropy, the assembly behaves as a composite material with regions that show significant plastic deformations while others little or no deformations at al. Without procedures adjusted to each material repairs involving heating are to be avoided, cold working should be employed when replacement is not possible.


2020 ◽  
Vol 10 (4) ◽  
pp. 404-418
Author(s):  
Kruti Borderwala ◽  
Ganesh Swain ◽  
Namrata Mange ◽  
Jaimini Gandhi ◽  
Manisha Lalan ◽  
...  

Background: The objective of this study was to develop solid lipid nanoparticles (SLNs) of poorly water soluble anti-hyperlipidemic drugs-Ezetimibe in combination with Simvastatin. Methods: This study describes a 32 full factorial experimental design to optimize the formulation of drug loaded lipid nanoparticles (SLN) by the high speed homogenization technique. The independent variables amount of lipid (GMS) and amount of surfactant (Poloxamer 188) were studied at three levels and arranged in a 32 factorial design to study the influence on the response variables- particle size, % entrapment efficiency (%EE) and cumulative drug release (% CDR) at 24 h. Results: The particle size, % EE and % CDR at 24 h for the 9 batches (B1 to B9) showed a wide variation of 104.6-496.6 nm, 47.80-82.05% (Simvastatin); 48.60-84.23% (Ezetimibe) and 54.64-92.27% (Simvastatin); 43.8-97.1% (Ezetimibe), respectively. The responses of the design were analysed using Design Expert 10.0.2. (Stat-Ease, Inc, USA), and the analytical tools of software were used to draw response surface plots. From the statistical analysis of data, polynomial equations were generated. Optimized formulation showed particle size of 169.5 nm, % EE of 75.43% (Simvastatin); 79.10% (Ezetimibe) and 74.13% (Simvastatin); 77.11% (Ezetimibe) %CDR after 24 h. Thermal analysis of prepared solid lipid nanoparticles gave indication of solubilisation of drugs within lipid matrix. Conclusion: Fourier Transformation Infrared Spectroscopy (FTIR) showed the absence of new bands for loaded solid lipid nanoparticles indicating no interaction between drugs and lipid matrix and being only dissolved in it. Electron microscope of transmission techniques indicated sphere form of prepared solid lipid nanoparticles with smooth surface with size approximately around 100 nm.


2020 ◽  
Vol 02 ◽  
Author(s):  
Laurel Stringer ◽  
Sarah Malley ◽  
Darrell M. Hutto ◽  
Jason A. Griggs ◽  
Susana M. Salazar Marocho

Background: The most common approach to remove yttria stabilized zirconia (YSZ) fixed-dental prostheses (FDPs) is by means of diamond burs attached to a high-speed handpiece. This process is time-consuming and destructive. The use of lasers over mechanical instrumentation for removal of FDPs can lead to efficient and predictable restoration retrievability. However, the heat produced might damage the tooth pulp (>42˚C). Objective: The purpose of this study was to determine the maximum temperature (T) reached during the use of different settings of the erbium, chromium:yttrium-scandium-gallium-garnet Er,Cr:YSGG laser through a YSZ ceramic. Methods: YSZ slices (1 mm thick) were assigned into 7 groups. For the control group, a diamond bur was used to cut a 1 mm groove into the YSZ slices. For the 6 experimental groups, the laser was operated at a constant combination of 33% water and 66% air during 30 s with two different power settings (W) at three frequencies (PPS), as follows (W/PPS): 2.5/20, 2.5/30, 2.5/45, 4.5/20, 4.5/30, 4.5/45. The T through the YSZ slice was recorded in degrees Celsius by using a digital thermometer with a K thermocouple. Results: The median T of the control group was 26.5˚C. The use of 4.5 W resulted in the median T (˚C) of 44.2 at 20 PPS, 53.3 at 30 PPS, and 58.9 at 45 PPS, while 2.5 W showed 34.6, 31.6, and 25.0 at 20, 30, and 45 PPS, respectively. KruskalWallis one-way ANOVA showed that within each power setting, the T was similar. The high power and lowest frequency (4.5/20) showed no significant difference from the 2.5 W settings and the control group. Conclusion: The lower power setting (2.5 W) is a potential method for the use of the Er,Cr:YSGG laser to debond YSZ structures. The higher power (4.5 W) with high frequencies (30 and 45 PPS) is unsuitable.


