scholarly journals Studying the Thermally Activated Processes Operating during Deformation of hcp and bcc Mg–Li Metal-Matrix Composites

Metals ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 473
Author(s):  
Zuzanka Trojanová ◽  
Zdeněk Drozd ◽  
Pavel Lukáč ◽  
Ján Džugan

Stress-relaxation tests were performed during plastic deformation at room temperature of three magnesium Mg–Li alloys reinforced with 10 vol% of short Saffil fibers. For comparison, the composite with the Mg matrix was studied. The time dependencies of the stress decrease were analyzed with the aim to determine the activation volume and the main types of thermally activated processes occurring during plastic flow. The Mg4Li matrix alloy exhibited the hcp structure, while the composite with the Mg12Li matrix alloy had the bcc structure. The third alloy, Mg8Li, combined both phases, hcp and bcc. The stress acting in the matrix was divided into two components: the internal stress and the effective stress. Activation volume and stress-sensitivity parameters were determined as a function of effective stress and strain. While the values of the activation volume depending on the effective stress lay on one “master” curve, the strain dependence was different for all materials. The main thermally activated process in the hcp structure was the dislocation motion in the noncompact planes, while in the bcc structure, massive recovery processes connected with an increase in dislocations were identified.

Transient creep following stress reductions has been analysed by the method described by McLean (1980) to determine the friction stress σ 0 as a function of temperature and directional solidification conditions for the γ-γ'-Cr 3 Cr 2 in-situ composite and for the γ-γ' matrix alloy. These values of σ 0 are identical to the flow stresses at creep strain rates and can be identified with the sums of the barriers to dislocation motion through the matrix by climb around γ'-particles and Orowan bowing between the carbide fibres. The friction stress and the kinetics of deformation of the composite are determined by the matrix behaviour, whereas its creep strength depends on the distribution of stress between fibre and matrix. When the steady-state creep behaviour of γ-γ'-Cr 3 C 2 is analysed by using the usual power law description in terms of the effective stress σ — σ 0 , rather than the applied stress σ, the stress exponent is ca 4 and the activation energy is similar to the activation energy of self-diffusion for nickel. The results provide strong evidence for the operation of recovery-creep in both the composite and matrix alloys.


2013 ◽  
Vol 592-593 ◽  
pp. 71-74
Author(s):  
Zuzana Zdražilová ◽  
Zuzanka Trojanová ◽  
Kristián Máthis ◽  
Pavel Lukáč

AS21 magnesium alloy (2.1Al-1Si-balance Mg in wt.%) and the alloy reinforced with short δ-Al2O3fibres (Saffil®) were deformed in compression at temperatures between 23 and 300 °C. Stress relaxation tests were performed in order to reveal features of the thermally activated dislocation motion. Internal and effective components of the applied stress have been estimated. The activation volume decreases with increasing effective stress. The values of the activation volume and the activation enthalpy indicate that the main thermally activated process in the alloy as well as in the composite is the dislocation motion in non-compact planes.


2009 ◽  
Vol 1185 ◽  
Author(s):  
Andreas S. Schneider ◽  
Blythe G. Clark ◽  
Carl P. Frick ◽  
Eduard Arzt

AbstractCompression tests with varying loading rates were performed on [001] and [235] oriented small-scale bcc Mo and Nb pillars to determine the contribution of thermally activated screw dislocation motion during deformation. Calculated activation volumes were shown to be in the range of 2 - 9 b3 and by further examination were found to decrease with pillar diameter. This suggests that the kink-pair nucleation of screw dislocations is enhanced by surface effects in the micron and submicron range.


