Effect of Si Content on Microstructure and Properties of 60Si2CrVA Spring Steel

2014 ◽  
Vol 968 ◽  
pp. 63-66 ◽  
Author(s):  
Fei Zhao ◽  
Zhan Ling Zhang ◽  
Jun Shuai Li ◽  
Cui Ye ◽  
Ni Li
Keyword(s):  
Mechanical Properties ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Testing Machine ◽  
Spring Steel ◽  
Impact Testing ◽  
X Ray ◽  
Comprehensive Properties ◽  
Spring Steels ◽  
Si Content

The microstructure and mechanical properties of the four spring steels with different Si content treated by Q-I-Q-T process were studied by metallographic microscope, MTS, impact testing machine and X-ray stress analyzer. The results show that the tensile strength and yield strength is first increased and then decreased with the increase of Si content, the volume fraction of retained austenite and elongation are fist decreased and then increased when the Si content is less than 2.1%, and the microstructure become finer and homogeneous. When Si content reaches 2.1%, the comprehensive properties of 60Si2CrVA spring steel is the best.

Fabrication and mechanical properties of Al/Al2O3 composite bodies by reactive infiltration of molten Al into SiO2 preform

2000 ◽  
Vol 15 (11) ◽  
pp. 2314-2321 ◽  
Author(s):  
Noboru Yoshikawa ◽  
Singo Funahashi ◽  
Shoji Taniguchi ◽  
Atsushi Kikuchi
Keyword(s):  
Mechanical Properties ◽  
Volume Fraction ◽  
Sintering Temperature ◽  
Pore Space ◽  
Pressure Infiltration ◽  
X Ray ◽  
Reactive Infiltration ◽  
Pore Size Distributions ◽  
Different Temperatures ◽  
Si Content

Al/Al2O3 composites were fabricated by a displacement reaction between SiO2 and molten Al. In this study, fabrication of Al/Al2O3 composites was attempted by means of reactive infiltration to provide variation of their mechanical properties. SiO2 preforms having various porosities and pore size distributions were prepared by sintering the powder at different temperatures between 1273 and 1723 K. Molten Al was infiltrated at 1373 K without application of pressure. Infiltration kinetics were studied and the microstructures of the composite bodies were observed by means of scanning electron microscopy (with energy dispersive x-ray microanalysis), wave dispersive x-ray microanalysis, and x-ray diffractions. The infiltrated specimens were mainly composed of Al and α–Al2O3 phases, and the Si content was less than 5 at.%. Volume fraction of Al phase in the composite bodies was not altered very much with the porosities of the SiO2 preforms because of the difficulty in filling out the entire pore space. Properties and microstructures of Al/Al2O3 composites, however, were dependent on the sintering temperature of the SiO2 preforms. In the case of low sintering temperature, a thick Al channel existed, which deformed upon compression. In the case of high sintering temperature, the microstructure became homogeneous and had thinner Al channels. The composite bodies became brittle. The deformation behavior was shown to be changed from ductile to brittle as an increase of the sintering temperature of the preforms.

Effect of Annealing Temperature on Austenite Stability of a δ-TRIP Steel

2019 ◽  
Vol 818 ◽  
pp. 82-86
Author(s):  
Xin Xu ◽  
Ren Dong Liu ◽  
Bao Yu Xu ◽  
Hong Liang Yi ◽  
Guo Dong Wang
Keyword(s):  
Mechanical Properties ◽  
Trip Steel ◽  
Retained Austenite ◽  
Annealing Temperature ◽  
Volume Fraction ◽  
X Ray Diffraction ◽  
X Ray ◽  
Austenite Stability ◽  
Poor Stability ◽  
Better Than

In this work, a novel type of δ-TRIP steel was designed, and the content and stability of retained austenite in δ-TRIP specimens under different annealing processes were detected and studied, respectively. The volume fraction of austenite was determined by X-ray diffraction (XRD). The microstructure and mechanical properties were analyzed systematically. The results show that a complex microstructure composed of three phases (ferrite, bainite and retained austenite) was obtained in the δ-TRIP steel. With the increasing of annealing temperature, both retained austenite and bainite content in the specimen increased, while the carbon content in retained austenite decreased, leading to a poor stability for retained austenite. Both tensile and yield strength improved with the increasing of annealing temperature, while the elongation reduced. The feature of retained austenite led to an excellent combination of ductility and strength, which was better than traditional TRIP steel.

