Microstructure and tribological property of self-lubrication CBN abrasive composites containing molybdenum disulfide

2019 ◽  
Vol 71 (5) ◽  
pp. 712-717 ◽  
Author(s):  
Biao Zhao ◽  
Wenfeng Ding ◽  
Weijie Kuang ◽  
Yucan Fu
Keyword(s):  
Friction Coefficient ◽  
Flexural Strength ◽  
Molybdenum Disulfide ◽  
Tribological Property ◽  
Cubic Boron Nitride ◽  
Three Dimensional ◽  
Optical Microscope ◽  
Transgranular Fracture ◽  
Vacuum Sintering ◽  
Content Type

Purpose This paper aims to evaluate the influence of molybdenum disulfide (MoS2) concentrations (5, 7.5, 10, 12.5 and 15 Wt.%) on the microstructure and tribological property of the self-lubrication cubic boron nitride (CBN) abrasive composites. Design/methodology/approach Three point bending method and rotating sliding test are used to evaluate the flexural strength and tribological property of self-lubricating CBN abrasive composites. Microstructure, wear morphology of the ball and scratch are supported by scanning electron microscopy, optical microscope and three-dimensional confocal microscopy, etc. Findings The MoS2 concentration has a significant influence on the interface microstructure between CBN abrasives and matrix alloys, and thus, affects the flexural strength of CBN abrasive composites. The grain fracture modes of CBN abrasive composites are transformed from the transgranular fracture into intergranular fracture as the MoS2 concentrations increase. Additionally, the friction coefficient of as-sintered samples decreases with the MoS2 concentrations. The MoS2 concentrations of 10 Wt.% are final determined to fabricate self-lubricating composites in basis of the mechanical and lubricating property. Originality/value The ball is fabricated under vacuum sintering process. The tribological property of self-lubricating CBN abrasive composites is evaluated in terms of the friction coefficient and morphologies of the ball and scratches after rotating sliding tests.

A comparison of the marginal fit and mechanical properties of a zirconia dental crown using CAM and 3DSP

2019 ◽  
Vol 25 (7) ◽  
pp. 1187-1197 ◽  
Author(s):  
Huang-Jan Hsu ◽  
Shyh-Yuan Lee ◽  
Cho-Pei Jiang ◽  
Richard Lin
Keyword(s):  
Flexural Strength ◽  
Three Dimensional ◽  
Optical Microscope ◽  
Dental Restoration ◽  
Solvent Free ◽  
Clinical Use ◽  
Green Body ◽  
Marginal Gap ◽  
Marginal Fit ◽  
Content Type

Purpose This study aims to compare the marginal fit, flexural strength and hardness for a ceramic premolar that is constructed using dental computer aided machining (CAM) and three-dimensional slurry printing (3DSP). Design/methodology/approach Dental CAM and 3DSP are used to fabricate a premolar model. To reduce the fabrication time for 3DSP, a new composition of solvent-free slurry is proposed. Before it is fabricated, the dimensions of the green body for the premolar model are enlarged to account for the shrinkage ratio. A two-stage sintering process ensures accurate final dimensions for the premolar model. The surface morphology of the green body and the sintered premolars that are produced using the two methods is then determined using scanning electronic microscopy. The sintered premolars are seated on a stone model to determine the marginal gap using an optical microscope. The hardness and the flexural strength are also measured for the purpose of comparison. Findings The developed solvent-free slurry for 3DSP can be used to produce a premolar green body without micro-cracks or delamination. The maximal marginal gap for the sintered premolar parts that are constructed using the green bodies from dental CAM is 98.9 µm and that from 3DSP is 72 µm. Both methods produce a highly dense zirconia premolar using the same sintering conditions. The hardness value for the dental CAM group is 1238.8 HV, which is slightly higher than that for the 3DSP group (1189.4 HV) because there is a difference in the pre-processing of the initial ceramic materials. However, the flexural strength for 3DSP is 716.76 MPa, which is less than the requirement for clinical use. Originality/value This study verifies that 3DSP can be used to fabricate a zirconia dental restoration device that is as good as the one that is produced using the dental CAM system and which has a marginal gap that is smaller than the threshold value. The resulting premolar restoration devices that are produced by sintering the green bodies that are produced using 3DSP and dental CAM under the same conditions have a similar hardness value, which is four times greater than that of enamel. The flexural strength of 3DSP does not meet the requirement for clinical use.

