Product diversification from pomelo peel. Essential oil, Pectin and semi-dried pomelo peel

Abstract Currently, agriculture has shifted to green production, in which the recycling of post-production by-products is a key issue. In the present work, by-products such as pomelos were studied to promote consumption and enhance the value of pomelo. From pomelo material, essential oils extracted from pomelo peels, pectin, and drying pomelo products have been diversified. In the extraction process of essential oils, the hydrodistillation method was applied in conjunction with the response surface method to obtain the optimal conditions of influence factors. These essential oils were quantified as well as determined for components by GC-MS. The pectin recognition process was done by immersion method in HCl acid (pH 2) and the drying process was made with a heat pump dryer under the effects of drying temperature, drying time and wind rate. The results of the essential oil products reached the highest (0.88 ±0.006 g) at the material size of 3 mm, the distillation time of 27 min, and the ratio of raw materials/solvents of 1/12 g/mL. The main components found in pomelo peeling essential oils included limonene (71.768%), γ-terponene (12,847%), α-Phellandrene (2.979%), β-myrcene (2.668%), 1R-α-pinene (2,656%), and β-pinene (1,191%). The pectin content was the highest under the temperature of 90 °C, extraction time of 60 min and ratio/solvent ratio of 1:32 g/mL. Under these extraction conditions, 48% of concentrated pectin content was obtained. Surveying conditions for drying white pomelo peels are capable of reversing: refunded drying pomelos are drying heat pumps in the following conditions: 50 °C drying temperature, the drying time of 90 min, and wind rate of 12 m/s. Product with hardness 309.862 N.

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Novel Method for The Valorization of Essential Oils From Orange By-Product

10.21203/rs.3.rs-150909/v1 ◽

2021 ◽

Author(s):

Roudaina Abdel Samad ◽

Karim Raafat ◽

Alissar Al Khatib ◽

Hadi Abou Chacra ◽

nada EL DARRA

Keyword(s):

Essential Oil ◽

Essential Oils ◽

Biofilm Formation ◽

Bacterial Load ◽

Minimum Energy ◽

Bacterial Biofilm ◽

Diffusion Method ◽

Oil Composition ◽

By Products ◽

Orange Essential Oil

Abstract Background: A huge amount of citrus by-products are being wasted every year; these by-products can be used in the extraction of essential oils which can be used in different fields. Many methods have been used in the extraction of orange essential oil (E.O). This study focuses on the extraction of essential oil from orange by-product, using a newly developed extraction technique. This technique is a prototype combining a conventional method, namely, the hydrodistillation with the ultrasound-assisted extraction. Indeed, the traditional extraction methods of essential oils are time-consuming and expensive, moreover many organic compounds may decompose at high retained temperatures.Methods: a combination of traditional method with sonication improves efficiency and quality of the extraction, since ultrasonic extraction with precise and controlled operating parameters leads to higher extraction yields with minimum energy consumption. Therefore, the orange essential oil obtained using the prototype was compared to two commercial oils (CO1 and CO2) to create a valid comparison. Quality and safety tests have been performed, as well as bacterial load, antibacterial activities using the disc diffusion method, minimum inhibitory concentration (MIC), and prevention of bacterial biofilm formation.Results: As a result of extraction, the prototype method has shorten the extraction time, gave a higher quantity, and improved the extraction of essential oil from citrus peels without affecting oil composition when comparing it to hydrodistillation method. Conclusion: Orange E.O can be used as natural antibacterial agents to minimize bacterial growth, and inhibit biofilm formation by Staphylococcus aureus, Listeria monocytogenes and E.coli.

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Effect of drying temperature on the content and composition of hop oils

Plant Soil and Environment ◽

10.17221/482/2018-pse ◽

2018 ◽

Vol 64 (No. 10) ◽

pp. 512-516 ◽

Cited By ~ 1

Author(s):

Rybka Adolf ◽

Krofta Karel ◽

Heřmánek Petr ◽

Honzík Ivo ◽

Pokorný Jaroslav

Keyword(s):