1999 ◽  
Vol 29 ◽  
pp. 151-154 ◽  
Author(s):  
Crescenzo Festa ◽  
Aristide Rossi

AbstractAn apparatus is described for measuring the thermal conductivity of ice by the transient hot-wire method. Thermal conductivity A, is determined by tracking the thermal pulse induced in the sample by a heating source consisting of a platinum resistor. A central segment of the same platinum heating resistor acts also as a thermal sensor. A heat pulse transferred to the ice for a period of 40s gives a maximum temperature increment of about 7-14°C. In good experimental conditions, the expected reproducibility of the measurements is within ±3%. The accuracy of the method depends on whether the instrument has been calibrated by reliable standard samples, certified by absolute methods.


Proceedings ◽  
2020 ◽  
Vol 65 (1) ◽  
pp. 25
Author(s):  
Antonio Garrido Marijuan ◽  
Roberto Garay ◽  
Mikel Lumbreras ◽  
Víctor Sánchez ◽  
Olga Macias ◽  
...  

District heating networks deliver around 13% of the heating energy in the EU, being considered as a key element of the progressive decarbonization of Europe. The H2020 REnewable Low TEmperature District project (RELaTED) seeks to contribute to the energy decarbonization of these infrastructures through the development and demonstration of the following concepts: reduction in network temperature down to 50 °C, integration of renewable energies and waste heat sources with a novel substation concept, and improvement on building-integrated solar thermal systems. The coupling of renewable thermal sources with ultra-low temperature district heating (DH) allows for a bidirectional energy flow, using the DH as both thermal storage in periods of production surplus and a back-up heating source during consumption peaks. The ultra-low temperature enables the integration of a wide range of energy sources such as waste heat from industry. Furthermore, RELaTED also develops concepts concerning district heating-connected reversible heat pump systems that allow to reach adequate thermal levels for domestic hot water as well as the use of the network for district cooling with high performance. These developments will be demonstrated in four locations: Estonia, Serbia, Denmark, and Spain.


2021 ◽  
Author(s):  
Eric J Snider ◽  
Lauren E Cornell ◽  
Brandon M Gross ◽  
David O Zamora ◽  
Emily N Boice

ABSTRACT Introduction Open-globe ocular injuries have increased in frequency in recent combat operations due to increased use of explosive weaponry. Unfortunately, open-globe injuries have one of the worst visual outcomes for the injured warfighter, often resulting in permanent loss of vision. To improve visual recovery, injuries need to be stabilized quickly following trauma, in order to restore intraocular pressure and create a watertight seal. Here, we assess four off-the-shelf (OTS), commercially available tissue adhesives for their ability to seal military-relevant corneal perforation injuries (CPIs). Materials and Methods Adhesives were assessed using an anterior segment inflation platform and a previously developed high-speed benchtop corneal puncture model, to create injuries in porcine eyes. After injury, adhesives were applied and injury stabilization was assessed by measuring outflow rate, ocular compliance, and burst pressure, followed by histological analysis. Results Tegaderm dressings and Dermabond skin adhesive most successfully sealed injuries in preliminary testing. Across a range of injury sizes and shapes, Tegaderm performed well in smaller injury sizes, less than 2 mm in diameter, but inadequately sealed large or complex injuries. Dermabond created a watertight seal capable of maintaining ocular tissue at physiological intraocular pressure for almost all injury shapes and sizes. However, application of the adhesive was inconsistent. Histologically, after removal of the Dermabond skin adhesive, the corneal epithelium was removed and oftentimes the epithelium surface penetrated into the wound and was adhered to inner stromal tissue. Conclusions Dermabond can stabilize a wide range of CPIs; however, application is variable, which may adversely impact the corneal tissue. Without addressing these limitations, no OTS adhesive tested herein can be directly translated to CPIs. This highlights the need for development of a biomaterial product to stabilize these injuries without causing ocular damage upon removal, thus improving the poor vision prognosis for the injured warfighter.


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