Effect of Q-P-T Process on the Microstructure and Mechanical Properties of 300M Steel

2013 ◽  
Vol 749 ◽  
pp. 287-293 ◽  
Author(s):  
Rui Wen Zhao ◽  
Tian Qi Liu ◽  
Xin Qing Zhao
Keyword(s):  
Mechanical Properties ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Optical Microscope ◽  
X Ray Diffraction ◽  
X Ray ◽  
Microstructure And Mechanical Properties ◽  
300M Steel ◽  
The Difference ◽  
Evolution Of Microstructure

The effect of Quenching-Partitioning-Tempering (Q-P-T) process on the microstructure and mechanical properties of 300M steel were investigated. X-ray diffraction, scanning electron microscopy and optical microscope were employed to characterize the evolution of microstructure as well as the volume fraction of retained austenite. The results showed that the samples treated by Q-P-T possess more retained austenite compared with traditional Quenching-Tempering process. After Q-P-T, the strength increased slightly, while the ductility and toughness improved markedly. Microstructure analysis indicated the difference between Q-T and Q-P-T process lies in the amount of the retained austenite as well as the size and size distribution of the martensite laths. The Q-T resulted in a little of thin film-like retained austenite in addition to wide martensite strip, while the Q-P-T resulted in large amount of thick-like austenite accompanying narrow martensite strip. Therefore, 300M steel with better ductility and toughness could be obtained by Q-P-T heat treatment.

scholarly journals On the Q&P Potential of a Commercial Spring Steel

Metals ◽  
2021 ◽  
Vol 11 (10) ◽  
pp. 1612
Author(s):  
Markus Härtel ◽  
Alisa Wilke ◽  
Sebastian Dieck ◽  
Pierre Landgraf ◽  
Thomas Grund ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Electron Backscatter Diffraction ◽  
Tensile Tests ◽  
Spring Steel ◽  
Process Window ◽  
Compression Tests ◽  
Process Step

Over the last years heat treatment concept of “quenching and partitioning” (Q&P) has reached popularity for its ability to precisely adjust material properties to desired values. Mostly, Q&P process are applied on tailor-made materials with high purities or prototype alloys. The research in hand presents the whole routine of how to investigate the potential of a commercial 0.54C-1.45Si-0.71Mn spring steel in terms of Q&P heat treatment from lab scale in dilatometer measurements to widely used inductive heat treatment on larger scale. In order to obtain the small process window for this material we were focusing on the interplay of the formed microstructure and the resulting mechanical properties in hardness measurements, compression tests as well as tensile tests. After full austenitizing, three different Q&P processing routes were applied. Microstructural analyses by optical microscopy, Scanning Electron Microscopy (SEM) and Electron Backscatter Diffraction (EBSD) exhibit a condition with 6.4 % and 15 % volume fraction of fine distributed retained austenite. Interestingly, the 15 % of retained austenite developed during the partitioning heat treatment. Contradictory to our expectations, tensile and compression testing were showing that the 6.4 % condition achieved improved mechanical properties compared to the 15 % retained austenite condition. The remarkable conclusion is that not only volume fraction and fine distribution of retained austenite determines the potential of improving mechanical properties by Q&P in commercial alloys: also the process step when the retained austenite is developing as well as occurring parallel formation of carbides may strongly influence this potential.

