scholarly journals Chemotypical diversity of Mentha longifolia L. oil

2021 ◽  
pp. 130-139
Author(s):  
O. M. Shevchuk ◽  
S. A. Feskov ◽  
N. A. Bagrikova ◽  
I. V. Tania
Keyword(s):  
Essential Oil ◽  
Mass Fraction ◽  
Raw Materials ◽  
Three Samples ◽  
Two Samples ◽  
Mentha Longifolia ◽  
Wet Weight

The article presents data on the content and composition of the essential oil of Mentha longifolia (L.) L. plants growing in natural phytocenoses on the territory of Crimea and Abkhazia. It was found that dry raw materials in two samples from natural phytocenoses of Crimea contain 1.27 and 1.76% of essential oil per wet weight, three samples from phytocenoses of Abkhazia contain less essential oil - 0.68, 0.98 and 1.19 %. About 60 components have been identified. Two new chemotypes were identified for Crimea: carvone-piperitone (mass fraction of carvone is 66.65%, piperitone oxide - 14.37%) and piperitone-sabinene (mass fraction of piperitone oxide - 55.19% and cis-sabinene hydrate - 23.51%), and two for Abkhazia: terpene-caryophyllene (α-terpinyl acetate - 51.48%;  β-caryophyllene - 9.26%), piperitone-non-petalactone (piperitone oxide - 46.29%;  nepetalactone 4aa, 7a, 7aa - 34.85%). These Mentha longifolia chemotypes are promising for use in the food, chemical, pharmaceutical and perfume industries. 

scholarly journals Comparative characteristics of the basic economic features of inter-specific hybrides of the genus lavandula

2019 ◽  
pp. 76-85
Author(s):  
Yu. S. Khokhlov ◽  
A. E. Paly
Keyword(s):  
Essential Oil ◽  
Interspecific Hybrids ◽  
Mass Fraction ◽  
Field Experiments ◽  
Raw Materials ◽  
Gas Chromatography Mass Spectrometry ◽  
High Yield ◽  
Linalyl Acetate ◽  
Wet Weight

The aim of the work was to obtain comparative data on the main economic characteristics of the four lavandins to identify a hybrid with high quality essential oil. Determination of the chemical composition of essential oil of lavandin interspecific hybrids bred in NBG-NSC, allows to judge the prospects for their use in the perfume industry. Cultivars of lavandin Temp (control), Snezhny Bars and lavandin genetype Brovka, № 53 were selected as the objects of study. Crop accounting was carried out according to the method of field experiments by Dospekhov. The mass fraction of essential oil in plants was determined by hydrodistillation. The composition of the volatiles substances was determined by gas chromatography-mass spectrometry. Based on the results, the following hybrids were identified: Brovka with a high yield of flower raw materials of 118,8 c / ha, Snezhny Bars with a high linalool content up to 62,5%. Hybrid No.53 was characterized by a high yield of essential oil on a wet weight up to 4,2%, a linalyl acetate content up to 31.1% and a low content of camphor, 1,8-cineole and borneol. It is shown that the essential oil of hybrid No. 53 is promising for use in perfumes.

scholarly journals TO THE QUESTION OF STANDARDIZATION OF THE TARRAGON RAW

2019 ◽  
pp. 58-62 ◽  
Author(s):  
N. N. Bakova ◽  
O. M. Shevchuk ◽  
L. A. Logvinenko ◽  
L. A. Timasheva
Keyword(s):  
Essential Oil ◽  
Mass Fraction ◽  
Raw Materials ◽  
Biologically Active ◽  
High Productivity ◽  
Type Size ◽  
Wet Weight ◽  
Technical Specifications ◽  
Main Components ◽  
Main Component

