scholarly journals Effect of Different Porosity Ratio on Mechanical Properties of Polycaprolactone and Polylactic Acid Scaffolds

2018 ◽  
Vol 1 (1) ◽  
pp. 1243-1248
Author(s):  
Adem Demir ◽  
Mustafa Keser ◽  
Fatih Çalışkan
Keyword(s):  
Mechanical Properties ◽  
Additive Manufacturing ◽  
Pore Size ◽  
Polylactic Acid ◽  
Mechanical Performance ◽  
Patient Specific ◽  
Porous Scaffolds ◽  
Medical Field ◽  
Tissue Engineering Scaffolds ◽  
Porosity Ratio

In recent years, patient-specific solutions and additive manufacturing (AM) have become increasingly important in the treatment of bone defects in studies performed on the medical field. In this direction, additive manufacturing methods use in scaffold fabrication, and many advantages of these systems come to the forefront. Porosity affects the mechanical properties, biocompatibility, and biodegradability of tissue engineering scaffolds. In this study, the effect of different porosity ratios on the mechanical properties of scaffolds for polylactic acid (PLA) and polycaprolactone (PCL) scaffolds was studied. With this fabrication method can be formed entirely 3D interconnected porous scaffolds with pore size. Three different (20%, 35%, and 50%) porosity ratios were determined for both materials, and the mechanical properties of the samples were determined by compression test. The scaffolds fabricated with larger pore size showed lower mechanical performance compared to scaffolds with smaller pore size.

scholarly journals Adapting the Pore Size of Individual, 3D-Printed CPC Scaffolds in Maxillofacial Surgery

2021 ◽  
Vol 10 (12) ◽  
pp. 2654
Author(s):  
David Muallah ◽  
Philipp Sembdner ◽  
Stefan Holtzhausen ◽  
Heike Meissner ◽  
André Hutsky ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Cell Migration ◽  
Pore Size ◽  
High Pressures ◽  
Maxillofacial Surgery ◽  
Patient Specific ◽  
Porous Scaffolds ◽  
Bone Augmentation ◽  
3D Printed

Three dimensional (3D) printing allows additive manufacturing of patient specific scaffolds with varying pore size and geometry. Such porous scaffolds, made of 3D-printable bone-like calcium phosphate cement (CPC), are suitable for bone augmentation due to their benefit for osteogenesis. Their pores allow blood-, bone- and stem cells to migrate, colonize and finally integrate into the adjacent tissue. Furthermore, the pore size affects the scaffold’s stability. Since scaffolds in maxillofacial surgery have to withstand high forces within the jaw, adequate mechanical properties are of high clinical importance. Although many studies have investigated CPC for bone augmentation, the ideal porosity for specific indications has not been defined yet. We investigated 3D printed CPC cubes with increasing pore sizes and different printing orientations regarding cell migration and mechanical properties in comparison to commercially available bone substitutes. Furthermore, by investigating clinical cases, the scaffolds’ designs were adapted to resemble the in vivo conditions as accurately as possible. Our findings suggest that the pore size of CPC scaffolds for bone augmentation in maxillofacial surgery necessarily needs to be adapted to the surgical site. Scaffolds for sites that are not exposed to high forces, such as the sinus floor, should be printed with a pore size of 750 µm to benefit from enhanced cell infiltration. In contrast, for areas exposed to high pressures, such as the lateral mandible, scaffolds should be manufactured with a pore size of 490 µm to guarantee adequate cell migration and in order to withstand the high forces during the chewing process.

scholarly journals Physical, thermal, and mechanical properties of highly porous polylactic acid/cellulose nanofibre scaffolds prepared by salt leaching technique

2021 ◽  
Vol 10 (1) ◽  
pp. 1469-1483
Author(s):  
Revati Radakisnin ◽  
Mohd Shukry Abdul Majid ◽  
Mohd Ridzuan Mohd Jamir ◽  
Mohd Faizal Mat Tahir ◽  
Cheng Ee Meng ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Polylactic Acid ◽  
Mechanical Performance ◽  
Cell Attachment ◽  
Composite Scaffold ◽  
Average Pore Size ◽  
Pennisetum Purpureum ◽  
Porous Scaffolds ◽  
Average Pore ◽  
Salt Leaching

