scholarly journals Optimization Model on the Effect of Clove Oil, Formaldehyde, and Chitosan Added to Batik Fabric Colored with Gambier (Uncaria gambir Roxb): Antifungal Properties and Stability

2019 ◽  
Vol 20 (1) ◽  
pp. 210 ◽  
Author(s):  
Edia Rahayuningsih ◽  
Felix Arie Setiawan ◽  
Conny Julanda Ayanie ◽  
Ambrosius Aditya Antoko ◽  
Yosephine Intan Ayuningtyas ◽  
...  

Triggered by the concept of sustainability, the use of natural dyes in batik fabric processing has increased recently. To inhibit fungus growth on batik fabric colored with natural dyes, either clove oil or formaldehyde was added as an antifungal agent. To increase the stability of the interaction between the antifungal agent and the batik fabric, chitosan was used as a crosslinker. A modified version of the standard tests American Association of Textile Chemists and Colorists (AATCC) 30 and Response Surface Methodology (RSM) was applied as the characterization method. The results showed that the growth percentage of fungi in Batik treated with either clove oil or formaldehyde was much lower than that in the control sample. Growth of Aspergillus niger could be prevented by about 32% using clove oil and 94% using formaldehyde. The optimal condition was obtained with 1% chitosan as a crosslinking reagent, 15.91 ppm of formaldehyde, and 60-min immersion time, with absorbance intensity of formaldehyde crosslinking solution and fungus growth areas being 0.159 and 2.47%, respectively.

2020 ◽  
Vol 36 (05) ◽  
pp. 879-888
Author(s):  
Ziad Ayyad ◽  
Muhannad Qurie ◽  
Amal Odeh Natshe ◽  
Saleh Sawalha ◽  
Fuad Al-Rimawi

The stability of virgin olive oil (VOO) used as a packing medium for traditional concentrated Yoghurt decreased during time and the product could deteriorate during the storage time. In this investigation, different natural additives such as dried Arum Palaestinum leaves (AP), Tomato Peel (TP) and Chili Pepper (CP) have been used to enhance the quality and stability of packing medium VOO for traditional canned concentrated Yoghurt balls. Parts VOO samples added with natural additives were stored as packing medium for traditional canned concentrated Yoghurt balls. Other part was stored without concentrated Yoghurt in the same storage conditions. All samples were analyzed for their initial quality indexes and during the storage period of six months. At the end of storage, results revealed that the % acidity for all VOO samples used as a packing medium showed a higher value than the samples stored without concentrated Yoghurt balls. On the other side, peroxide values for all stored samples of both parts were less than the control sample without additives. Extinction coefficients (K232, K270) for VOO samples with the natural additives showed increased trend during the storage time, but it didn't exceed the accepted limit for VOO. Total phenol content for all samples were gradually decreased during storage period, whereas samples with the natural additives showed higher values than the controls. All the natural additives (CP, TP, AP) showed a positive trend in enhancing and improving the different VOO quality indexes in our study in particular those samples added with CP during the storage time.


KOVALEN ◽  
2020 ◽  
Vol 6 (3) ◽  
pp. 212-217
Author(s):  
Khairuddin ◽  
Joy Noldy Baciang ◽  
Indriani ◽  
Nov Irmawati Inda

Research on the extraction and stability test of natural dye from red spinach (Alternanthera amoena Voss) has been carried out. This study aims to determine the effect of pH and length of sun exposure on the stability of the dye from red spinach. Extraction using the maceration method with ethanol solvent and measurement using a UV-Vis spectrophotometer. Stability testing is carried out at pH 2-5 and sun exposure for 1-4 hours using a dark and light container. The results obtained, at pH 2 and pH 3, anthocyanins were more stable, compared to pH 4 and 5 which had greater color degradation. In exposure to sunlight, dark containers with a degradation percentage of 31.70% were better than clear containers with a percentage of 48.78%. Keywords: Anthocyanin, red spinach, natural dyes stability.