Tarragon (Artemisia dracunculus L.) is a spicy aromatic culture, perspective to use in the food and medical industry. In the collection of aromatic and medicinal plants of the Nikita Botanical Gardens, tarragon is represented by two varieties: Isumrud and Travnevy. The Isumrud variety is characterized by a high content of essential oil (0.6% of the wet weight) of the methylchavicol chemotype (the main component of the essential oil is methylchavicol, whose mass fraction is up to 91%) and is perspective to use not only as a spice, but also in medicine as a reducing facilities. The variety Travnevy contains only 0.1% of the essential oil from the wet mass of the sabineno-elemicin chemotype (the main components of the essential oil are sabinen (40.0%) and trans-from-iso-elemicin – 26.1%), characterized by high productivity of the aerial mass (12 kg/m2), the main direction of use in the food industry as a spice. Due to the lack of requirements for dry raw tarragon, we have developed a draft technical specifications for dry crushed tarragon raw materials TS 01.28.30-009-01579640-2018. Specifications apply to dried whole and crushed raw materials, intended for the manufacture of water and water-alcohol infusions, as a source of biologically active substances, as a component for seasonings to meat, fish dishes, for use in cooking, as well as in the production of alcohol and soft drinks. The main physicochemical indicators of whole and crushed tarragon raw materials (type, size, smell, taste, mass fraction of essential oil, impurities, moisture, ash) are presented.

scholarly journals Changes in the component composition of Thymus vulgaris L. essential oil depending on the method of distillation

2020 ◽  
pp. 106-115
Author(s):  
Yu. S. Khokhlov ◽  
I. A. Fedotova ◽  
O. M. Shevchuk
Keyword(s):  
Essential Oil ◽  
Mass Fraction ◽  
Raw Materials ◽  
Component Composition ◽  
Raw Material ◽  
Gas Chromatography Mass Spectrometry ◽  
Thymus Vulgaris ◽  
Mass Flowering ◽  
Two Samples ◽  
Volatile Terpene

The objective of the work was to identify changes in the amount and component composition of essential oil in the raw material of Thymus vulgaris L. (common thyme) when using different distillation methods. The object of the study was two samples of thyme-thymol and linalool chemotypes. Essential oil was obtained from freshly harvested raw materials (inflorescences in the mass flowering phase) by the following methods: hydrodistillation method on Clevenger apparatuses and steam extraction method on the installation for the production of essential oil and intermediates "Alpha-Ether Compact". The component composition of volatile substances was determined by gas chromatography-mass spectrometry. In the composition of volatile compounds of plant essential oil, 29 components for the thymol chemotype were identified, and 18 components for the linalool chemotype were identified. It was found that the use of the hydrodistillation method allows extracting 40-50% more essential oil. Significant differences were found between the mass fraction of extracted essential oil components using different methods and the content of the mass fraction of essential oil in the raw material of Th. vulgaris and found that depending on the method of obtaining essential oil, the proportion of volatile terpene hydrocarbons and oxygen-containing compounds changes. The method of steam distillation leads to a deterioration of the component composition of the essential oil, reducing the content of the dominant components of both chemotypes (thymol and linalool).

scholarly journals Elemental composition of wild colisa lalia in relation to body size and condition factor from Pakistan

2016 ◽  
Vol 4 (2) ◽  
pp. 202
Author(s):  
Summera Fatima ◽  
Muhammad Naeem
Keyword(s):  
Condition Factor ◽  
Industrial Area ◽  
Mean Value ◽  
Human Consumption ◽  
Flame Atomic Absorption ◽  
Flame Atomic Absorption Spectrophotometer ◽  
Three Samples ◽  
Two Samples ◽  
Colisa Lalia ◽  
Wet Weight

Twenty three samples of wild fish Colisa lalia were collected from Nala Daik, a stream in Sialkot. The concentration of Cadmium (Cd), Cobalt (Co), Iron (Fe), Manganese (Mn) and Nickel (Ni) in the whole fish were determined by Flame atomic absorption spectrophotometer to estimate the water contamination and health risk of human consumption in Sialkot region which is a popular industrial area. The detected cobalt in twenty two samples and nickel in eight samples exceeds the permitted limits for fish set by IAEA-407 (Wyse et al. 2003).While the concentration of Cadmium, Iron and Manganese in all samples were below permitted level set by European and other International Organizations. The concentration of Cd, Co, Fe, Mn and Ni was ranging from 0.20-1.71, 0.84-55.38, 82.82-137.63, 1.61-22.73, 2.23-5.98 having mean value as 0.67, 39.31, 139.09, 13.26 and 0.56 (ug/g wet weight) respectively. Regressions analysis was performed for both size and condition factor with metal concentrations. As far as correlation with total length and weight was concerned, a decreasing trend was shown by Cd and Ni while Co, Fe and Mn showed an increasing trend and these correlations were found significant for all these elements. No effect of condition factor was observed in the study on Colisa lalia. Inter-elemental regression showed significant correlations among metals.