scholarly journals Tribological Properties of Molybdenum Disulfide and Helical Carbon Nanotube Modified Epoxy Resin

Materials ◽  
2019 ◽  
Vol 12 (6) ◽  
pp. 903 ◽  
Author(s):  
Zhiying Ren ◽  
Yu Yang ◽  
Youxi Lin ◽  
Zhiguang Guo
Keyword(s):  
Elastic Modulus ◽  
Friction Coefficient ◽  
Epoxy Resin ◽  
Molybdenum Disulfide ◽  
Tribological Properties ◽  
Testing Machine ◽  
Three Dimensional ◽  
Friction Testing ◽  
Helical Carbon Nanotubes ◽  
Modified Epoxy

In this study, epoxy resin (EP) composites were prepared by using molybdenum disulfide (MoS2) and helical carbon nanotubes (H-CNTs) as the antifriction and reinforcing phases, respectively. The effects of MoS2 and H-CNTs on the friction coefficient, wear amount, hardness, and elastic modulus of the composites were investigated. The tribological properties of the composites were tested using the UMT-3MT friction testing machine, non-contact three-dimensional surface profilometers, and nanoindenters. The analytical results showed that the friction coefficient of the composites initially decreased and then increased with the increase in the MoS2 content. The friction coefficient was the smallest when the MoS2 content in the EP was 6%, and the wear amount increased gradually. With the increasing content of H-CNTs, the friction coefficient of the composite material did not change significantly, although the wear amount decreased gradually. When the MoS2 and H-CNTs contents were 6% and 4%, respectively, the composite exhibited the minimum friction coefficient and a small amount of wear. Moreover, the addition of H-CNTs significantly enhanced the hardness and elastic modulus of the composites, which could be applied as materials in high-temperature and high-pressure environments where lubricants and greases do not work.

The study of friction layer and tribological property of PI–matrix composites

2017 ◽  
Vol 69 (2) ◽  
pp. 267-275 ◽  
Author(s):  
Xiulin Xu ◽  
Xing Lu ◽  
Zuoxiang Qin ◽  
Dalong Yang
Keyword(s):  
Friction Coefficient ◽  
Tribological Property ◽  
Wear Debris ◽  
Friction Pair ◽  
Matrix Composites ◽  
Low Friction ◽  
Friction Layer ◽  
Content Type ◽  
Compact Zone ◽  
Pin On Disk

Purpose This paper aims to study the friction layer and tribological property of polyimide (PI)–matrix composites under different friction speeds. Design/methodology/approach Friction tests were conducted under friction speeds ranging from 20-120 km/h and pressure of 0.57 MPa by a pin-on-disk tribometer. Findings The results indicate that the friction coefficient decreases with the increasing of the friction speed. Under different friction speeds, the structure of the friction layer and debris are different, which affects the actual tribological performance of the composites. At low friction speed, the morphology of the friction layer is mainly particulate. The higher level of clenching action between the friction pair leads to a high friction coefficient, and the morphology of the particles in the particulate zone and the wear debris are mostly equiaxial particles. At high friction speed, the morphology of the friction layer is mainly a compact zone. The reduction of the surface roughness leads to a low friction coefficient. The debris collected on the counter surface at high friction speeds are mostly big sheets, and the morphology of the particles in the particulate zone is mostly rod-like. Controlling the conditions of the disk and the pin can reveal the influence of friction speed on the friction layer. The wear mechanisms at different friction speeds are also discussed. Originality/value By controlling the conditions of the disk and the pin to reveal the influence of friction speed on the friction layer, and the evolutions of the friction layer, wear debris were carefully inspected with the aim of demonstrating the relationship between friction speed and wear mechanism of PI–matrix composites.