2016 ◽  
Vol 47 (4) ◽  
Author(s):  
Jebur & et al.

This study was aimed to know the efficiency of partially purified L- asparaginase produced from local isolate from Erwinia spp. to reduce the percentage of acrylamide formed in Biscuit. Four types of biscuit from wheat flour were prepared (T1, T2, T3, T4),and T1 as control. High performance liquid chromatography technique was used to estimate acrylamide ratio in biscuit , Effect of enzyme addition  on flour chemical and rheological properties was studied, also dough behavior ,gluten percentage, water absorption and amylase enzyme activity was estimated. The results revealed  that  the  addition of  experimental asparaginase ( specific activity 20.5 unite mg-1 ) with 1% of flour weight lead to reduce in acrylamide formation in Biscuit  to 89 %  compared  to  control sample ( in absence of enzyme ) . Moreover, the addition of Asparagine to flour at 0.1 % of its weight, where L- asparaginase was available caused a negative effect on enzyme efficiency in reducing the acrylamide in biscuit. So the level of acrylamide was reduced to 57.7 %. In the other hand , the percentage of acryl amide in biscuit was increased to   233 % when the asparagine was added to mixture in absence of L- asparaginase .Addition of  the enzyme to flour have no effect on the percentage value of gluten but improved the  stability of dough .The  enzyme  addition also led to increase amylases activities.  Addition of experimental enzyme had no effect on quality and sensory evaluation of biscuit.


2021 ◽  
Vol 23 (1) ◽  
pp. 85
Author(s):  
Rocío Díaz-Ruiz ◽  
Amanda Laca ◽  
Marta Sánchez ◽  
Manuel Ramón Fernández ◽  
María Matos ◽  
...  

Trans-resveratrol (RSV) needs to be encapsulated to maintain its beneficial properties on the human body. This is due to its extreme photosensitivity, short biological half-life, and easy oxidation. In this study, the use of double emulsions for RSV encapsulation and their further application on functional yoghurts was studied. Different types of yoghurts were prepared: with and without RSV and with two types of volumetric emulsion formulations (20/80 and 30/70). In order to study the influence of the addition of double emulsions to the physical properties of the prepared yoghurts, they were characterised fresh and after a month under storage at 4 °C, in terms of droplet size, morphology, stability, rheology, texturometry, colorimetry, and antioxidant capacity. Results obtained showed that the presence of emulsion in the yoghurts produced a generalised decrease in the predominant droplet size (from 48 µm to 15–25 µm) and an increase in the stability. Additionally, a predominantly elastic character was observed. The firmness values obtained were very similar for all the yoghurts analysed and did not suffer important modifications with time. A slight colour variation was observed with storage time in the control sample, whereas a more notable variation in the case of emulsion yoghurts was observed. An appreciable increase of the antioxidant capacity of the final functional yoghurt (100 g) was observed when it contained 5–8 mg of RSV. Encapsulated RSV added to yoghurts presented a larger protection against RSV oxidation compared with free RSV, presenting a larger antioxidant inhibition after one month of storage. Moreover, the antioxidant capacity of yoghurts with encapsulated RSV was not affected under storage, since slight reductions (3%) were registered after one month of storage at 4 °C.


2021 ◽  
Vol 59 (1) ◽  
Author(s):  
Camila Verly de Miranda Sabino ◽  
Bárbara Janaína Paula da Silva ◽  
Danielle Lima Bezerra de Menezes ◽  
Felipe Moura Araújo da Silva ◽  
Tatiane Pereira de Souza ◽  
...  

