scholarly journals Phase Transformations upon Ageing in Ti15Mo Alloy Subjected to Two Different Deformation Methods

Metals ◽  
2021 ◽  
Vol 11 (8) ◽  
pp. 1230
Author(s):  
Kristína Bartha ◽  
Josef Stráský ◽  
Anna Veverková ◽  
Jozef Veselý ◽  
Jakub Čížek ◽  
...  

Ti15Mo alloy was subjected to two techniques of intensive plastic deformation, namely high pressure torsion and rotary swaging at room temperature. The imposed strain resulted in the formation of an ultrafine-grained structure in both deformed conditions. Detailed inspection of the microstructure revealed the presence of grains with a size of around 100 nm in both conditions. The microstructure after rotary swaging also contained elongated grains with a length up to 1 µm. Isothermal ageing at 400 °C and 500 °C up to 16 h was applied to both conditions to investigate the kinetics of precipitation of the α phase and the recovery of lattice defects. Positron annihilation spectroscopy indicated that the recovery of lattice defects in the β matrix had already occurred at 400 °C and, in terms of positron trapping, was partly compensated by the precipitation of incoherent α particles. At 500 °C the recovery was fully offset by the formation of incoherent α/β interfaces. Contrary to common coarse-grained material, in which the α phase precipitates in the form of lamellae, precipitation of small and equiaxed α particles occurred in the deformed condition. A refined two-phase equiaxed microstructure with α particles and β grain sizes below 1 μm is achievable by simple rotary swaging followed by ageing.

2008 ◽  
Vol 584-586 ◽  
pp. 182-187
Author(s):  
Lilia Kurmanaeva ◽  
Yulia Ivanisenko ◽  
J. Markmann ◽  
Ruslan Valiev ◽  
Hans Jorg Fecht

Investigations of mechanical properties of nanocrystalline (nc) materials are still in interest of materials science, because they offer wide application as structural materials thanks to their outstanding mechanical properties. NC materials demonstrate superior hardness and strength as compared with their coarse grained counterparts, but very often they possess a limited ductility or show low uniform elongation due to poor strain hardening ability. Here, we present the results of investigation of the microstructure and mechanical properties of nc Pd and Pd-x%Ag (x=20, 60) alloys. The initially coarse grained Pd-x% Ag samples were processed by high pressure torsion, which resulted in formation of homogenous ultrafine grain structure. The increase of Ag contents led to the decrease of the resulted grain size and change in deformation behavior, because of decreasing of stacking fault energy (SFE). The samples with larger Ag contents demonstrated the higher values of hardness, yield stress and ultimate stress. Remarkably the uniform elongation had also increased with increase of strength.


2021 ◽  
Vol 1016 ◽  
pp. 1659-1663
Author(s):  
Tatyana Vitalyevna Yakovleva ◽  
Grigory Dyakonov ◽  
Andrey Stotskiy ◽  
Iuliia Mikhailovna Modina ◽  
Irina Semenova

The paper studies the microstructure of two-phase ultrafine-grained titanium VT8M-1 alloy (Ti-5.7Al-3.8Mo-1.2Zr-1.3Sn), which was obtained by rotary swaging (RS). Parameters of the microstructure and the change of the phase elemental / chemical composition were investigated by scanning electron microscopy and transmission electronic microscopy. It was shown that the silicide particles like S2 - (Ti,Zr)6Si3 were precipitated in the process of rotary swaging. The influence of silicide precipitations on the characteristics of high temperature strength of the ultrafine-grained two-phase titanium VT8M-1 alloy was discussed in the paper. The alloy microstructure was analyzed after the creep-rupture tests in the operation temperature range 300-400oС.