Macroprobe Mode for the Study of Segregation in Steels

1990 ◽  
Vol 48 (2) ◽  
pp. 260-261
Author(s):  
Auclair Gilles ◽  
Benoit Danièle
Keyword(s):  
Mechanical Properties ◽  
Spatial Distribution ◽  
High Performance ◽  
Volume Fraction ◽  
Sheet Steel ◽  
Acquisition Time ◽  
Chemical Information ◽  
X Ray ◽  
Accurate Quantitative Analysis ◽  
Optical Micrographs

During these last 10 years, high performance correction procedures have been developed for classical EPMA, and it is nowadays possible to obtain accurate quantitative analysis even for soft X-ray radiations. It is also possible to perform EPMA by adapting this accurate quantitative procedures to unusual applications such as the measurement of the segregation on wide areas in as-cast and sheet steel products.The main objection for analysis of segregation in steel by means of a line-scan mode is that it requires a very heavy sampling plan to make sure that the most significant points are analyzed. Moreover only local chemical information is obtained whereas mechanical properties are also dependant on the volume fraction and the spatial distribution of highly segregated zones. For these reasons we have chosen to systematically acquire X-ray calibrated mappings which give pictures similar to optical micrographs. Although mapping requires lengthy acquisition time there is a corresponding increase in the information given by image anlysis.

Effect of Different Coiling Temperature on Mechanical Properties in Hot Rolled TRIP Steel

2011 ◽  
Vol 239-242 ◽  
pp. 1092-1095
Author(s):  
Xu Tao Gao ◽  
Ai Min Zhao ◽  
Zheng Zhi Zhao ◽  
Ming Ming Zhang ◽  
Di Tang
Keyword(s):  
Mechanical Properties ◽  
Retained Austenite ◽  
X Ray Diffraction ◽  
Coiling Temperature ◽  
Experimental Steel ◽  
Transformation Induced Plasticity ◽  
X Ray ◽  
Trip Steels ◽  
Hot Rolled ◽  
Scanning Electron

By means of optical microscopy(OM), scanning electron microscopy(SEM),X-ray diffraction(XRD),And tensile test, Mechanical Properties of hot rolled transformation -induced plasticity (TRIP) steels which were prepared through three different coiling temperature was investigated. Result reveals that the formability index of the experimental steel descends when the coiling temperature becomes low. Different coiling temperature has greater impact on retained austenite. Amount and carbon content of retained austenite in the experimental steel get less with lower coiling temperature.

Stress in Hydrogenated Microcrystalline Silicon Thin Films

1999 ◽  
Vol 557 ◽  
Author(s):  
D. Peiró ◽  
C. Voz ◽  
J. Bertomeu ◽  
J. Andreu ◽  
E. Martínez ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Vapor Deposition ◽  
Volume Fraction ◽  
Chemical Vapor ◽  
Hot Wire ◽  
X Ray Diffraction ◽  
Microcrystalline Silicon ◽  
X Ray ◽  
Silicon Thin Films ◽  
Abrupt Changes

AbstractHydrogenated microcrystalline silicon films have been obtained by hot-wire chemical vapor deposition (HWCVD) in a silane and hydrogen mixture at low pressure (<5 × 10-2 mbar). The structure of the samples and the residual stress were characterised by X- ray diffraction (XRD). Raman spectroscopy was used to estimate the volume fraction of the crystalline phase, which is in the range of 86 % to 98%. The stress values range between 150 and -140 MPa. The mechanical properties were studied by nanoindentation. Unlike monocrystalline wafers, there is no evidence of abrupt changes in the force-penetration plot, which have been attributed to a pressure-induced phase transition. The hardness was 12.5 GPa for the best samples, which is close to that obtained for silicon wafers.

Isothermal Transformation, Microstructure and Mechanical Properties of Ausformed Low-Carbon Carbide-Free Bainitic Steel

2018 ◽  
Vol 941 ◽  
pp. 329-333 ◽  
Author(s):  
Jiang Ying Meng ◽  
Lei Jie Zhao ◽  
Fan Huang ◽  
Fu Cheng Zhang ◽  
Li He Qian
Keyword(s):  
Mechanical Properties ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Bainitic Ferrite ◽  
Isothermal Transformation ◽  
Bainitic Transformation ◽  
Isothermal Treatment ◽  
Bainitic Steel ◽  
Low Carbon ◽  
Microstructure And Mechanical Properties

