scholarly journals Microstructure Evolution and Mechanical Properties of As-Cast and As-Compressed ZM6 Magnesium Alloys during the Two-Stage Aging Treatment Process

Materials ◽  
2021 ◽  
Vol 14 (24) ◽  
pp. 7760
Author(s):  
Jia Fu ◽  
Su Chen
Keyword(s):  
Mechanical Properties ◽  
Yield Strength ◽  
Grain Boundary ◽  
Aging Process ◽  
Treatment Process ◽  
Phase Particle ◽  
Aging Treatment ◽  
Grain Boundary Sliding ◽  
Second Phase ◽  
Two Stage

In the present study, different solid solution and aging processes of as-cast and as-compressed ZM6 (Mg2.6Nd0.4Zn0.4Zr) alloy were designed, and the microstructure and precipitation strengthening mechanisms were discussed. After the pre-aging treatment, a large amount of G.P. zones formed in the α-Mg matrix over the course of the subsequent secondary G.P. prescription, where the fine and dispersed Mg12(Nd,Zn) phases were precipitated at the grain boundaries. The pre-aging and secondary aging processes resulted in the Mg12(Nd, Zn) phase becoming globular, preventing grain boundary sliding and decreasing grain boundary diffusion. Meanwhile, precipitation phase â″(Mg3Nd) demonstrated a coherent relationship with the α-Mg matrix after the pre-aging process, and after the secondary aging phase, Mg12Nd increases and became semi-coherent in the matrix. Compared to an as-cast ZM6 alloy, the yield strength of the as-compressed ZM6 alloy increased sharply due to an increase in the yield strength that was proportional to the particle spacing, where the dislocation bypassed the second phase particle. Compared to the single-stage aging process, the two-stage aging process greatly improved the mechanical properties of both the as-cast and as-compressed ZM6 alloys. The difference between the as-cast and as-compressed states is that an as-compressed ZM6 alloy with more dislocations and twins has more dispersed precipitates in the G.P. zones after secondary aging, meaning that it is greatly strengthened after the two-stage aging treatment process.

Functional Gradation in Precipitation Hardenable AA7075 Alloy by Differential Cooling Strategies

2021 ◽  
Vol 883 ◽  
pp. 159-166
Author(s):  
Emad Scharifi ◽  
Moritz Roscher ◽  
Steffen Lotz ◽  
Ursula Weidig ◽  
Eric Jägle ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Phase Particle ◽  
Hot Stamping ◽  
Aging Treatment ◽  
Tensile Tests ◽  
Uniaxial Tensile ◽  
Material Strength ◽  
Second Phase ◽  
Contrast Imaging ◽  
Forming Tools

Inspired by steel forming strategies, this study focuses on the effect of differential cooling on mechanical properties and precipitation kinetics during hot stamping of high strength AA7075 alloy. For this aim, different forming strategies were performed using segmented and differentially heated forming tools to provide locally tailored microstructures. Upon processing, uniaxial tensile tests and hardness measurements were used to characterize the mechanical properties after the aging treatment. Microstructure investigations were conducted to examine the strengthening mechanisms using the electron channeling contrast imaging (ECCI) technique in a scanning electron microscope (SEM). Based on the obtained results, it can be deduced that the tool temperatures play a key role in influencing the mechanical properties. Lower tool temperatures result in higher material strength and higher tool temperatures in lower mechanical properties. By changing the cooling rate with the use of differently heated forming tools, the mechanical properties can be controlled. Microstructure investigations revealed the formation of very fine and homogeneously distributed particles at cooled zones, which were associated with elevated mechanical properties due to the suppression of second phase particle formation during cooling. In contrast, coarse particles were observed at lower cooling rates, explaining the lower material strength found in these zones.

Study on Aging Treatment Microstructure of Magnesium-Zinc Alloy

2017 ◽  
Vol 748 ◽  
pp. 250-253
Author(s):  
Zhi Ling Wang
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Grain Boundary ◽  
Aging Treatment ◽  
Experimental Results ◽  
Zinc Alloy ◽  
Second Phase ◽  
Zn Alloy

In this paper, the aging treatment is performed to Mg-Zn alloy with different Zinc contents,the effect of aging treatment on the microstructure of Mg-Zn alloy was studied. The experimental results show that Zinc precipitated from the mg substrate, and exists in the form of Mg-Zn phase after aging treatment of Mg-Zn alloy, which greatly improves the Mg-Zn alloy's mechanical properties. After heat treatment of Mg-Zn alloy, the second phase along the grain boundary changes from the patch distribution to the network distribution with the increase of the content of Zn.