2010 ◽  
Vol 667-669 ◽  
pp. 331-336 ◽  
Author(s):  
Rinat K. Islamgaliev ◽  
Marina A. Nikitina ◽  
Aidar F. Kamalov

The paper reports on microstructure, strength and fatigue of ultrafine-grained (UFG) samples of the Al-Cu-Mg-Si aluminum alloy processed by high pressure torsion (HPT) at various temperatures. Application of the HPT treatment led to strong grain refinement, as well as to a raise of the mean-root square strains and dynamic precipitation. In case of optimal HPT treatment the UFG samples have demonstrated the enhanced thermal stability, an increase in ultimate tensile strength in 2.5 times and enhancement in fatigue endurance limit by 20 % in comparison with coarse-grained alloy subjected to standard treatment. It is shown that the regime of the HPT treatment governs the volume fraction of precipitates and segregations, thereby affecting a grain size and thermal stability of ultrafine-grained structure.


2021 ◽  
Vol 63 (10) ◽  
pp. 1572
Author(s):  
Т.С. Орлова ◽  
Д.И. Садыков ◽  
М.Ю. Мурашкин ◽  
В.У. Казыханов ◽  
Н.А. Еникеев

The effect of small additions of copper on the microstructure and physic-mechanical properties of an ultrafine-grained Al-1.47Cu-0.34Zr (wt%) alloy structured by high pressure torsion after preliminary annealing at 375 °C for 140 h has been studied. As a result of processing, high values of strength characteristics (conditional yield strength 430 MPa, ultimate tensile strength 574 MPa) with an acceptable level of electrical conductivity (46.1% IACS) and ductility (elongation to fracture ~ 5%) have been achieved. On the basis of the microstructural parameters determined by X-ray diffraction analysis and transmission electron microscopy, hardening mechanisms responsible for such high strength have been analyzed. It was shown that Cu plays the key role in strengthening. The addition of copper significantly contributes to grain refinement and, consequently, to grain-boundary hardening. Alloying with copper leads to significant additional hardening (~ 130 MPa) in the ultrafine-grained alloy, which is not typical for coarse-grained state. Segregation of Cu at grain boundaries and the formation of Cu nanoclusters are the most probable reasons for this hardening.


2018 ◽  
Vol 385 ◽  
pp. 228-233
Author(s):  
Elena V. Bobruk ◽  
Denis G. Tyulenev ◽  
Oleg V. Golubev ◽  
Maxim Y. Murashkin

High pressure torsion (HPT) and equal channel angular pressing in parallel channels (ECAP-PC) at room temperature are used to form homogeneous ultrafine-grained (UFG) structure with a grain size of the aluminum matrix of 350 and 700 nm, respectively, in Al-30Zn (wt. %) specimens. The UFG samples with special geometry produced from the specimens processed by SPD techniques were subjected to sphere-shaped dimple extrusion testing (via the Erikson test method) and bended plate extrusion to determine the material formability during cold sheet metal forming. The same tests were performed on the material with coarse-grained (CG) structure for the sake of comparison. The obtained results are discussed.


Materials ◽  
2019 ◽  
Vol 12 (12) ◽  
pp. 1939 ◽  
Author(s):  
Gheorghe Gurau ◽  
Carmela Gurau ◽  
Felicia Tolea ◽  
Vedamanickam Sampath

Severe plastic deformation (SPD) is widely considered to be the most efficient process in obtaining ultrafine-grained bulk materials. The aim of this study is to examine the effects of the SPD process on Ni-Fe-Ga ferromagnetic shape memory alloys (FSMA). High-speed high-pressure torsion (HSHPT) was applied in the as-cast state. The exerted key parameters of deformation are described. Microstructural changes, including morphology that were the result of processing, were investigated by optical and scanning electron microscopy. Energy-dispersive X-ray spectroscopy was used to study the two-phase microstructure of the alloys. The influence of deformation on microstructural features, such as martensitic plates, intragranular γ phase precipitates, and grain boundaries’ dependence of the extent of deformation is disclosed by transmission electron microscopy. Moreover, the work brings to light the influence of deformation on the characteristics of martensitic transformation (MT). Vickers hardness measurements were carried out on disks obtained by SPD so as to correlate the hardness with the microstructure. The method represents a feasible alternative to obtain ultrafine-grained bulk Ni-Fe-Ga alloys.