Moisture Content ◽

Essential Oils ◽

Experimental Chamber ◽

Drying Time ◽

Drying Temperature ◽

Different Temperatures ◽

Traditional Manner

In terms of content, the paper is aimed at analysing and comparing the quality of fresh green hops and hops dried at two drying temperatures – 55°C (in the traditional manner) and 40°C (using the so-called gentle drying), regarding the maximum preservation of hop essential oils. Comparative experiments were carried out in an experimental chamber dryer with two Czech hop cultivars Saaz and Harmonie. The moisture content of hops at the beginning of drying was 75% and at the end of drying it was 9–10%. By lowering the drying temperature from 55°C to 40°C, the drying time in cv. Saaz prolonged from 8 to 10 h and for the cv. Harmonie from 9 h to 12 h. Compared to fresh hops, the amount of hop oils decreased by 10% when dried at 40°C and by 36% (cv. Saaz) and 43% (cv. Harmonie) when dried at 55°C. These losses can be considered significant, especially for hops intended for late and dry beer hopping. However, by drying the hops at different temperatures, the ratios between various components of the essential oils and thus also their sensory character remained approximately unchanged. Due to the reduced amount of essential oils, the drying effect reduces the intensity of hop aroma depending on the drying temperature.

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INFLUENCE OF HARVESTING SITES ON THE ANTIHYPERTENSIF EFFECTS OF ESSENTIAL OILS OF LIPPIA MULTIFLORA MOLDENKE (VERBENACEAE) IN BENIN

10.36106/ijsr/0435123 ◽

2021 ◽

pp. 44-47

Author(s):

Clément Dossa Gandonou ◽

Jean-Marie Kossi Denis Tokoudagba ◽

Hypolite Ganse Houehoume ◽

Louis Fagbohoun ◽

Lamine Saïd BabaMoussa ◽

...

Keyword(s):

Essential Oil ◽

Essential Oils ◽

Geographic Origin ◽

Positive Control ◽

Control Group ◽

Drying Time ◽

Lippia Multiflora ◽

Chemical Characters ◽

Drying Conditions ◽

Control Batch

A comparative study of the major compounds was carried out despite the great diversity of the constituents characteristic of the essential oil of Lippia multiflora. It was interested to note the imprint that makes each locality with the chemical characters of the gasoline. The variation in the chemical composition of essential oils, was depended on many factors such as the method used, the parts of the plant used, the products and reagents used in the extraction, the environment, the genotype of the plant, the geographic origin, harvest period of the plant, degree of drying, drying conditions, temperature and drying time and the presence of pests, viruses and weeds. The effects of essential oils of Lippia multiflora were evaluated in Wistar rats on arterial pressure (BP) and on heart rate (HR). Administration of L-NAME was caused a signicant increase in SBP in rats from 142.4 mmHg (D0) to 172.4 mmHg (D8) and from 122.8 mmHg (D0) to 138.6 mmHg (D8) respectively for the positive control batch and the batch subsequently treated with essential oil. Administration of the essential oil from D8 to D29 was caused a signicant decrease in the SBPof the rats from 140 mmHg (D8) to 122.4 mmHg (D29). This decrease was markedly lower than that of the untreated rats which is 150.5 mmHg (D29). The administration of L-NAME was caused a signicant increase in the DBPof the rats going from 93.8 mmHg (D0) to 137.5 mmHg (D8) and from 92.5 mmHg (D0) to 136.75 mmHg (D8) respectively for the positive control batch and the batch subsequently treated with essential oil.. The administration of the essential oil from D8 to D29 was caused a signicant decrease in the DBP of the rats going from 136.75 mmHg (D8) to 99.8 mmHg (D29) and nally the administration of L-NAME caused a signicant increase in the MAP of the rats going from 109.25 mmHg (D0) to 159.75 mmHg (D8) and from 99.8 mmHg (D0) to 151.25 mmHg (D8) respectively for the positive control group and the batch then treated with the raw extract). Administration of the essential oil from D8 to D29 was caused a signicant decrease in the AMP of the rats, dropping from 151.25 mmHg (D8) to 114 mmHg (D29) (p <0.05). These effects could be justify the use of this plant in traditional medicine in the treatment of high blood pressure.

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Pengaruh Waktu Ekstraksi, Rasio Bahan/Pelarut, dan Daya Microwave Terhadap Hasil Ekstraksi Minyak Serai Dapur dengan Bantuan Gelombang Mikro

Jurnal Teknik Kimia USU ◽

10.32734/jtk.v10i2.6489 ◽

2021 ◽

Vol 10 (2) ◽

pp. 51-57

Author(s):

Venitalitya A. S. Augustia ◽

Naufal Charfadz ◽

Rizki Akbar ◽

Diana

Keyword(s):

