Microstructures in Beta-III Titanium Alloys

1975 ◽  
Vol 33 ◽  
pp. 24-25
Author(s):  
S. Fujishiro
Keyword(s):  
Mechanical Properties ◽  
Elastic Modulus ◽  
Mechanical Characteristics ◽  
Volume Fraction ◽  
Beta Phase ◽  
X Ray ◽  
Alpha Omega ◽  
Water Quench ◽  
Forming Temperature ◽  
Mo Content

In an effort to increase the elastic modulus of commercial Beta-III Titanium alloy (Ti-12Mo4.5Sn5.5Zr) without impairing other mechanical properties, the alloy has been solutionized in the beta and beta/alpha fields and subsequently aged at the alpha and alpha/omega forming temperature range, following water quench; the volume fraction and morphology of the precipitation phases govern the elastic modulus and other mechanical characteristics. Dilatometric technique was employed to determine the omega forming range which is indicated by a notable contraction; contraction is due to depletion of the Mo content in the beta phase. TEM was utilized in order to identify the phases and define morphology whereas the volume fraction of phases was determined by X-ray.

scholarly journals Microstructure and Mechanical Properties of Rapidly Solidified β-Type Ti–Fe–Sn–Mo Alloys with High Specific Strength and Low Elastic Modulus

Metals ◽  
2019 ◽  
Vol 9 (11) ◽  
pp. 1135 ◽  
Author(s):  
Li ◽  
Ma ◽  
Jia ◽  
Meng ◽  
Tang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Elastic Modulus ◽  
Volume Fraction ◽  
High Yield ◽  
Specific Strength ◽  
High Specific Strength ◽  
Microstructure And Mechanical Properties ◽  
Low Elastic Modulus ◽  
Mo Content ◽  
Rapidly Solidified

The microstructure and mechanical properties of rapidly solidified β-type Ti–Fe–Sn–Mo alloys with high specific strength and low elastic modulus were investigated. The results show that the phases of Ti–Fe–Sn–Mo alloys are composed of the β-Ti, α-Ti, and TiFe phases; the volume fraction of TiFe phase decreases with the increase of Mo content. The high Fe content results in the deposition of TiFe phase along the grain boundary of the Ti phase. The Ti75Fe19Sn5Mo1 alloy exhibits the high yield strength, maximum compressive strength, large plastic deformation, high specific strength, high Vickers hardness, and large toughness value, which is a superior new engineering material. The elastic modulus (42.1 GPa) of Ti75Fe15Sn5Mo5 alloy is very close to the elastic modulus of human bone (10–30 GPa), which indicating that the alloy can be used as a good biomedical alloy. In addition, the large H/Er and H3/Er2 values of Ti75Fe19Sn5Mo1 alloy indicate the good wear resistance and long service life as biomedical materials.

Effects of Hot Isostatic Pressing (HIP) on Microstructure and Mechanical Properties of K403 Nickel-Based Superalloy

2016 ◽  
Vol 35 (5) ◽  
pp. 463-471 ◽  
Author(s):  
Haocheng Zhang ◽  
Anqiang Wang ◽  
Zhixun Wen ◽  
Zhufeng Yue ◽  
Chengjiang Zhang
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Elastic Modulus ◽  
Volume Fraction ◽  
Cast Alloy ◽  
Hot Isostatic Pressing ◽  
X Ray ◽  
Nickel Based Superalloy ◽  
Nanoindentation Experiment ◽  
Scanning Electron

AbstractThe microstructure of as-cast and as-HIPed (hot isostatic pressed) K403 superalloy was investigated using a scanning electron microscopy (SEM), as component analysis was conducted by energy dispersive x-ray spectrometer (EDS). It was found that the microstructure of the alloy was improved significantly through HIP. Firstly, the microporosity and micropores in as-cast alloy were ameliorated effectively and the morphology of grains tended to be uniform. Moreover, the morphology of carbides at grain boundaries transformed from thread-like to granular. Uppermost, the size, shape and volume fraction of γ′ phase were significantly optimized and γ′ precipitates in two different sizes were generated in matrix. Nanoindentation experiment was then carried out to obtain the nanohardness and elastic modulus of as-cast and as-HIPed K403 superalloy. The results revealed an obvious increase in both nanohardness and elastic modulus after HIP. Conclusions could be drawn from the research that HIP could improve the microstructure of as-cast K403 superalloy, which could enhance the mechanical properties of the alloy positively.