Author(s):  
S. Mahajan ◽  
M. R. Pinnel ◽  
J. E. Bennett

The microstructural changes in an Fe-Co-V alloy (composition by wt.%: 2.97 V, 48.70 Co, 47.34 Fe and balance impurities, such as C, P and Ni) resulting from different heat treatments have been evaluated by optical metallography and transmission electron microscopy. Results indicate that, on air cooling or quenching into iced-brine from the high temperature single phase ϒ (fcc) field, vanadium can be retained in a supersaturated solid solution (α2) which has bcc structure. For the range of cooling rates employed, a portion of the material appears to undergo the γ-α2 transformation massively and the remainder martensitically. Figure 1 shows dislocation topology in a region that may have transformed martensitically. Dislocations are homogeneously distributed throughout the matrix, and there is no evidence for cell formation. The majority of the dislocations project along the projections of <111> vectors onto the (111) plane, implying that they are predominantly of screw character.


2020 ◽  
Vol 72 (10) ◽  
pp. 1153-1158 ◽  
Author(s):  
Yafei Deng ◽  
Xiaotao Pan ◽  
Guoxun Zeng ◽  
Jie Liu ◽  
Sinong Xiao ◽  
...  

Purpose This paper aims to improve the tribological properties of aluminum alloys and reduce their wear rate. Design/methodology/approach Carbon is placed in the model at room temperature, pour 680°C of molten aluminum into the pressure chamber, and then pressed it into the mold containing carbon felt through a die casting machine, and waited for it to cool, which used an injection pressure of 52.8 MPa and held the same pressure for 15 s. Findings The result indicated that the mechanical properties of matrix and composite are similar, and the compressive strength of the composite is only 95% of the matrix alloy. However, the composite showed a low friction coefficient, the friction coefficient of Gr/Al composite is only 0.15, which just is two-third than that of the matrix alloy. Similarly, the wear rate of the composite is less than 4% of the matrix. In addition, the composite can avoid severe wear before 200°C, but the matrix alloy only 100°C. Originality/value This material has excellent friction properties and is able to maintain this excellent performance at high temperatures. Peer review The peer review history for this article is available at: https://publons.com/publon/10.1108/ILT-10-2019-0454/


2021 ◽  
Vol 9 (1) ◽  
Author(s):  
Daniel Bohnsack ◽  
Martin Potten ◽  
Simon Freitag ◽  
Florian Einsiedl ◽  
Kai Zosseder

AbstractIn geothermal reservoir systems, changes in pore pressure due to production (depletion), injection or temperature changes result in a displacement of the effective stresses acting on the rock matrix of the aquifer. To compensate for these intrinsic stress changes, the rock matrix is subjected to poroelastic deformation through changes in rock and pore volume. This in turn may induce changes in the effective pore network and thus in the hydraulic properties of the aquifer. Therefore, for the conception of precise reservoir models and for long-term simulations, stress sensitivity of porosity and permeability is required for parametrization. Stress sensitivity was measured in hydrostatic compression tests on 14 samples of rock cores stemming from two boreholes of the Upper Jurassic Malm aquifer of the Bavarian Molasse Basin. To account for the heterogeneity of this carbonate sequence, typical rock and facies types representing the productive zones within the thermal reservoir were used. Prior to hydrostatic investigations, the hydraulic (effective porosity, permeability) and geomechanical (rock strength, dynamic, and static moduli) parameters as well as the microstructure (pore and pore throat size) of each rock sample were studied for thorough sample characterization. Subsequently, the samples were tested in a triaxial test setup with effective stresses of up to 28 MPa (hydrostatic) to simulate in-situ stress conditions for depths up to 2000 m. It was shown that stress sensitivity of the porosity was comparably low, resulting in a relative reduction of 0.7–2.1% at maximum effective stress. In contrast, relative permeability losses were observed in the range of 17.3–56.7% compared to the initial permeability at low effective stresses. Stress sensitivity coefficients for porosity and permeability were derived for characterization of each sample and the different rock types. For the stress sensitivity of porosity, a negative correlation with rock strength and a positive correlation with initial porosity was observed. The stress sensitivity of permeability is probably controlled by more complex processes than that of porosity, where the latter is mainly controlled by the compressibility of the pore space. It may depend more on the compaction of precedented flow paths and the geometry of pores and pore throats controlling the connectivity within the rock matrix. In general, limestone samples showed a higher stress sensitivity than dolomitic limestone or dolostones, because dolomitization of the rock matrix may lead to an increasing stiffness of the rock. Furthermore, the stress sensitivity is related to the history of burial diagenesis, during which changes in the pore network (dissolution, precipitation, and replacement of minerals and cements) as well as compaction and microcrack formation may occur. This study, in addition to improving the quality of input parameters for hydraulic–mechanical modeling, shows that hydraulic properties in flow zones largely characterized by less stiff, porous limestones can deteriorate significantly with increasing effective stress.