Essential Oil ◽

Essential Oils ◽

Soxhlet Extraction ◽

Geranyl Acetate ◽

Solvent Ratio ◽

Microwave Assisted ◽

Lemongrass Oil ◽

Oil Density ◽

Lemongrass Essential Oil

Lemongrass, one type of source of essential oils, is widely cultivated in Indonesia. There are several methods for extracting the essential oils from lemongrasses, such as hydro-distillation, steam distillation, soxhlet extraction, extraction with supercritical fluids, ultrasonic extraction, and microwave-assisted hydro-distillation. In this study, microwave-assisted hydro-distillation was used as the extraction method. The purpose of this study was to determine the effect of extraction time (60 minutes, 75 minutes, and 90 minutes), lemongrass/solvent ratio (1:4 g/mL and 1:5 g/mL), and microwave power (500 watt and 600 watt) on quantity and quality of lemongrass essential oil. The essential oils obtained were analyzed in the form of calculation of the essential oil density, yield, and GC-MS analysis. The results of the analysis showed that the density of the extracted lemongrass oil ranged from 0.880 g/mL – 0.920 g/mL at a temperature of 30 oC, with the highest yield ranging from 0.0044% – 0.0046% in samples with a material/solvent ratio of 1:5 g/mL. The components found in lemongrass oil were Z-citral, geranyl acetate, geraniol.

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Chemical Composition and Assessment of Antimicrobial Activity of Lavender Essential Oil and Some By-Products

Plants ◽

10.3390/plants10091829 ◽

2021 ◽

Vol 10 (9) ◽

pp. 1829

Author(s):

Alexandru Ciocarlan ◽

Lucian Lupascu ◽

Aculina Aricu ◽

Ion Dragalin ◽

Violeta Popescu ◽

...

Keyword(s):

Antimicrobial Activity ◽

Chemical Composition ◽

Essential Oil ◽

Essential Oils ◽

Xanthomonas Campestris ◽

Mass Spectrometry Analysis ◽

Gas Chromatography Mass Spectrometry ◽

Residual Water ◽

By Products

The producers of essential oils from the Republic of Moldova care about the quality of their products and at the same time, try to capitalize on the waste from processing. The purpose of the present study was to analyze the chemical composition of lavender (Lavanda angustifolia L.) essential oil and some by-products derived from its production (residual water, residual herbs), as well as to assess their “in vitro” antimicrobial activity. The gas chromatography-mass spectrometry analysis of essential oils produced by seven industrial manufacturers led to the identification of 41 constituents that meant 96.80–99.79% of the total. The main constituents are monoterpenes (84.08–92.55%), followed by sesquiterpenes (3.30–13.45%), and some aliphatic compounds (1.42–3.90%). The high-performance liquid chromatography analysis allowed the quantification of known triterpenes, ursolic, and oleanolic acids, in freshly dried lavender plants and in the residual by-products after hydrodistillation of the essential oil. The lavender essential oil showed good antibacterial activity against Bacillus subtilis, Pseudomonas fluorescens, Xanthomonas campestris, Erwinia carotovora at 300 μg/mL concentration, and Erwinia amylovora, Candida utilis at 150 μg/mL concentration, respectively. Lavender plant material but also the residual water and ethanolic extracts from the solid waste residue showed high antimicrobial activity against Aspergillus niger, Alternaria alternata, Penicillium chrysogenum, Bacillus sp., and Pseudomonas aeroginosa strains, at 0.75–6.0 μg/mL, 0.08–0.125 μg/mL, and 0.05–4.0 μg/mL, respectively.

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Content and chemical composition of the essential oil of Lippia gracilis Schauer accessions in different drying times

Bioscience Journal ◽

10.14393/bj-v35n6a2019-39748 ◽

2019 ◽

Vol 35 (6) ◽

Author(s):

Juliana Oliveira de Melo ◽

Arie Fitzgerald Blank ◽

Alisson Marcel Souza de Oliveira ◽

Thiago Matos Andrade ◽

Maria de Fátima Arrigoni-Blank ◽

...

Keyword(s):