Phase Transformations in Ti-7w/oMo-3w/oMe Alloy

1974 ◽  
Vol 32 ◽  
pp. 514-515
Author(s):  
S. Fujishiro
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Transmission Electron Microscopy ◽  
Tensile Strength ◽  
Mechanical Processing ◽  
Ray Method ◽  
X Ray ◽  
Transmission Electron ◽  
Water Quench ◽  
Alpha Beta

The mechanical properties of three titanium alloys (Ti-7Mo-3Al, Ti-7Mo- 3Cu and Ti-7Mo-3Ta) were evaluated as function of: 1) Solutionizing in the beta field and aging, 2) Thermal Mechanical Processing in the beta field and aging, 3) Solutionizing in the alpha + beta field and aging. The samples were isothermally aged in the temperature range 300° to 700*C for 4 to 24 hours, followed by a water quench. Transmission electron microscopy and X-ray method were used to identify the phase formed. All three alloys solutionized at 1050°C (beta field) transformed to martensitic alpha (alpha prime) upon being water quenched. Despite this heavily strained alpha prime, which is characterized by microtwins the tensile strength of the as-quenched alloys is relatively low and the elongation is as high as 30%.

Macroprobe Mode for the Study of Segregation in Steels

1990 ◽  
Vol 48 (2) ◽  
pp. 260-261
Author(s):  
Auclair Gilles ◽  
Benoit Danièle
Keyword(s):  
Mechanical Properties ◽  
Spatial Distribution ◽  
High Performance ◽  
Volume Fraction ◽  
Sheet Steel ◽  
Acquisition Time ◽  
Chemical Information ◽  
X Ray ◽  
Accurate Quantitative Analysis ◽  
Optical Micrographs

During these last 10 years, high performance correction procedures have been developed for classical EPMA, and it is nowadays possible to obtain accurate quantitative analysis even for soft X-ray radiations. It is also possible to perform EPMA by adapting this accurate quantitative procedures to unusual applications such as the measurement of the segregation on wide areas in as-cast and sheet steel products.The main objection for analysis of segregation in steel by means of a line-scan mode is that it requires a very heavy sampling plan to make sure that the most significant points are analyzed. Moreover only local chemical information is obtained whereas mechanical properties are also dependant on the volume fraction and the spatial distribution of highly segregated zones. For these reasons we have chosen to systematically acquire X-ray calibrated mappings which give pictures similar to optical micrographs. Although mapping requires lengthy acquisition time there is a corresponding increase in the information given by image anlysis.

Effect of Si Content on Microstructure and Properties of 60Si2CrVA Spring Steel

2014 ◽  
Vol 968 ◽  
pp. 63-66 ◽  
Author(s):  
Fei Zhao ◽  
Zhan Ling Zhang ◽  
Jun Shuai Li ◽  
Cui Ye ◽  
Ni Li
Keyword(s):  
Mechanical Properties ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Testing Machine ◽  
Spring Steel ◽  
Impact Testing ◽  
X Ray ◽  
Comprehensive Properties ◽  
Spring Steels ◽  
Si Content

The microstructure and mechanical properties of the four spring steels with different Si content treated by Q-I-Q-T process were studied by metallographic microscope, MTS, impact testing machine and X-ray stress analyzer. The results show that the tensile strength and yield strength is first increased and then decreased with the increase of Si content, the volume fraction of retained austenite and elongation are fist decreased and then increased when the Si content is less than 2.1%, and the microstructure become finer and homogeneous. When Si content reaches 2.1%, the comprehensive properties of 60Si2CrVA spring steel is the best.