Effect of Aging Treatment on Properties and Microstructure of an Al-7.5Zn-1.3Mg-1.4Cu-0.12Zr Alloy

2010 ◽  
Vol 638-642 ◽  
pp. 273-278 ◽  
Author(s):  
Xi Wu Li ◽  
Bai Qing Xiong ◽  
Yon Gan Zhang ◽  
Guo Jun Wang ◽  
Zhi Hui Li ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Electrical Conductivity ◽  
Grain Boundary ◽  
Response Rate ◽  
Aging Treatment ◽  
Aging Response ◽  
Peak Aging

In this study, the effect of various aging treatment (T6 and T7 treatment) on the mechanical properties, electrical conductivity and the microstructure of an Al-7.5Zn-1.3Mg-1.4Cu-0.12Zr alloy has been investigated. The results show that with elevating the aging treatment temperatures, the aging response rate is greatly accelerated. When T6 temper is performed at 140°C for 12h, as compared to peak aging for 24h at 120°C, the UTS and the corresponding Elongation values keep the same level, whereas the TYS and the electrical conductivity obviously increase by 5% and 9%, which is up to 560 MPa and 22.6 MS/m, respectively. And there are clear PFZs along the grain boundary and slightly coarser precipitates inside the grain. GPI zones, GPII zones and η' phases are major precipitates for the alloy under T6 condition. When T7 temper is performed on the alloy, the main precipitates are GPII zones, η′ and η phases. The coarser precipitates inside the grain and discontinuous grain boundary precipitates are favorable to electrical conductivity, which decrease the strength of 5~17% compared to T6 treatment. After T76 treatment (i.e., 110°C/6 h + 160°C/6 h), the UTS, TYS, Elongation and electrical conductivity values were 540 MPa, 510 MPa, 16.7% and 23.5 MS/m, respectively.

scholarly journals Effect of Dissolution of η′ Precipitates on Mechanical Properties of A7075-T6 Alloy

2022 ◽  
Vol 60 (1) ◽  
pp. 83-93
Author(s):  
Young-We Kim ◽  
Yong-Hee Jo ◽  
Yun-Soo Lee ◽  
Hyoung-Wook Kim ◽  
Je-In Lee
Keyword(s):  
Mechanical Properties ◽  
Yield Strength ◽  
Solution Treatment ◽  
Aluminum Matrix ◽  
Natural Aging ◽  
Aging Treatment ◽  
Nucleation Site ◽  
Treatment Temperature ◽  
Solution Treatment Temperature ◽  
Bake Hardening

The effects of dissolution of the η′ phase by solution treatment on the mechanical properties of A7075-T6 alloy were investigated. Immediately after solution treatment of the T6 sheet at 450 oC or higher, elongation significantly increased and dissolution of the η′ phase occurred. η′ is the main hardening phase. After natural-aging, GPI, which is coherent with the aluminum matrix, was formed and strength increased. When bake hardening after natural-aging was performed, the yield strength slightly increased due to partial dissolution of the GPI and re-precipitation of the η′ phase. In contrast, after solution treatment at 400 oC, there was less elongation increase due to the precipitation of the coarse η phase at grain boundaries and low dissolution of the η′ phase. In addition, when bake hardening after natural-aging was performed, the yield strength decreased due to insufficient GPI, which is the nucleation site of the η′ phase. To promote reprecipitation of the η′ phase, the solution treatment temperature was set to a level that would increase solubility. As a result, the yield strength was significantly increased through re-precipitation of a large number of fine and uniform η′ phase. In addition, to increase the effect of dissolution, a pre-aging treatment was introduced and the bake hardenability can be improved after dissolution.

Research on Micro-Mechanism of Nanocomposite Ceramic in Two-Dimensional Ultrasound Grinding

2007 ◽  
Vol 359-360 ◽  
pp. 344-348 ◽  
Author(s):  
Bo Zhao ◽  
Yan Wu ◽  
Guo Fu Gao ◽  
Feng Jiao
Keyword(s):  
Grain Boundary ◽  
Grain Boundaries ◽  
Deformation Mechanism ◽  
Ground Surface ◽  
Grain Boundary Sliding ◽  
Second Phase ◽  
Two Dimensional ◽  
Composite Ceramics ◽  
Nano Composite ◽  
Boundary Sliding

Surface microstructure of nano-composite ceramics prepared by mixed coherence system and machined by two-dimensional ultrasonic precision grinding was researched using TEM, SEM, XRD detector and other equipments. Structure, formation mechanism and characteristic of metamorphic layer of ground surface of nano-composite ceramics were researched. The experiment shows micro deformation mechanism of ceramic material in two-dimensional ultrasound grinding is twin grain boundary and grain-boundary sliding for Al2O3, and it is crystal dislocation of enhanced phase, matrix grain boundary sliding, coordination deformation of intergranular second phase as well as its deformation mechanism for nano-composite ceramics. The fracture surfaces of nano-composite materials with different microscopic structure were observed using TEM and SEM. Research shows that ZrO2 plays an important influence on the generation and expansion of crack, and enhances the strength of grain boundaries. When grain boundaries is rich in the ZrO2 particles, the crack produced in grinding process will be prevented, and the surface with plastic deformation will be smooth. The results shows nanoparticles dispersed in grain boundary prevents crack propagation and makes materials fracture transgranularly which makes the processed surface fine.