Research background. The current commercial scenario indicates an increase in the demand for natural dyes. Compared to synthetic dyes, natural ones have the advantage of being sustainable, making them of great interest for the food and cosmetic industries. The development of new natural dyes is necessary, as well as the carrying out of complementary research regarding the existing ones. Experimental approach. The present study aimed to characterize the chemical and physicochemical characteristics of the dehydrated endocarp of the genipap (Genipa americana) fruit, as well as performing the relevant stability and cytotoxicity tests. The chemical characterization was performed by LC/MS/MS analyses. The stability studies were carried out by spectrophotometry and cytotoxicity assays using cell culture and fluorometric methods. Results and conclusions. After dehydration and milling of the fruit's endocarp, a powder was obtained, which with 20 % water was used to extract the dye. Five compounds were elucidated using HPLC-MS and confirmed the presence of the geniposide as its main compound. Via the X-ray diffraction test and electron microscopy analysis, it was possible to describe the powder obtained as being amorphous and of porous structure with a variable size, respectively. The thermogravimetric analysis indicated a maximum loss of 61 % mass after exposure to a temperature range of 240 °C to 760 °C. The obtained blue dye showed to be stable in the absence of light, at room temperature and presented neutral pH. In the cytotoxicity assay, 95.05±1.33 % of viable human fibroblast were observed after exposure to this dye. The genipap fruit can be a viable alternative for the obtention of natural blue dye, since it is easy to obtain and has very low toxicity for food, pharmaceutical or cosmetic industries. Novelty and scientific contribution. This study demonstrates for the first time the physicochemical and biological properties of a natural blue dye from G. americana fruit.


2021 ◽  
Vol 921 (1) ◽  
pp. 012067
Author(s):  
D R G Kabo ◽  
M Tumpu ◽  
H Parung

Abstract One of the treatments that can be given to asphalt mixtures to determine the durability of the mixture is by water immersion. This study aims to analyze the stability value of Marshall mixture of AC-WC (Asphalt Concrete Wearing Course) by using modified Asbuton as a binder and gondorukem as added material due to water immersion. The method used in this research is experimental in the laboratory. AC-WC mixture is produced using modified Asbuton as a binder (Retona Blend 55) at optimum asphalt content of 6.25% and gondorukem as an additive at 0.0% and 2.5% content. The treatment given to the mixture is by soaking water for 0, 1, 3 and 7 days. The treatment given to the mixture is by soaking water for 0, 1, 3 and 7 days. The results showed that the Marshall stability value decreased with increasing water immersion time. Decrease in Marshall stability values that occur in specimens with immersion time of 1, 3 and 7 days for specimens without immersion are 21.34%, 25.56% and 28.25%, respectively.


2020 ◽  
Vol 21 (10) ◽  
Author(s):  
Silvi Ikawati ◽  
Toto Himawan ◽  
Abdul Latief Abadi ◽  
Hagus Tarno

Abstract. Ikawati S, Himawan T, Abadi AL, Tarno H. 2020. Thermostability, photostability, and toxicity of clove oil nanoparticles against Cryptolestes ferrugineus (Stephens) (Coleoptera: Laemophloeidae). Biodiversitas 21: 4764-4771. Problems related to the essential oils as insecticides are their volatility, poor solubility in water and environmental degradation (such as caused by high temperatures and UV light) which can adversely affect the application. An ideal botanical insecticide formulation would maintain the level of the main compounds adequate for pest control. This study was to evaluate the stability of polyethylene glycol (PEG) coated nanoparticles loaded with clove (Syzygium aromaticum) essential oil to high temperature and UV light also their toxicity to C. ferrugineus. There is a reduction in nanoparticle size after heating from 257 to 173 nm and there is no difference in size distribution. After heating and UV-light treatment, eugenol content in free clove oil decreased significantly, while on nanoparticles there were not significantly changed, that indicated greater stability on the nanoformulation. The median lethal concentration (LC50) of CO-NPs to C. ferrugineus adults value for 72 and 120 hours was 0.734 and 0.676%.