Stress in Hydrogenated Microcrystalline Silicon Thin Films

1999 ◽  
Vol 557 ◽  
Author(s):  
D. Peiró ◽  
C. Voz ◽  
J. Bertomeu ◽  
J. Andreu ◽  
E. Martínez ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Vapor Deposition ◽  
Volume Fraction ◽  
Chemical Vapor ◽  
Hot Wire ◽  
X Ray Diffraction ◽  
Microcrystalline Silicon ◽  
X Ray ◽  
Silicon Thin Films ◽  
Abrupt Changes

AbstractHydrogenated microcrystalline silicon films have been obtained by hot-wire chemical vapor deposition (HWCVD) in a silane and hydrogen mixture at low pressure (<5 × 10-2 mbar). The structure of the samples and the residual stress were characterised by X- ray diffraction (XRD). Raman spectroscopy was used to estimate the volume fraction of the crystalline phase, which is in the range of 86 % to 98%. The stress values range between 150 and -140 MPa. The mechanical properties were studied by nanoindentation. Unlike monocrystalline wafers, there is no evidence of abrupt changes in the force-penetration plot, which have been attributed to a pressure-induced phase transition. The hardness was 12.5 GPa for the best samples, which is close to that obtained for silicon wafers.

Biomimetic composites inspired by venous leaf

2017 ◽  
Vol 52 (3) ◽  
pp. 361-372 ◽  
Author(s):  
Gongdai Liu ◽  
R Ghosh ◽  
A Vaziri ◽  
A Hossieni ◽  
D Mousanezhad ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Elastic Modulus ◽  
Yield Stress ◽  
Poisson’S Ratio ◽  
Composite Structures ◽  
Volume Fraction ◽  
Matrix Material ◽  
Poisson's Ratio ◽  
Fiber Volume ◽  
Young’S Moduli

A typical plant leaf can be idealized as a composite having three principal fibers: the central mid-fiber corresponding to the mid-rib, straight parallel secondary fibers attached to the mid-fiber representing the secondary veins, and then another set of parallel fibers emanating from the secondary fibers mimicking the tertiary fibers embedded in a matrix material. This paper introduces a biomimetic composite design inspired by the morphology of venous leafs and investigates the effects of venation morphologies on the in-plane mechanical properties of the biomimetic composites using finite element method. The mechanical properties such as Young’s moduli, Poisson’s ratio, and yield stress under uniaxial loading of the resultant composite structures was studied and the effect of different fiber architectures on these properties was investigated. To this end, two broad types of architectures were used both having similar central main fiber but differing in either having only secondary fibers or additional tertiary fibers. The fiber and matrix volume fractions were kept constant and a comparative parametric study was carried out by varying the inclination of the secondary fibers. The results show that the elastic modulus of composite in the direction of main fiber increases linearly with increasing the angle of the secondary fibers. Furthermore, the elastic modulus is enhanced if the secondary fibers are closed, which mimics composites with closed cellular fibers. In contrast, the elastic modulus of composites normal to the main fiber ( x direction) exponentially decreases with the increase of the angle of the secondary fibers and it is little affected by having secondary fibers closed. Similar results were obtained for the yield stress of the composites. The results also indicate that Poisson’s ratio linearly increases with the secondary fiber angle. The results also show that for a constant fiber volume fraction, addition of various tertiary fibers may not significantly enhance the mechanical properties of the composites. The mechanical properties of the composites are mainly dominated by the secondary fibers. Finally, a simple model was proposed to predict these behaviors.

STUDYING THE EFFECT OF DIFFERENT ADDITIVES ON THE THERMAL CONDUCTIVITY AND MECHANICAL CHARACTERISTICS OF EPOXY-BASED COMPOSITE MATERIALS

2021 ◽  
Vol 25 (Special) ◽  
pp. 2-72-2-77
Author(s):  
Hassanein M. Nhoo ◽  
◽  
Raad. M. Fenjan ◽  
Ahmed A. Ayash ◽  
◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Thermal Conductivity ◽  
Particle Size ◽  
Tensile Strength ◽  
Mechanical Characteristics ◽  
Volume Fraction ◽  
Pyrolysis Process ◽  
Volume Percent ◽  
Fair Comparison ◽  
Filler Level