Investigation on spatial distribution and evolution features of the running-in attractor based on a new approach

2018 ◽  
Vol 70 (9) ◽  
pp. 1636-1641
Author(s):  
Cong Ding ◽  
Hua Zhu ◽  
Guodong Sun ◽  
Chun Ling Wei ◽  
Yu Jiang
Keyword(s):  
Spatial Distribution ◽  
Friction Coefficient ◽  
Design Methodology ◽  
Three Dimensional ◽  
New Approach ◽  
Dynamic Behaviors ◽  
Content Type ◽  
Evolution Rule ◽  
Uniform State ◽  
Variation Tendency

Purpose The purpose of this work is to comprehensively reveal the spatial distribution and evolution features of a running-in attractor. Design/methodology/approach The friction coefficient signals extracted from wear experiments are reconstructed. A projected matrix is obtained based on the reconstructed matrix. Then the approach of three-dimensional (3D) histogram of phase points is proposed, which is used to intuitively characterize the complex properties of the running-in attractor. Findings The space occupied by the running-in attractor gradually contracts, then stabilizes and finally expands; the maximum of phase points number in a certain bin initially decreases, then keeps stable and finally increases rapidly; yet the percentage of bins number storing phase points shows an inverse variation tendency. Consequently, 3D histogram evolves from a nonuniform state to a uniform state then returns back to the nonuniform state, which indicates the evolution rule of “formation, stabilization and disappearance” of the running-in attractor. Originality/value Characterization on the features of the running-in attractor can provide valuable information about friction systems and their dynamic behaviors.

Development of polycaprolactone/hydroxyapatite composite resin for 405 nm digital light projection 3D printing

2020 ◽  
Vol 26 (5) ◽  
pp. 951-958
Author(s):  
Yuan-Min Lin ◽  
Hsuan Chen ◽  
Chih-Hsin Lin ◽  
Pin-Ju Huang ◽  
Shyh-Yuan Lee
Keyword(s):  
Composite Materials ◽  
3D Printing ◽  
Flexural Strength ◽  
Layer Structure ◽  
Resin Composite ◽  
Flexural Modulus ◽  
Three Dimensional ◽  
Surface Element ◽  
Layer By Layer ◽  
Content Type

Purpose The purpose of this study is to develop resin composite materials composed of polycaprolactone (PCL) acrylates and hydroxyapatite (HA) nanoparticles for ultraviolet digital light projection (DLP) three-dimensional (3D) printing technique. Design/methodology/approach Two PCL-based triacrylates, namely, glycerol-3 caprolactone-triacrylate (Gly-3CL-TA) and glycerol-6 caprolactone-triacrylate (Gly-6CL-TA) were synthesized from ring-opening polymerization of ε-caprolacton monomer in the presence of glycerol and then acrylation was performed using acryloyl chloride. 3D printing resins made of Gly-3CL-TA or Gly-6CL-TA, 5% HA and 3% of photoinitiator 2,4,6-Trimethylbenzoyl-diphenyl-phosphineoxide were then formulated. The surface topography, surface element composition, flexural strength, flexural modulus, cytotoxicity and degradation of the PCL-based scaffolds were then characterized. Findings Resin composite composed of Gly-3CL-TA or Gly-6CL-TA and 5% (w/w) of HA can be printed by 405 nm DLP 3D printers. The former has lower viscosity and thus can form a more uniform layer-by-layer structure, while the latter exhibited a higher flexural strength and modulus after being printed. Both composite materials are non-cytotoxic and degradable. Originality/value This study provides a direction of the formulation of environment-friendly resin composite for DLP 3D printing. Both resin composites have huge potential in tissue engineering applications.

scholarly journals Hybrid multi-layered scaffolds produced via grain extrusion and electrospinning for 3D cell culture tests

2019 ◽  
Vol 26 (3) ◽  
pp. 593-602
Author(s):  
Paola Ginestra ◽  
Stefano Pandini ◽  
Elisabetta Ceretti
Keyword(s):  
Cell Attachment ◽  
Three Dimensional ◽  
3D Culture ◽  
3D Cell Culture ◽  
Optical Microscope ◽  
Biological Interactions ◽  
Compression Tests ◽  
Content Type ◽  
Extrusion Head ◽  
Mechanical Performances