Study on Hardening Potential of Isostatic Pressed Beryllium

2020 ◽  
Vol 842 ◽  
pp. 199-204
Author(s):  
Boris Syrnev ◽  
Alexandr Revutskiy ◽  
Oksana Semilutskaya
Keyword(s):  
Mechanical Properties ◽  
Yield Strength ◽  
Grain Boundary ◽  
Elastic Limit ◽  
Hot Isostatic Pressing ◽  
Beryllium Oxide ◽  
Electron Microscopic ◽  
Research Results ◽  
Reinforcing Particles ◽  
Microscopic Studies

The effect of beryllium hardening has been studied. Beryllium is sintered by method of hot isostatic pressing (HIP), depending on the temperature of powders pressing. The research results of electron microscopic studies were the base for demonstrating formation of the hydraulic phase at the grain boundary of sintered beryllium and influence of the reinforcing phase on the mechanical properties of the HIP blank. The dependence of beryllium precision elastic limit and conventional yield strength from the size of the reinforcing particles of beryllium oxide has been found. The obtained equation provides a description of the “dispersion-grain-boundary" mechanism of isostatic pressed Beryllium hardening.

Effect of Artificial Aging on Microstructures and Mechanical Properties of Extruded Mg Alloy ZK60

2014 ◽  
Vol 697 ◽  
pp. 72-75
Author(s):  
De Liang Yin ◽  
Jian Qiao ◽  
Hong Liang Cui
Keyword(s):  
Mechanical Properties ◽  
Yield Strength ◽  
Aging Time ◽  
Artificial Aging ◽  
Aging Treatment ◽  
Tensile Tests ◽  
Tensile Yield Strength ◽  
Uniaxial Tensile ◽  
Fracture Elongation ◽  
Strength And Ductility

An extruded ZK60 magnesium alloy was subjected to artificial aging at 180 oC for an investigation of the effect of aging time on its precipitation behavior and mechanical properties. Uniaxial tensile tests were conducted to obtain the mechanical properties. Optical microscopy and transmission electron microscopy (TEM) were employed to observe microstructure change before and after aging treatment. It is shown that, both tensile yield strength and ultimate tensile strength increases with aging time. The fracture elongation after aging for 20 h reaches up to 21.0%, and the yield strength increases to 269.5 MPa, 19.4% higher than that of extruded specimens (un-aged), showing a good match of strength and ductility. Three newly-formed precipitates were observed after aging for over 20 h, among which particulate and dispersive precipitates should be responsible for the good combination of strength and ductility.

Effect of mechanical-annealing on the mechanical properties of a Zr-based bulk metallic glass

2019 ◽  
Vol 33 (01n03) ◽  
pp. 1940052
Author(s):  
P. Deng ◽  
X. C. Wang ◽  
F. Zhang ◽  
X. M. Qin ◽  
P. Gao ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Yield Strength ◽  
Metallic Glass ◽  
Bulk Metallic Glass ◽  
Room Temperature ◽  
Constant Pressure ◽  
Aging Treatment ◽  
Model Material ◽  
Glass Forming ◽  
Plastic Stage

The mechanical-annealing referred in this work is also named pre-strain, which is widely investigated in TRIP steel, stainless steel, magnesium alloy and aluminum alloy. In this case, we used preloading to input energy into a bulk metallic glass (BMG) to observe the changes in the structure and mechanical properties. We selected Zr[Formula: see text]Co[Formula: see text]Al[Formula: see text] BMG as a model material owning to its outstanding glass forming ability and excellent mechanical properties. The samples were kept at a constant pressure of 1900, 1700 and 1500 MPa (below the yield strength) for 40, 55 and 70 h. The study found out that the density of those samples increased after being pre-loaded. Then, the samples underwent aging treatment at room-temperature for more than 30 days after unloading. After re-compressing the samples, the results show that the yield strength and fracture strength of the samples decreased, and the amplitude of the serrated plastic flow increased during the plastic stage. Our finding might have some implications for understanding the plastic deformation of BMGs.

Microstructure and Mechanical Properties of Equitomic CoCrFeCuNi High Entropy Alloy

2018 ◽  
Vol 765 ◽  
pp. 149-154 ◽  
Author(s):  
Seung Min Oh ◽  
Sun Ig Hong
Keyword(s):  
Mechanical Properties ◽  
Yield Strength ◽  
Cold Rolling ◽  
Cast Alloy ◽  
Cold Work ◽  
High Entropy Alloy ◽  
Second Phase ◽  
Rich Phase ◽  
High Entropy ◽  
Microstructure And Mechanical Properties

Microstructure and mechanical properties of cast and cold-rolled equitomic CoCrFeCuNi alloy in which Mn was substituted by Cu from Cantor alloy was studied. The separation into two solid solutions (Cr-Co-Fe rich and Cu-rich phases) were observed in CoCrFeCuNi. Coarsening and widening of interdendritic Cu-rich phase after homogenization was observed after homogenization, suggesting Cu-rich phase is thermodynamically stable. The compressive stress-strain curves of homogenized cast CoCrFeCuNi alloy exhibited the reasonably high strength and excellent deformability for the cast alloy. The yield strength increased up to 960MPa after cold rolling from 265MPa of the homogenized cast alloy. The significant increase of yield strength is thought to be associated with the alignment of Cu-rich second phase in addition to cold work dislocation storage after cold rolling.

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