Chemical Composition ◽

Chemical Analysis ◽

Essential Oil ◽

Essential Oils ◽

Drying Process ◽

Drying Time ◽

Mean Values ◽

Randomized Design ◽

Chemical Profiles ◽

Completely Randomized Design

Lippia gracilis, popularly known in Brazil as ‘alecrim-de-tabuleiro’, is used for many purposes, especially as antimicrobial and antiseptic. The drying process of aromatic and medicinal plants aims to minimize the loss of active principles and slow their deterioration, which may greatly influence the yield and chemical composition of some species. The objective of this study was to evaluate the effect of drying times (0, 2, 4, and 8 days) on the content and chemical composition of the essential oil of L. gracilis accessions LGRA-106, LGRA-109, and LGRA-201. The leaves were dried at 40 oC, and essential oil was extracted by hydrodistillation. Chemical analysis was performed by GC/MS. The experiment was carried out in a completely randomized design with three replications. The accessions of L. gracilis LGRA-106, LGRA-109, and LGRA-201 presented higher essential oil at four days of drying time. The accession LGRA-201 showed the highest essential oil yields at four and eight days of drying, with mean values of 0.038 and 0.029 mL g-1, respectively. The drying time did not influence the contents of thymol, methyl-thymol, γ-terpinene, and carvacrol in the essential oils of L. gracilis, but affected the contents of β-caryophyllene, p-cymene, and carvacrol acetate. The essential oils of the three accessions analyzed in this study revealed different chemical profiles.

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Characterization and Chemical Composition Analysis of Tea Tree (Meleuca alternifolia) Leaf Hydrosols Growing on Lombok Island

Jurnal Penelitian Pendidikan IPA ◽

10.29303/jppipa.v8i1.1239 ◽

2022 ◽

Vol 8 (1) ◽

pp. 119-123

Author(s):

Baiq Riyankati ◽

Surya Hadi ◽

Sri Seno Handayani

Keyword(s):

Chemical Composition ◽

Essential Oil ◽

Essential Oils ◽

Composition Analysis ◽

Distilled Water ◽

Tree Leaves ◽

Tea Tree ◽

Chemical Composition Analysis ◽

By Products ◽

Lombok Island

Tea tree is an essential oil-producing plant from Australia which is also found growing in several parts of Indonesia, including the island of Lombok. So far, tea tree essential oil producers on the island of Lombok do not utilize by-products in the form of hydrosol (distilled water) produced in the process of making essential oils. In this study, the characterization and analysis of the chemical composition of the hydrosol of tea tree leaves growing on the island of Lombok was carried out. The characteristic aroma of hydrosol is similar to that of tea tree essential oil. The results of the GC-MS analysis also showed that the hydrosol of tea tree leaves also had similarities with the essential oil, composed of major compounds in the form of trans-caryophyllene (28.58%), limonene (13.98%) and terpinen-4-ol (16.27%). Other compounds detected were -pinene (4.14%), -pinene (6.50%), -myrcene (8.09%), -terpineol (10.10%) and -terpinene (5.77%).

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Drying And Extraction of Moringa Oleifera And Its Application In Wastewater Treatment

Journal of Physics Conference Series ◽

10.1088/1742-6596/2120/1/012002 ◽

2021 ◽

Vol 2120 (1) ◽

pp. 012002

Author(s):

M Ibrahim ◽

N Ismail ◽

BL Chua ◽

ASM Adnan

Keyword(s):

Wastewater Treatment ◽

Protein Content ◽

Moringa Oleifera ◽

Solvent Ratio ◽

Dye Wastewater ◽

Chi Square ◽

Drying Time ◽

Drying Temperature ◽

Jar Test ◽

Coagulant Dosage

Abstract Conventional coagulants such as aluminum sulfate and ferric sulphate have proved to be harmful to human health as it may cause neurological diseases like Alzheimer and percentile dementia. These health concerns have led to the use of natural coagulants which are environmental friendly and not harmful to human health. In this study, Moringa Oleifera seeds are selected to study the preparation of the natural coagulant and further use it in dye wastewater treatment. The two important steps used in preparing the natural coagulants are drying of the raw materials and extraction of the protein content. Moringa Oleifera seeds were oven dried at 40°C, 50°C and 60°C and the drying data was recorded. The recorded data was then fitted into five thin layer kinetic models to obtain the most suitable drying temperature and its corresponding drying time. Using Microsoft Excel Solver 2011, values of (R2), (RMSE) and chi-square (X2 ) were calculated. Based on the highest value of (R2 ) and lowest value of (RMSE), Page kinetic model was selected. Moreover, for the selected Page kinetic model, values of (R2) and (X2) were also compared for all three temperatures and the temperature with the highest (R2) value and lowest chi-square value (X2) was selected as the most optimum drying temperature. The most optimum drying temperature for drying Moringa Oleifera seeds was obtained as 50°C as the seeds dried at this temperature holds the maximum protein content concentration which enhances its coagulation properties. Furthermore, the corresponding drying time of about 6.5 hours for seeds dried at 50°C was also taken as the most optimum drying time. In the next step, Moringa Oleifera seeds which have been dried at 50°C for 6.5 hours were used for protein extraction. Solid to solvent ratios of 0.5:100, 1:100, 2:100 and 5: 100 (g of dried Moringa oleifera seeds: ml of distilled water) were used to extract the protein by using a domestic blender for 2 minutes. Using the Bradford method, the absorbance for each solid to solvent ratio solution was recorded and the protein content concentration was further calculated. The highest protein content concentration of 0.0017 ug/uL was obtained in the best solid to solvent ratio which is 5.0: 100. Therefore, this solid to solvent ratio was used in the jar test. The jar test was based on three process parameters which includes coagulant dosage, pH and initial concentration of dye wastewater. The coagulant dosage of 300 mg/L, initial concentration of dye wastewater of 50 ppm and pH of 7 were selected as the most optimum process parameters for a maximum turbidity removal of 70.4% and a maximum color removal of 44.54% in the dye wastewater treatment with Moringa Oleifera seeds.