In the present study, the effects of ausforming on the bainitic transformation, microstructure and mechanical properties of a low-carbon rich-silicon carbide-free bainitic steel have been investigated. Results show that prior ausforming shortens both the incubation period and finishing time of bainitic transformation during isothermal treatment at a temperature slightly above the Mspoint. The thicknesses of bainitic ferrite laths are reduced appreciably by ausforming; however, ausforming increases the amount of large blocks of retained austenite/martenisite and decreases the volume fraction of retained austenite. And accordingly, ausforming gives rise to significant increases in both yield and tensile strengths, but causes noticeable decreases in ductility and impact toughness.

scholarly journals Novel Approach of Nanostructured Bainitic Steels’ Production with Improved Toughness and Strength

Materials ◽  
2020 ◽  
Vol 13 (5) ◽  
pp. 1220
Author(s):  
Peter Kirbiš ◽  
Ivan Anžel ◽  
Rebeka Rudolf ◽  
Mihael Brunčko
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Fine Structure ◽  
Retained Austenite ◽  
Bainitic Ferrite ◽  
High Hardness ◽  
Tensile Tests ◽  
Isothermal Transformation ◽  
Impact Testing ◽  
Bainitic Steels

The tendencies of development within the field of engineering materials show a persistent trend towards the increase of strength and toughness. This pressure is particularly pronounced in the field of steels, since they compete with light alloys and composite materials in many applications. The improvement of steels’ mechanical properties is sought to be achieved with the formation of exceptionally fine microstructures ranging well into the nanoscale, which enable a substantial increase in strength without being detrimental to toughness. The preferred route by which such a structure can be produced is not by applying the external plastic deformation, but by controlling the phase transformation from austenite into ferrite at low temperatures. The formation of bainite in steels at temperatures lower than about 200 °C enables the obtainment of the bulk nanostructured materials purely by heat treatment. This offers the advantages of high productivity, as well as few constraints in regard to the shape and size of the workpiece when compared with other methods for the production of nanostructured metals. The development of novel bainitic steels was based on high Si or high Al alloys. These groups of steels distinguish a very fine microstructure, comprised predominantly of bainitic ferrite plates, and a small fraction of retained austenite, as well as carbides. The very fine structure, within which the thickness of individual bainitic ferrite plates can be as thin as 5 nm, is obtained purely by quenching and natural ageing, without the use of isothermal transformation, which is characteristic for most bainitic steels. By virtue of their fine structure and low retained austenite content, this group of steels can develop a very high hardness of up to 65 HRC, while retaining a considerable level of impact toughness. The mechanical properties were evaluated by hardness measurements, impact testing of notched and unnotched specimens, as well as compression and tensile tests. Additionally, the steels’ microstructures were characterised using light microscopy, field emission scanning electron microscopy (FESEM) and high-resolution transmission electron microscopy (HRTEM). The obtained results confirmed that the strong refinement of the microstructural elements in the steels results in a combination of extremely high strength and very good toughness.

Mechanical Properties of PVC/ABS Composite Material

2011 ◽  
Vol 217-218 ◽  
pp. 1170-1173
Author(s):  
Wei Wei Qiao ◽  
Hui Wang ◽  
Yan Hua Zhao ◽  
Yi Xia Han
Keyword(s):  
Mechanical Properties ◽  
Composite Material ◽  
Testing Machine ◽  
Impact Testing ◽  
Elongation At Break ◽  
Poly Vinyl Chloride ◽  
Maximum Value ◽  
Material Testing Machine ◽  
The Impact ◽  
Butadiene Styrene

We investigate the mechanical properties of Poly Vinyl Chloride (PVC)/ acrylnitrile-butadiene-styrene copolymer (ABS) composite material with an impact testing machine，a material testing machine and other accessory devices. The result shows that the mechanical properties of PVC/ABS composite are a function of composition, the addition of ABS improved the mechanical properties of PVC/ ABS composite，the impact strength and elongation at break rise significantly with increasing ABS content in PVC/ABS composite and appears maximum value，While the tensile strength and modulus almost decrease monotonously with increasing ABS content in PVC/ABS composite.

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