Purpose The purpose of this paper is to focus on the production of scaffolds with specific morphology and mechanical behavior to satisfy specific requirements regarding their stiffness, biological interactions and surface structure that can promote cell-cell and cell-matrix interactions though proper porosity, pore size and interconnectivity. Design/methodology/approach This case study was focused on the production of multi-layered hybrid scaffolds made of polycaprolactone and consisting in supporting grids obtained by Material Extrusion (ME) alternated with electrospun layers. An open source 3D printer was utilized, with a grain extrusion head that allows the production and distribution of strands on the plate according to the designed geometry. Square grid samples were observed under optical microscope showing a good interconnectivity and spatial distribution of the pores, while scanning electron microscope analysis was used to study the electrospun mats morphology. Findings A good adhesion between the ME and electrospinning layers was achieved by compression under specific thermomechanical conditions obtaining a hybrid three-dimensional scaffold. The mechanical performances of the scaffolds have been analyzed by compression tests, and the biological characterization was carried out by seeding two different cells phenotypes on each side of the substrates. Originality/value The structure of the multi-layered scaffolds demonstrated to play an important role in promoting cell attachment and proliferation in a 3D culture formation. It is expected that this design will improve the performances of osteochondral scaffolds with a strong influence on the required formation of an interface tissue and structure that need to be rebuilt.

Stereotactic radiosurgery versus stereotactic radiotherapy for patients with vestibular schwannoma: a Leksell Gamma Knife Society 2000 debate

2000 ◽  
Vol 93 (supplement_3) ◽  
pp. 90-92 ◽  
Author(s):  
Mark E. Linskey
Keyword(s):  
Gamma Knife ◽  
Stereotactic Radiotherapy ◽  
Three Dimensional ◽  
Late Recurrence ◽  
Vestibular Schwannomas ◽  
Tumor Control ◽  
Complication Rates ◽  
Content Type ◽  
Single Fraction ◽  
Fine Print

✓ By definition, the term “radiosurgery” refers to the delivery of a therapeutic radiation dose in a single fraction, not simply the use of stereotaxy. Multiple-fraction delivery is better termed “stereotactic radiotherapy.” There are compelling radiobiological principles supporting the biological superiority of single-fraction radiation for achieving an optimal therapeutic response for the slowly proliferating, late-responding, tissue of a schwannoma. It is axiomatic that complication avoidance requires precise three-dimensional conformality between treatment and tumor volumes. This degree of conformality can only be achieved through complex multiisocenter planning. Alternative radiosurgery devices are generally limited to delivering one to four isocenters in a single treatment session. Although they can reproduce dose plans similar in conformality to early gamma knife dose plans by using a similar number of isocenters, they cannot reproduce the conformality of modern gamma knife plans based on magnetic resonance image—targeted localization and five to 30 isocenters. A disturbing trend is developing in which institutions without nongamma knife radiosurgery (GKS) centers are championing and/or shifting to hypofractionated stereotactic radiotherapy for vestibular schwannomas. This trend appears to be driven by a desire to reduce complication rates to compete with modern GKS results by using complex multiisocenter planning. Aggressive advertising and marketing from some of these centers even paradoxically suggests biological superiority of hypofractionation approaches over single-dose radiosurgery for vestibular schwannomas. At the same time these centers continue to use the term radiosurgery to describe their hypofractionated radiotherapy approach in an apparent effort to benefit from a GKS “halo effect.” It must be reemphasized that as neurosurgeons our primary duty is to achieve permanent tumor control for our patients and not to eliminate complications at the expense of potential late recurrence. The answer to minimizing complications while maintaining maximum tumor control is improved conformality of radiosurgery dose planning and not resorting to homeopathic radiosurgery doses or hypofractionation radiotherapy schemes.

Study on high-temperature wear and mechanism of Al-Si/graphite composites prepared by the die-casting process

2020 ◽  
Vol 72 (10) ◽  
pp. 1153-1158 ◽  
Author(s):  
Yafei Deng ◽  
Xiaotao Pan ◽  
Guoxun Zeng ◽  
Jie Liu ◽  
Sinong Xiao ◽  
...  
Keyword(s):  
Friction Coefficient ◽  
Wear Rate ◽  
Peer Review ◽  
Die Casting ◽  
Casting Machine ◽  
Injection Pressure ◽  
Casting Process ◽  
Matrix Alloy ◽  
Content Type ◽  
The Matrix