Author(s):  
Marjan Ashegh Moalla ◽  
Mahboobeh Mahmoodi ◽  
Masoumeh Tabatabaee

Introduction: Ginger is a plant that is used as a drug for pain relieving and anti-inflammatory in traditional medicine, but conventional prescribing of it faces serious challenges. One way to overcome these problems is the loading of ginger extract in polymer carriers. The aim of this study was characterization and evaluation of the loading and releasing of ginger extract from hyaluronic acid nanocapsules for medical applications. Methods: In this applied study, ginger extract as a pain-relieving drug was loaded in hyaluronic acid nanocapsules. The hyaluronic acid nanocapsules containing ginger extract were fabricated by emulsion method. The surface morphology, particle size and zeta potential, surface roughness and functional groups on the sample surface were evaluated by field emission electron microscopy (FESEM), dynamic light scattering (DLS), atomic force microscopy (AFM) and fourier transform infrared spectroscopy (FTIR), respectively. The stability and ginger release from nanocapsules were also determined via DLS and HPLC, respectively. The toxicity and fibroblast cells viability of ginger extract encapsulated in hyaluronic acid were evaluated by MTT assay. Data were analyzed by SPSS 16 Software. The t-Student test was performed for statistical comparison of data and statistically significant was P < 0.05. Results: The ginger entrapment efficiency (EE %) in nanocapsules was 74%.  The average particle diameter and charge surface of the samples were calculated 413 nm and -10 mV, respectively. The negative charge of samples showed the stability of samples without agglomeration. Therefore, the surface morphology of the samples was observed as relatively spherical particles. In vitro test showed 95% fibroblast cell growth and proliferation on nanocapsules compared to the control sample (P < 0.05). Conclusion: The hyaluronic acid nanocapsules have a great potential for delivery of ginger extract in the area of pain and inflammation.


Author(s):  
Saraladevi V ◽  
Ravichandran S ◽  
Bhavani J ◽  
Satheesh Kumar D ◽  
Chandrasekaran A R ◽  
...  

Teeth and mouth are the supportive organs to enable us in doing all the functions of the body by consuming. So, cleanliness of the oral areas is important for the healthy and nourished body which is devoid of microorganisms. Herbs have been in the investigations for the antibacterial and antiviral properties along with the history of the medical systems. They were effective and safer relative to the available synthetic drugs. Three formulations of gargle were prepared using Extract of Neem, Aloe Gel and clove oil which were named as GNF, GAF and GCF. The physical parameters were estimated, such as pH and one formulation failed in the stability study. The prepared GNF and GAF showed better antibacterial activity against the bacteria extracted by swabbing the mouth and also the three strains like E coil, Streptomyces and staphylococcus.


Coatings ◽  
2019 ◽  
Vol 9 (1) ◽  
pp. 34 ◽  
Author(s):  
Bàrbara Micó-Vicent ◽  
Jorge Jordán ◽  
Esther Perales ◽  
Francisco Miguel Martínez-Verdú ◽  
Francisco Cases

Interest in applications of natural dye applications has increased because of their antibacterial properties and the possibility of extracting them from nature and residues. Using nanoclays as hosts to reinforce natural dye properties has been successfully demonstrated. However, no one has attempted to optimize the polymer matrix and hybrid pigment properties at the same time to ensure the best final properties for bio-composite applications. Using a statistical design for experiments, we propose the best combination of modifiers with the best nanoclay as the host of three natural dyes: chlorophyll, β-carotene, and betanine. Using the L9 Taguchi designs, we learned both the influence of the nanoclay structure, and the addition moment of surfactant, mordant salt, and silane modifiers. FTIR, XRD, DTG, integration sphere spectrophotometer, and UV-aging tests were used to characterize the hybrid pigments and epoxy bioresin composites. The degradation temperatures of the three natural dyes rose and the reinforcement of the stability of three natural dyes to UV–Vis radiation exposure was demonstrated, which avoided the migration of these dyes from bioresin to wet ribbing. Optimal results were obtained with hydrotalcite clay (calcined or not) by using surfactant and mordant before the natural dye, and before or after silane.


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