The current paper deals with investigating the effect of two different fillers on the thermal and mechanical characteristics of epoxy-based composite. The filler used throughout the study are: charcoal and Pyrex, both of them are different in nature and have not been investigated thoroughly or even compared fairly in terms of their effect on polymer matrix. Further, they can be considered as a cheap filler, charcoal can be obtained from a simple pyrolysis process of plants (charcoal) and Pyrex waste can be collected easily. Both types are added to the selected matrix with volume percent ranged from 10 to 60 with increments of 10. To ensure a fair comparison, the particle size is fixed (is about 1.7 micrometer). The results showed that the epoxy thermal conductivity has enhanced by about two orders of magnitudes over the studied range of filler. In terms of mechanical properties, the charcoal improves the tensile strength about 84% at 60% volume fraction while the Pyrex effect is about 40% at the same filler level. On the contrast, the results of compressive strength do not show an appreciable improvement overall. It decreases by about 12% at 60% volume fraction of charcoal while increases about the same percent with Pyrex at the same filler level.

Misalignment Error in Cancellous Bone Apparent Elastic Modulus Depends on Bone Volume Fraction and Degree of Anisotropy

2020 ◽  
Vol 143 (2) ◽  
Author(s):  
Matthew B. L. Bennison ◽  
A. Keith Pilkey ◽  
W. Brent Lievers
Keyword(s):  
Mechanical Properties ◽  
Elastic Modulus ◽  
Cancellous Bone ◽  
Volume Fraction ◽  
Experimental Studies ◽  
Bone Volume ◽  
Bone Volume Fraction ◽  
Skeletal Site ◽  
Degree Of Anisotropy ◽  
Misalignment Error

Abstract Cancellous bone is an anisotropic structure with architectural and mechanical properties that vary due to both skeletal site and disease state. This anisotropy means that, in order to accurately and consistently measure the mechanical properties of cancellous bone, experiments should be performed along the primary mechanical axis (PMA), that is, the orientation in which the mechanical properties are at their maximum value. Unfortunately, some degree of misalignment will always be present, and the magnitude of the resulting error is expected to be architecture dependent. The goal of this work is to quantify the dependence of the misalignment error, expressed in terms of change in apparent elastic modulus (ΔE), on both the bone volume fraction (BV/TV) and the degree of anisotropy (DA). Finite element method (FEM) models of bovine cancellous bone from five different skeletal sites were created at 5 deg and 20 deg from the PMA determined for each region. An additional set of models was created using image dilation/erosion steps in order to control for BV/TV and better isolate the effect of DA. Misalignment error was found to increase with increasing DA and decreasing BV/TV. At 5 deg misaligned from the PMA, error is relatively low (&lt;5%) in all cases but increases to 8–24% error at 20 deg. These results suggest that great care is needed to avoid introducing misalignment error into experimental studies, particularly when studying regions with high anisotropy and/or low bone volume fraction, such as vertebral or osteoporotic bone.

scholarly journals The Effect of Excess Carbon on the Crystallographic, Microstructural, and Mechanical Properties of CVD Silicon Carbide Fibers

2006 ◽  
Vol 982 ◽  
Author(s):  
James V Marzik ◽  
William J. Croft ◽  
Richard J. Staples ◽  
Warren J. MoberlyChan
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Silicon Carbide ◽  
Elastic Modulus ◽  
Chemical Vapor ◽  
High Strength ◽  
Excess Carbon ◽  
X Ray ◽  
Silicon Carbide Fibers ◽  
Sic Fiber

ABSTRACTSilicon carbide (SiC) fibers made by chemical vapor deposition (CVD) are of interest for organic, ceramic, and metal matrix composite materials due their high strength, high elastic modulus, and retention of mechanical properties at elevated processing and operating temperatures. The properties of SCS-6™ silicon carbide fibers, which are made by a commercial process and consist largely of stoichiometric SiC, were compared with an experimental carbon-rich CVD SiC fiber, to which excess carbon was added during the CVD process. The concentration, homogeneity, and distribution of carbon were measured using energy dispersive x-ray spectroscopy (SEM/EDS). The effect of excess carbon on the tensile strength, elastic modulus, and the crystallographic and microstructural properties of CVD silicon carbide fibers was investigated using tensile testing, x-ray diffraction, scanning electron microscopy (SEM), and transmission electron microscopy (TEM).

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