SEM-EDX and FTIR analysis of archaeological ceramic potteries from southern Italy

Microscopy ◽  
2020 ◽  
Vol 69 (6) ◽  
pp. 371-380
Author(s):  
Tania Dey ◽  
Joseph Coleman Carter ◽  
Keith Swift
Keyword(s):  
Firing Temperature ◽  
Southern Italy ◽  
Raw Materials ◽  
Silica Nanoparticle ◽  
Glassy Matrix ◽  
Processing Temperature ◽  
Valuable Insight ◽  
Sem Image ◽  
Three Samples ◽  
Two Samples

Abstract Sherds of ancient ceramics potteries, dating back to the seventh century BC and excavated from southern Italy, were analyzed in terms of microstructure and porosity (SEM), elemental composition (EDX), chemical bonding and mineralogical components (FTIR) in order to establish correlation with firing temperature, firing condition and provenance. Si/Al ratio from EDX analysis showed three major categories of raw materials (illite/montmorillonite, kaolinite and mullite), suggesting difference in provenance. Uniformly sized silica nanoparticle (0.7 μm diameter) and trace amount of silver are being reported for the first time in one sample. Anorthite mineral and quartz inclusion was detected by FTIR in certain samples. All samples showed a prominent band for Si-O stretching, which shifted from 1062 cm−1, broadened and appeared as doublet, relative to processing temperature. FTIR results proved incomplete dihydroxylation and undissociated carbonate in three samples, indicating a firing temperature of 700–800°C, whereas other samples were fired above 900°C. Only one sample among these three showed bloating pores in between interconnecting glassy matrix in SEM image, indicating a firing temperature of 1100–1200°C. The absence of magnetite along with significant Fe and Mn content indicated the formation of jacobsite, an iron manganese spinel complex, MnFe2O4, which is responsible for the black gloss effect in two particular samples and can be further confirmed by XRD. The presence of numerous small pores in SEM image of one of these two samples (1.2 μm diameter) was indicative of extended vitrification at higher temperature than the other one. However, magnetite was responsible for black gloss effect in two other samples, proving difference in provenance. Therefore, SEM-EDX and FTIR results can offer valuable insight into the firing conditions, gloss decoration and provenance of ancient ceramic potteries.

scholarly journals Elemental Characterization of Ciders and Other Low-Percentage Alcoholic Beverages Available on the Polish Market

Molecules ◽  
2021 ◽  
Vol 26 (8) ◽  
pp. 2186
Author(s):  
Magdalena Gajek ◽  
Aleksandra Pawlaczyk ◽  
Piotr Wysocki ◽  
Malgorzata I. Szynkowska-Jozwik
Keyword(s):  
Raw Materials ◽  
Statistical Tests ◽  
Analytical Data ◽  
Alcoholic Beverages ◽  
Data Set ◽  
Apple Variety ◽  
Three Samples ◽  
Two Samples ◽  
Elemental Fingerprint ◽  
The Impact

Seventy-three samples of alcoholic beverages and juices that were purchased on the Polish market and home-made were analyzed for their elemental profiles. The levels of 23 metals were determined by ICP-MS (Ag, Ba, Bi, Cd, Co, Cr, Li, Mn, Ni, Pb, Sr and Tl), ICP-OES (Al, B, Ca, Cu, Fe, K, Mg, Na, Ti and Zn) and CVAAS (Hg) techniques in twenty-five samples of ciders widely available on the Polish market; six samples of home-made ciders; two samples of juices used in the production of these ciders; and forty samples of low-percentage, flavored alcoholic beverages based on beer. The gathered analytical data confirmed that the final elemental fingerprint of a product is affected by the elemental fingerprint of the ingredients used (apple variety) as well as the technology and equipment used by the producer, and in the case of commercial ciders, also the impact of type of the packaging used was proven. These factors are specific to each producer and the influence of the mentioned above parameters was revealed as a result of the performed analysis. Additionally, the inclusion of the home-made ciders in the data set helped us to understand the potential origin of some elements, from the raw materials to the final products. The applied statistical tests revealed (Kruskal–Wallis and ANOVA) the existence of statistically significant differences in the concentration of the following metals: Ag, Al, B, Bi, Co, Cr, Cu, Fe, K, Li, Mg, Na, Ni, Ti and Zn in terms of the type of cider origin (commercial and home-made). In turn, for different packaging (can or bottle) within one brand of commercial cider, the existence of statistically significant differences for Cu, Mn and Na was proved. The concentrations of all determined elements in the commercial cider from the Polish market and home-made cider samples can be considered as nontoxic, because the measured levels of elements indicated in the regulations were lower than the allowable limits. Moreover, the obtained results can be treated as preliminary for the potential authentication of products in order to distinguish the home-made (fake) from the authentic products, especially for premium-class alcoholic beverages.