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The influence of duration of the distillation of fresh and dried flowers on the essential oil composition of lavandin cultivated in Republic of Macedonia

Macedonian Pharmaceutical Bulletin ◽

10.33320/maced.pharm.bull.2012.58.004 ◽

2012 ◽

Vol 58 ◽

pp. 31-38 ◽

Cited By ~ 4

Author(s):

Marija Karapandzova ◽

Ivana Cvetkovikj ◽

Gjoshe Stefkov ◽

Vlatko Stoimenov ◽

Martin Crvenov ◽

...

Keyword(s):

Essential Oil ◽

Essential Oils ◽

Plant Material ◽

Essential Oil Composition ◽

International Standards ◽

Oil Composition ◽

Linalyl Acetate ◽

Drying Time ◽

Republic Of Macedonia ◽

Total Oil

The main objective of this study was to analyze the essential oil composition of cultivated lavandin (Lavandula x intermedia Emeric ex Loisel., Lamiaceae) from Republic of Macedonia and to evaluate the influence of the drying time of plant material and the distillation duration on the oil composition. Four different essential oils were obtained by hydrodistillation in a Clevenger type apparatus from freshly harvested and air dried flowers of lavandin and varying in distillation time (30 min and 2 h). Fifty-six compounds were identified by GC/ FID/MS representing 96.57% to 98.23% of the total oil. Prevailing constituents in all tested oils were linalool, borneol and terpinene-4-ol, present in amounts from 35.23 to 42.24%, 12.28 to 16.68% and 4.44 to 5.62%, respectively. The content of 1,8-cineole varied from 3.99% to 8.42% while that of camphor was between 5.96% and 7.04%. Linalyl acetate was present in amounts from 1.26% to 3.21%. Unexpectedly, the duration of distillation insignificantly influenced the essential oil composition. Few differences, mainly in the content of borneol (13.71% and 16.68% in the oil from fresh and dried flowers, respectively) were recorded in the essential oils obtained by 30 minutes distillation, while the content of the other constituents was almost unchanged. However, the isolated essential oils of lavandin did not comply with the international standards requirements for the lavandin essential oil composition.

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Hydrolates: By-products of essential oil distillation: Chemical composition, biological activity and potential uses

Advanced technologies ◽

10.5937/savteh2002054a ◽

2020 ◽

Vol 9 (2) ◽

pp. 54-70

Author(s):

Milica Aćimović ◽

Vele Tešević ◽

Katarina Smiljanić ◽

Mirjana Cvetković ◽

Jovana Stanković ◽

...

Keyword(s):

Biological Activity ◽

Essential Oil ◽

Essential Oils ◽

Food Industry ◽

Fruits And Vegetables ◽

Steam Distillation ◽

Raw Material ◽

Chemical Compositions ◽

Organoleptic Properties ◽

By Products

Hydrolates, also referred to as hydrosols, floral or distillate waters, as well as aromatic waters, are produced in the same isolation process with essential oils by steam distillation. A small amount of essential oil constituents is dissolved in hydrolates providing specific organoleptic properties and flavor, as well as biological activity which makes them useful as raw material in many industries. Their popularity is still on the rise, especially in aromatherapy. The objective in this review is to analyze the chemical compositions of hydrolates and their corresponding essential oils, as well as biological activity of hydrolates (antimicrobial, antioxidant and antiinflamatory) and potential uses, not only in food industry for flavoring, and preservation of fresh-cut fruits and vegetables, but also as functional (soft) drinks. However, hydrolates can be used in aromatherapy and cosmetics, as well as in organic agriculture and aquaculture.

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