Abstract This study aimed to prepare and characterise polylactic acid (PLA) reinforced with cellulose nanofibre (CNF) from a Pennisetum purpureum-based composite scaffold and determine its structural and mechanical properties. Porous scaffolds with CNF compositions of 5‒20 wt% in the PLA matrix were developed using solvent casting and particulate leaching of its porogen at 90 wt% of loadings. Morphology studies using field emission scanning electron microscopy revealed that the scaffolds had well-interconnected pores with an average pore size range of 67‒137 µm and porosity >76%. X-ray diffraction confirmed the interconnectivity and homogeneity of the pores and the fibrous structure of the scaffolds. The compressive strength of the fabricated scaffolds varied between 2.34 and 6.66 MPa, while their compressive modulus was between 1.95 and 6.04 MPa for various CNF contents. Furthermore, water absorption and thermal degradation studies showed that the scaffold had good hydrophilicity and improved thermal stability. These findings highlight the need to modify the pore structure and mechanical performance simultaneously for tissue engineering. Thus, this study concludes that the developed PLA scaffolds reinforced with CNF from Pennisetum purpureum are potential candidates for cell attachment and extracellular matrix generation.

scholarly journals Preparation of Long Sisal Fiber-Reinforced Polylactic Acid Biocomposites with Highly Improved Mechanical Performance

Polymers ◽  
2021 ◽  
Vol 13 (7) ◽  
pp. 1124
Author(s):  
Zhifang Liang ◽  
Hongwu Wu ◽  
Ruipu Liu ◽  
Caiquan Wu
Keyword(s):  
Mechanical Properties ◽  
Polylactic Acid ◽  
Mechanical Performance ◽  
Tensile Elongation ◽  
Sisal Fiber ◽  
Fiber Reinforced ◽  
Impact Performance ◽  
The Matrix ◽  
Blending Process ◽  
Extension Direction

Green biodegradable plastics have come into focus as an alternative to restricted plastic products. In this paper, continuous long sisal fiber (SF)/polylactic acid (PLA) premixes were prepared by an extrusion-rolling blending process, and then unidirectional continuous long sisal fiber-reinforced PLA composites (LSFCs) were prepared by compression molding to explore the effect of long fiber on the mechanical properties of sisal fiber-reinforced composites. As a comparison, random short sisal fiber-reinforced PLA composites (SSFCs) were prepared by open milling and molding. The experimental results show that continuous long sisal fiber/PLA premixes could be successfully obtained from this pre-blending process. It was found that the presence of long sisal fibers could greatly improve the tensile strength of LSFC material along the fiber extension direction and slightly increase its tensile elongation. Continuous long fibers in LSFCs could greatly participate in supporting the load applied to the composite material. However, when comparing the mechanical properties of the two composite materials, the poor compatibility between the fiber and the matrix made fiber’s reinforcement effect not well reflected in SSFCs. Similarly, the flexural performance and impact performance of LSFCs had been improved considerably versus SSFCs.

scholarly journals Additive manufacturing of PLA-based scaffolds intended for bone regeneration and strategies to improve their biological properties

e-Polymers ◽  
2020 ◽  
Vol 20 (1) ◽  
pp. 571-599
Author(s):  
Ricardo Donate ◽  
Mario Monzón ◽  
María Elena Alemán-Domínguez
Keyword(s):  
Mechanical Properties ◽  
Tissue Engineering ◽  
Additive Manufacturing ◽  
Bone Regeneration ◽  
Polylactic Acid ◽  
State Of The Art ◽  
Biological Properties ◽  
Design Stage ◽  
Bone Scaffolds ◽  
Regeneration Of Bone

AbstractPolylactic acid (PLA) is one of the most commonly used materials in the biomedical sector because of its processability, mechanical properties and biocompatibility. Among the different techniques that are feasible to process this biomaterial, additive manufacturing (AM) has gained attention recently, as it provides the possibility of tuning the design of the structures. This flexibility in the design stage allows the customization of the parts in order to optimize their use in the tissue engineering field. In the recent years, the application of PLA for the manufacture of bone scaffolds has been especially relevant, since numerous studies have proven the potential of this biomaterial for bone regeneration. This review contains a description of the specific requirements in the regeneration of bone and how the state of the art have tried to address them with different strategies to develop PLA-based scaffolds by AM techniques and with improved biofunctionality.

scholarly journals Suitability of Recycled PLA Filament Application in Fused Filament Fabrication Process

2021 ◽  
Vol 15 (4) ◽  
pp. 491-497
Author(s):  
Tomislav Breški ◽  
Lukas Hentschel ◽  
Damir Godec ◽  
Ivica Đuretek
Keyword(s):  
Mechanical Properties ◽  
Additive Manufacturing ◽  
Polylactic Acid ◽  
Design Of Experiment ◽  
Experimental Approach ◽  
Manufacturing Processes ◽  
Support Structures ◽  
Fused Filament Fabrication ◽  
Layer Height ◽  
Printing Parameters

Fused filament fabrication (FFF) is currently one of the most popular additive manufacturing processes due to its simplicity and low running and material costs. Support structures, which are necessary for overhanging surfaces during production, in most cases need to be manually removed and as such, they become waste material. In this paper, experimental approach is utilised in order to assess suitability of recycling support structures into recycled filament for FFF process. Mechanical properties of standardized specimens made from recycled polylactic acid (PLA) filament as well as influence of layer height and infill density on those properties were investigated. Optimal printing parameters for recycled PLA filaments are determined with Design of Experiment methods (DOE).