scholarly journals Biologically active substances of Helichrysum italicum (Roth) G.Don

2019 ◽  
pp. 70-79
Author(s):  
O. M. Shevchuk ◽  
S. P. Lukashuk ◽  
S. A. Feskov ◽  
S. L. Adzhiakhmetova ◽  
N. M. Chervonnaya ◽  
...  
Keyword(s):  
Essential Oil ◽  
Raw Materials ◽  
Total Content ◽  
Component Composition ◽  
Uv Spectra ◽  
Biologically Active ◽  
The Crimea ◽  
Wet Weight ◽  
Phenolic Substances ◽  
Main Components

The article provides data on a comparative study of the content and component composition of essential oil, the total content of antioxidants and flavonoids of two cultivars and two promising cultivar samples of Italian strawflower ( Helichrysum italicum (Roth) G. Don) grown on the Southern Coast of the Crimea in the collection of aromatic and medicinal plants of the Nikitsky Botanical Gardens. It has been found that the content of essential oil in the green weight of top of H. italicum varies from 0.1% of the wet weight (‘Crystal’ cultivar) to 0.2 (cultivar No. 5). The main components of ‘VIM’ cultivar essential oil are α-pinene and D-limonene, of ‘Crystal’ cultivar is neril acetate, of the sample No. 5 is α-pinene and rosiforiol, of the sample No. 158 is neryl acetate and γ-turmeric. A significant relative content of β-diketones (38%) in the essential oil of ‘Crystal’ cultivar was noted. The greatest amount of antioxidants (2.59 mg / g (in conversion to quercetin) and flavonoids (0.366%) in the inflorescences of Italian strawflower ‘VIM’ cultivar is contained in the budding phase. The results of chromatographic analysis prove the presence of 4 phenolic substances in the inflorescences of Italian strawflower. UV-spectra of alcohol solutions of the studied raw materials had a maximum absorption at a wavelength of 418 ± 2nm. Quantitative determination of flavonoids by differential spectroscopy calculated as isosalipurposide showed that the content of flavonoids in inflorescences varies from 0.262% to 0.366% depending on a cultivar and a phase of vegetation.

Problems of ensuring metrological traceability of measurement results of indicators of quality for food products and food raw materials

2020 ◽  
pp. 64-70
Author(s):  
Mariya Y. Medvedevskikh ◽  
Anna S. Sergeeva
Keyword(s):  
Reference Materials ◽  
Mass Fraction ◽  
Nutritional Value ◽  
Animal Feed ◽  
Raw Materials ◽  
Meat Products ◽  
Metrological Traceability ◽  
Food Products ◽  
Freeze Dried ◽  
Measurement Results

The article raises the problem of ensuring metrological traceability of the measurement results of indicators of quality and nutritional value for food products and food raw materials: water (moisture), nitrogen (protein, crude protein), fat, ash and carbohydrates. The problem under consideration can be solved by applying reference materials of food composition, traceable to state primary measurement standards GET 173-2017 and GET 176-2019 and primary reference measurement procedures (PRMP), for attestation of measurement procedures and accuracy checking of measurement results. The article discusses the results of the PRMP development of mass fraction of fat, ash and carbohydrates in food products and food raw materials, as well as mass fraction of crude fat (oil content) in oil crops seeds and products based on them. The paper also presents metrological characteristics of reference materials of composition of dry dairy products, grain-milk dry porridges for nutrition of babies, grain dry porridges for nutrition of babies, egg powder, freeze-dried meat products, animal feed. The results of the work allow for building a chain of metrological traceability from GET 173-2017, GET 176-2019 and PRMP to routine measurement procedures, thereby ensuring the uniformity of measurements of nutritional value of food products.