Purpose This paper aims to improve the tribological properties of aluminum alloys and reduce their wear rate. Design/methodology/approach Carbon is placed in the model at room temperature, pour 680°C of molten aluminum into the pressure chamber, and then pressed it into the mold containing carbon felt through a die casting machine, and waited for it to cool, which used an injection pressure of 52.8 MPa and held the same pressure for 15 s. Findings The result indicated that the mechanical properties of matrix and composite are similar, and the compressive strength of the composite is only 95% of the matrix alloy. However, the composite showed a low friction coefficient, the friction coefficient of Gr/Al composite is only 0.15, which just is two-third than that of the matrix alloy. Similarly, the wear rate of the composite is less than 4% of the matrix. In addition, the composite can avoid severe wear before 200°C, but the matrix alloy only 100°C. Originality/value This material has excellent friction properties and is able to maintain this excellent performance at high temperatures. Peer review The peer review history for this article is available at: https://publons.com/publon/10.1108/ILT-10-2019-0454/

scholarly journals Polarization-sensitive photodetectors based on three-dimensional molybdenum disulfide (MoS2) field-effect transistors

Nanophotonics ◽  
2020 ◽  
Vol 9 (16) ◽  
pp. 4719-4728
Author(s):  
Tao Deng ◽  
Shasha Li ◽  
Yuning Li ◽  
Yang Zhang ◽  
Jingye Sun ◽  
...  
Keyword(s):  
Molybdenum Disulfide ◽  
Field Effect ◽  
High Performance ◽  
Field Effect Transistors ◽  
Three Dimensional ◽  
Polarized Light ◽  
Optical Field ◽  
Two Dimensional ◽  
Polarization Ratio ◽  
Two Dimensional Materials

AbstractThe molybdenum disulfide (MoS2)-based photodetectors are facing two challenges: the insensitivity to polarized light and the low photoresponsivity. Herein, three-dimensional (3D) field-effect transistors (FETs) based on monolayer MoS2 were fabricated by applying a self–rolled-up technique. The unique microtubular structure makes 3D MoS2 FETs become polarization sensitive. Moreover, the microtubular structure not only offers a natural resonant microcavity to enhance the optical field inside but also increases the light-MoS2 interaction area, resulting in a higher photoresponsivity. Photoresponsivities as high as 23.8 and 2.9 A/W at 395 and 660 nm, respectively, and a comparable polarization ratio of 1.64 were obtained. The fabrication technique of the 3D MoS2 FET could be transferred to other two-dimensional materials, which is very promising for high-performance polarization-sensitive optical and optoelectronic applications.

scholarly journals Is Micro X-ray Computer Tomography a Suitable Non-Destructive Method for the Characterisation of Dental Materials?

Polymers ◽  
2021 ◽  
Vol 13 (8) ◽  
pp. 1271
Author(s):  
Andreas Koenig ◽  
Leonie Schmohl ◽  
Johannes Scheffler ◽  
Florian Fuchs ◽  
Michaela Schulz-Siegmund ◽  
...  
Keyword(s):  
Flexural Strength ◽  
Computer Tomography ◽  
Mechanical Performance ◽  
Dental Materials ◽  
Three Dimensional ◽  
X Rays ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Multiple Measurements ◽  
High Doses

The aim of the study was to investigate the effect of X-rays used in micro X-ray computer tomography (µXCT) on the mechanical performance and microstructure of a variety of dental materials. Standardised bending beams (2 × 2 × 25 mm3) were forwarded to irradiation with an industrial tomograph. Using three-dimensional datasets, the porosity of the materials was quantified and flexural strength was investigated prior to and after irradiation. The thermal properties of irradiated and unirradiated materials were analysed and compared by means of differential scanning calorimetry (DSC). Single µXCT measurements led to a significant decrease in flexural strength of polycarbonate with acrylnitril-butadien-styrol (PC-ABS). No significant influence in flexural strength was identified for resin-based composites (RBCs), poly(methyl methacrylate) (PMMA), and zinc phosphate cement (HAR) after a single irradiation by measurement. However, DSC results suggest that changes in the microstructure of PMMA are possible with increasing radiation doses (multiple measurements, longer measurements, higher output power from the X-ray tube). In summary, it must be assumed that X-ray radiation during µXCT measurement at high doses can lead to changes in the structure and properties of certain polymers.

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