2021 ◽  
Vol 1016 ◽  
pp. 922-927
Author(s):  
Iuliia Mikhailovna Modina ◽  
Alexander V. Polyakov ◽  
Grigory Dyakonov ◽  
Tatyana Vitalyevna Yakovleva ◽  
Andrey G. Stotskiy ◽  
...  

This paper is aimed to study the creep behavior of two-phase ultrafine-grained VT8M-1 (Ti-5.7Al-3.8Mo-1.2Zr-1.3Sn) titanium alloy obtained by rotary swaging (RS). It is shown that the 100-hour creep strength of the ultra-fine grained (UFG) VT8M-1 alloy retains high values at temperatures up to 400 °C. An increase in the testing temperature to >450 °C leads to a decrease in the creep rupture strength. The relationship between the microstructure and creep resistance of UFG alloy is discussed.


Metals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1800
Author(s):  
Elvina R. Shayakhmetova ◽  
Mariya A. Murzinova ◽  
Ayrat A. Nazarov

Solid state joints of samples of coarse-grained (CG) and ultrafine-grained (UFG) nickel have been obtained for the first time using spot ultrasonic welding (USW). The UFG structure in disk-shaped samples was processed by means of high-pressure torsion (HPT). On the basis of lap shear tests, the optimal values of the clamping force resulting in the highest values of the joint strength are determined. The microstructures in the weld joints obtained at optimal parameters of USW are characterized by scanning electron microscopy. It is shown that during ultrasonic welding of coarse-grained nickel, a thin layer with an UFG microstructure is formed near the weld surfaces. The bulks of sheets retain the CG microstructure, but a significant dislocation activity is observed in these regions. During USW of samples having an UFG initial microstructure, significant grain growth occurs. Fine grains are observed only along the welding interface. An average lap shear strength of 97 MPa was obtained by welding the UFG samples, which was approximately 40% higher than the strength of samples processed by welding coarse-grained sheets (70 MPa). It is concluded that higher strength weld joints can be obtained by using sheets with the UFG structure as compared to the CG sheets.


2003 ◽  
Vol 18 (8) ◽  
pp. 1991-1997 ◽  
Author(s):  
Yizhou Zhou ◽  
Wei Zhang ◽  
Baoquan Wang ◽  
Jingdong Guo

High-current-density electropulsing was applied to a coarse-grained Cu–Zn alloy with two phases of α-phase and β′-phase. It was found that with an electropulsing treatment, ultrafine-grained (UFG) microstructure could be formed in the α-phase, but could not be formed in the β-phase. The results indicated that the formation of UFG microstructure was dependent on solid-state phase transformation. The main reason for the formation of UFG microstructure by electropulsing treatment resulted from the effect of a decrease in thermodynamic barrier and enhancement of nucleation rate in a current-carrying system, but not from the high heating and cooling rate during electropulsing treatment. The bulk UFG samples prepared by electropulsing treatment were free of porosity and contamination and had no large microstrain. It was reasonable to anticipate that a new method might be developed to produce ideal bulk UFG samples directly from the conventional coarse-grained materials by application of electropulsing.


2015 ◽  
Vol 364 ◽  
pp. 147-156 ◽  
Author(s):  
Vladimir V. Popov ◽  
A.V. Sergeev ◽  
A.V. Stolbovsky

Grain boundaries in coarse-grained Mo with grain boundaries of recrystallization origin and in ultrafine-grained (UFG) Mo obtained by high pressure torsion have been studied by the emission Mössbauer spectroscopy on the57Co (57Fe) nuclei. It is demonstrated that Co atoms diffuse along grain boundaries by interstitials. The temperature dependence of grain-boundary segregation factor of Co in coarse-grained Mo has been determined. It is shown that the state of Co atoms in grain boundaries and near-boundary areas in UFG Mo differs from that in coarse-grained Mo.


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