Comparative analysis of essential oil obtained from fresh and dried leaves of medicinal sage

2020 ◽  
pp. 39-53
Author(s):  
Tatyana Shcheglova
Keyword(s):  
Comparative Analysis ◽  
Essential Oil ◽  
Raw Materials ◽  
Quantitative Difference ◽  
Botanical Garden ◽  
Component Composition ◽  
Gas Chromatography Mass Spectrometry ◽  
Qualitative And Quantitative ◽  
Salvia Officinalis L ◽  
Medical University

The article presents results of the study of a comparative analysis of essential oil obtained from fresh and dried leaves of medicinal sage (Salvia officinalis L.), growing in the Botanical Garden of the First Moscow State Medical University named after Sechenov. The studies were carried out using gas chromatography– mass spectrometry. Qualitative and quantitative difference in the component composition of the essential oil obtained from fresh and dried raw materials was determined as a result of the study.

scholarly journals Variability in chemical composition and antimicrobial activity of essential oil of Rosa × damascena Herrm. from mountainous regions of Iran

2021 ◽  
Vol 8 (1) ◽  
Author(s):  
Mansureh Ghavam ◽  
Afsaneh Afzali ◽  
Maria Manconi ◽  
Gianluigi Bacchetta ◽  
Maria Letizia Manca
Keyword(s):  
Antimicrobial Activity ◽  
Chemical Composition ◽  
Essential Oil ◽  
Essential Oils ◽  
Environmental Conditions ◽  
Raw Materials ◽  
Rosa Damascena ◽  
Mountainous Regions ◽  
Aspergillus Brasiliensis ◽  
Suitable Area

Abstract Background Essential oil of Rosa × damascena Herrm. is one of the most valuable and important raw materials for the flavor and fragrance industry. The cultivation of this plant has ancient origins, and Kashan was one of the first mountainous regions of Iran dealing with the cultivation of R. × damascena. In this study, both chemical composition and antimicrobial activity of different rose essential oils obtained from five mountainous areas of Kashan region (Maragh, Qamsar, Sadeh, Javinan, and Kamoo) has been investigated along with the influence of the environmental conditions on these properties. Results Results showed that yield and chemical composition of essential oils obtained from Rosa × damascena were significantly affected by the collection area. In particular, the yield of oils varied from ~0.08 to ~0.132% and citronellol (36.70-9.18%), geraniol (12.82-0.47%), nonadecane (22.73-10.36%), heneicosane (31.7-11.43%), and 1-nonadecene (6.03-3.93%) have been detected as main compounds in all the plants collected, but at different concentrations depending on the collection area. The best fragrance and the highest yield were found in the oil from Kamoo area. Similarly to the chemical composition, the antimicrobial activity of the essential oils was affected by their origin, and essential oil obtained from plants collected from Kamoo area disclosed the highest antibacterial and antifungal efficacy. Its inhibition halos were 17.33±0.58 mm against Aspergillus brasiliensis, 15.67±0.58 mm against Staphylococcus aureus, and 12.33±0. 58 mm against Streptococcus pyogenes. Essential oils of R. damascena were also effective against Gram-negative Pseudomonas aeruginosa and they had a MIC value of 62.50 μg/mL irrespective of the collection area (except the oil from Javinan area). On the contrary, the highest antifungal power against Candida albicans yeast was reached using the essential oil obtained from plants collected in Javinan region (MIC and MBC ~62.50 μg/mL). Conclusions Overall results underline the influence of environmental conditions of the different areas of Kashan region, on the chemical composition of and antimicrobial activity of the essential oils of Rosa × damascena. In addition, results disclosed that Kamoo seemed to be the most suitable area for the competitive cultivation of R. × damascena to the intensive production of aromatic flower oil and natural antimicrobial essential oils.

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