scholarly journals Characterisation of a High-Performance Al–Zn–Mg–Cu Alloy Designed for Wire Arc Additive Manufacturing

Materials ◽  
2020 ◽  
Vol 13 (7) ◽  
pp. 1610 ◽  
Author(s):  
Paulo J. Morais ◽  
Bianca Gomes ◽  
Pedro Santos ◽  
Manuel Gomes ◽  
Rudolf Gradinger ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Additive Manufacturing ◽  
High Performance ◽  
Mechanical Performance ◽  
Fluorescence Analysis ◽  
Cold Metal Transfer ◽  
Direction Parallel ◽  
X Ray ◽  
Wire Arc Additive Manufacturing

Ever-increasing demands of industrial manufacturing regarding mechanical properties require the development of novel alloys designed towards the respective manufacturing process. Here, we consider wire arc additive manufacturing. To this end, Al alloys with additions of Zn, Mg and Cu have been designed considering the requirements of good mechanical properties and limited hot cracking susceptibility. The samples were produced using the cold metal transfer pulse advanced (CMT-PADV) technique, known for its ability to produce lower porosity parts with smaller grain size. After material simulations to determine the optimal heat treatment, the samples were solution heat treated, quenched and aged to enhance their mechanical performance. Chemical analysis, mechanical properties and microstructure evolution were evaluated using optical light microscopy, scanning electron microscopy, energy dispersive X-ray spectroscopy, X-ray fluorescence analysis and X-ray radiography, as well as tensile, fatigue and hardness tests. The objective of this research was to evaluate in detail the mechanical properties and microstructure of the newly designed high-performance Al–Zn-based alloy before and after ageing heat treatment. The only defects found in the parts built under optimised conditions were small dispersed porosities, without any visible cracks or lack of fusion. Furthermore, the mechanical properties are superior to those of commercial 7xxx alloys and remarkably independent of the testing direction (parallel or perpendicular to the deposit beads). The presented analyses are very promising regarding additive manufacturing of high-strength aluminium alloys.

scholarly journals Additive Manufacturing of High-Entropy Alloys: A Review

Entropy ◽  
2018 ◽  
Vol 20 (12) ◽  
pp. 937 ◽  
Author(s):  
Shuying Chen ◽  
Yang Tong ◽  
Peter Liaw
Keyword(s):  
Mechanical Properties ◽  
Additive Manufacturing ◽  
High Efficiency ◽  
Mechanical Performance ◽  
Heating Temperature ◽  
Intermetallic Phase ◽  
Solid Solution Phase ◽  
High Entropy Alloys ◽  
Scanning Method ◽  
High Entropy

Owing to the reduced defects, low cost, and high efficiency, the additive manufacturing (AM) technique has attracted increasingly attention and has been applied in high-entropy alloys (HEAs) in recent years. It was found that AM-processed HEAs possess an optimized microstructure and improved mechanical properties. However, no report has been proposed to review the application of the AM method in preparing bulk HEAs. Hence, it is necessary to introduce AM-processed HEAs in terms of applications, microstructures, mechanical properties, and challenges to provide readers with fundamental understanding. Specifically, we reviewed (1) the application of AM methods in the fabrication of HEAs and (2) the post-heat treatment effect on the microstructural evolution and mechanical properties. Compared with the casting counterparts, AM-HEAs were found to have a superior yield strength and ductility as a consequence of the fine microstructure formed during the rapid solidification in the fabrication process. The post-treatment, such as high isostatic pressing (HIP), can further enhance their properties by removing the existing fabrication defects and residual stress in the AM-HEAs. Furthermore, the mechanical properties can be tuned by either reducing the pre-heating temperature to hinder the phase partitioning or modifying the composition of the HEA to stabilize the solid-solution phase or ductile intermetallic phase in AM materials. Moreover, the processing parameters, fabrication orientation, and scanning method can be optimized to further improve the mechanical performance of the as-built-HEAs.

scholarly journals Effect of Porosity and Crystallinity on 3D Printed PLA Properties

Polymers ◽  
2019 ◽  
Vol 11 (9) ◽  
pp. 1487 ◽  
Author(s):  
Yuhan Liao ◽  
Chang Liu ◽  
Bartolomeo Coppola ◽  
Giuseppina Barra ◽  
Luciano Di Maio ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Additive Manufacturing ◽  
3D Printing ◽  
Polylactic Acid ◽  
Complex Geometry ◽  
Fused Filament Fabrication ◽  
3D Printed ◽  
Physical Changes ◽  
Crystalline Forms