2018 ◽  
Vol 138 (5) ◽  
pp. 2989-2998 ◽  
Author(s):  
Nina Obradović ◽  
Vladimir Blagojević ◽  
Suzana Filipović ◽  
Nataša Đorđević ◽  
Darko Kosanović ◽  
...  

Metals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1815
Author(s):  
Feng Fang ◽  
Diwen Hou ◽  
Zhilei Wang ◽  
Shangfeng Che ◽  
Yuanxiang Zhang ◽  
...  

Based on conventional hot rolling processes and strip casting processes, Cu precipitation strengthening is used to improve the strength of non-oriented silicon steel in order to meet the requirements of high-speed driving motors of electric vehicles. Microstructure evolution was studied, and the effects of Cu precipitates on magnetic and mechanical properties are discussed. Compared with conventional processes, non-oriented silicon steel prepared by strip casting exhibited advantages with regard to microstructure optimization with coarse grain and {100} texture. Two-stage rolling processes were more beneficial for uniform microstructure, coarse grains and improved texture. The high magnetic induction B50 of 1.762 T and low core losses with P1.5/50, P1.0/400 and P1.0/1000 of 1.93, 11.63 and 44.87 W/kg, respectively, were obtained in 0.20 mm sheets in strip casting. Cu precipitates significantly improved yield strength over ~120 MPa without deteriorating magnetic properties both in conventional process and strip casting. In the peak stage aged at 550 °C for 120 min, Cu precipitates retained bcc structure and were coherent with the matrix, and the yield strength of the 0.20 mm sheet was as high as 501 MPa in strip casting. The main mechanism of precipitation strengthening was attributed to coherency strengthening and modulus strengthening. The results indicated that balanced magnetic and mechanical properties can be achieved in thin-gauge non-oriented silicon steel with Cu addition in strip casting.


Author(s):  
V. A. Kalinichenko ◽  
A. S. Kalinichenko ◽  
S. V. Grigoriev

To create friction pairs operating in severe working conditions, composite materials are now increasingly used. Composite materials obtained with the use of casting technologies are of interest due to the possibility to manufacture wide range of compositions at low price compared to powder metallurgy. Despite the fact that many composite materials have been sufficiently studied, it is of interest to develop new areas of application and give them the properties required by the consumer. In the present work the composite materials on the basis of silumin reinforced with copper granules were considered. Attention was paid to the interaction between the matrix alloy and the reinforcing phase material as determining the properties of the composite material. The analysis of distribution of the basic alloying elements in volume of composite material and also in zones of the interphases interaction is carried out. The analysis of the possibility of obtaining a strong interphase zone of contact between the reinforcing component and the matrix material without significant dissolution of the reinforcing material is carried out.


2011 ◽  
Vol 20 (3) ◽  
pp. 213
Author(s):  
Patricia Donnadieu ◽  
Kenji Matsuda ◽  
Thierry Epicier ◽  
Joel Douin

Owing the phase image method (Hytch, 1998), strain fields can be derived from HREM images. The method is here applied to the nanoscale precipitates responsible for hardening in Aluminum alloys. Since the method is a very sensitive one, we have examined the impact of several aspects of the image quality (noise, fluctuations, distortion). The strain field information derived from the HREM image analysis is further introduced in a simulation of the dislocation motion in the matrix.


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