Additive manufacturing (AM) is a promising technology for the rapid tooling and fabrication of complex geometry components. Among all AM techniques, fused filament fabrication (FFF) is the most widely used technique for polymers. However, the consistency and properties control of the FFF product remains a challenging issue. This study aims to investigate physical changes during the 3D printing of polylactic acid (PLA). The correlations between the porosity, crystallinity and mechanical properties of the printed parts were studied. Moreover, the effects of the build-platform temperature were investigated. The experimental results confirmed the anisotropy of printed objects due to the occurrence of orientation phenomena during the filament deposition and the formation both of ordered and disordered crystalline forms (α and δ, respectively). A heat treatment post-3D printing was proposed as an effective method to improve mechanical properties by optimizing the crystallinity (transforming the δ form into the α one) and overcoming the anisotropy of the 3D printed object.

scholarly journals Next Generation Orthopaedic Implants by Additive Manufacturing Using Electron Beam Melting

2012 ◽  
Vol 2012 ◽  
pp. 1-14 ◽  
Author(s):  
Lawrence E. Murr ◽  
Sara M. Gaytan ◽  
Edwin Martinez ◽  
Frank Medina ◽  
Ryan B. Wicker
Keyword(s):  
Mechanical Properties ◽  
Electron Beam ◽  
Additive Manufacturing ◽  
Electron Beam Melting ◽  
Stress Shielding ◽  
Bone Cell ◽  
Cellular Structures ◽  
Patient Specific ◽  
Porous Structures ◽  
Orthopaedic Implants

This paper presents some examples of knee and hip implant components containing porous structures and fabricated in monolithic forms utilizing electron beam melting (EBM). In addition, utilizing stiffness or relative stiffness versus relative density design plots for open-cellular structures (mesh and foam components) of Ti-6Al-4V and Co-29Cr-6Mo alloy fabricated by EBM, it is demonstrated that stiffness-compatible implants can be fabricated for optimal stress shielding for bone regimes as well as bone cell ingrowth. Implications for the fabrication of patient-specific, monolithic, multifunctional orthopaedic implants using EBM are described along with microstructures and mechanical properties characteristic of both Ti-6Al-4V and Co-29Cr-6Mo alloy prototypes, including both solid and open-cellular prototypes manufactured by additive manufacturing (AM) using EBM.

Laser Additive Manufacturing of Novel Aluminum Based Nanocomposite Parts: Tailored Forming of Multiple Materials

2015 ◽  
Vol 138 (2) ◽  
Author(s):  
Dongdong Gu ◽  
Hongqiao Wang ◽  
Donghua Dai
Keyword(s):  
Mechanical Properties ◽  
Additive Manufacturing ◽  
Microstructural Evolution ◽  
Mechanical Performance ◽  
Laser Energy ◽  
Dimensional Accuracy ◽  
Ring Structure ◽  
Multiple Materials ◽  
Depth Relationship ◽  
Tailored Forming

The present study has proved the feasibility to produce the bulk-form TiC/AlSi10Mg nanocomposite parts with the novel reinforcing morphology and enhanced mechanical properties by selective laser melting (SLM) additive manufacturing (AM) process. The influence of linear laser energy density (η) on the microstructural evolution and mechanical performance (e.g., densification level, microhardness, wear and tribological properties) of the SLM-processed TiC/AlSi10Mg nanocomposite parts was comprehensively studied, in order to establish an in-depth relationship between SLM process, microstructures, and mechanical performance. It showed that the TiC reinforcement in the SLM-processed TiC/AlSi10Mg nanocomposites experienced an interesting microstructural evolution with the increase of the applied η. At an elevated η above 600 J/m, a novel regularly distributed ring structure of nanoscale TiC reinforcement was tailored in the matrix due to the unique metallurgical behavior of the molten pool induced by the operation of Marangoni flow. The near fully dense TiC/AlSi10Mg nanocomposite parts (>98.5% theoretical density (TD)) with the formation of ring-structured reinforcement demonstrated outstanding mechanical properties. The dimensional accuracy of SLM-processed parts well met the demand of industrial application with the shrinkage rates of 1.24%, 1.50%, and 1.72% in X, Y, and Z directions, respectively, with the increase of η to 800 J/m. A maximum microhardness of 184.7 HV0.1 was obtained for SLM-processed TiC/AlSi10Mg nanocomposites, showing more than 20% enhancement as compared with SLM-processed unreinforced AlSi10Mg part. The high densification response combined with novel reinforcement of SLM-processed TiC/AlSi10Mg nanocomposite parts also led to the considerably low coefficient of friction (COF) of 0.28 and wear rate of 2.73 × 10−5 mm3 · N−1 · m−1. The present work accordingly provides a fundamental understanding of the tailored forming of lightweight multiple nanocomposite materials system by laser AM.

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