Preparation of Iron Oxide Red from Red Mud

2013 ◽  
Vol 826 ◽  
pp. 92-96
Author(s):  
Zheng Xian Ma ◽  
Qiao Ling Liu ◽  
Lan Qin Wang ◽  
Lu Feng Pang
Keyword(s):  
Particle Size ◽  
Iron Oxide ◽  
Hydrochloric Acid ◽  
Chemical Analysis ◽  
Quality Indicators ◽  
Red Mud ◽  
Chemical Precipitation ◽  
Bayer Process ◽  
Optimal Experimental Condition ◽  
Particle Size Analyzer

With using the red mud of Bayer process and industrial hydrochloric acid as main initial materials, iron oxide red was prepared by chemical precipitation technique. The character of the sample were characterized and analyzed by means of XRD, SEM, particle size analyzer, and chemical analysis methods, respectively. The optimal experimental condition of extraction of iron from red mud was obtained, and the key quality indicators of sample was conformed the requirements of iron oxide red by a variety of test and characterization.

Synthesis of Calcium Metaphosphates Fine Powders by Chemical Precipitation Methods

2010 ◽  
Vol 105-106 ◽  
pp. 532-535 ◽  
Author(s):  
Yin Zhang ◽  
De Shuang Kong ◽  
Ya Qiu Tao ◽  
Jian Ping Zhu ◽  
Neng Jian Yao
Keyword(s):  
Particle Size ◽  
Chemical Precipitation ◽  
Precipitation Method ◽  
Fine Powders ◽  
Heat Treated ◽  
Particle Size Analyzer ◽  
Powder Characteristics ◽  
Ft Ir ◽  
Phosphorus Precursor ◽  
Hydrolysis Of

Calcium metaphosphate (CMP) fine powders were produced by a chemical precipitation method. In order to produce the powders, CMP was prepared by the mixing of two precursors, such as calcium oxide (CaO) and phosphate acid (H3PO4). Sparingly soluble chemicals, the Ca/P ratio of the mixture was set to be 0.50 to produce stoichiometric CMP, were chemical agitated in phosphate acid solution. At least 3 hours of pre-hydrolysis of phosphorus precursor were required to obtain CMP phase. The CMP powders were dried in a drying oven at 60°C for 72 hours and then heat-treated at various temperatures at a ramp of 1°C /min in air for various hours. The obtained powder was analyzed using XRD, XRF, FT-IR, SEM, TG-DTA, Zeta Potential Meter, Specific Surface Area, and Particle Size Analyzer. The results showed that obtained CMP powders have a significantly powder characteristics.

Preparing and Application of Polymerized Aluminum-Ferrum Chloride

2011 ◽  
Vol 183-185 ◽  
pp. 1956-1960
Author(s):  
Gui Lin Lu ◽  
Hai Yan Yu ◽  
Shi Wen Bi
Keyword(s):  
Iron Oxide ◽  
Reaction Time ◽  
Hydrochloric Acid ◽  
Ferric Chloride ◽  
Reaction Temperature ◽  
Red Mud ◽  
Raw Material ◽  
New Method ◽  
Reaction Processes ◽  
The Way

Put forward a new method to prepare polyaluminium ferric chloride (PAFC). Discuss the effect of starting materials, reaction processes on the leaching ratios of alumina and iron oxide. Application properties were tested. The results showed that both diasporic bauxite and the red mud from gibbsite (RMG) do not need to be baked. In the case of diasporic bauxite, the leaching ratios of alumina and iron oxide reach 4.15% and 78.32% respectively under the conditions that the concentration of hydrochloric acid is 6mol/L, the reaction time is 60 minutes, the reaction temperature is about 109°C, and the way of extracting is two-step extracting. In the case of RMG, the leaching ratios of alumina and iron oxide reach 89.00% and 98.39% respectively under the same conditions. Diasporic bauxite is not a suitable raw material for PAFC synthesizing. The PAFC prepared from RMG was used to treat active black KN-B dye-containing wastewater and the Kaolin-containing wastewater. The maximum depollution ratio is 98.0% and 97.0 % respectively.

Research of Leaching Alumina and Iron Oxide from Bayer Red Mud

2012 ◽  
Vol 151 ◽  
pp. 355-359 ◽  
Author(s):  
Rong Rong Lu ◽  
Yi He Zhang ◽  
Feng Shan Zhou ◽  
Xin Ke Wang
Keyword(s):  
Sulfuric Acid ◽  
Iron Oxide ◽  
Hydrochloric Acid ◽  
Red Mud ◽  
Acid Leaching ◽  
Raw Material ◽  
Good Effect ◽  
Mixed Acid ◽  
Leaching Experiments ◽  
Bayer Red Mud

Adopting Bayer red mud as raw material, researching five acid leaching of alumina and iron oxide methods, hydrochloric acid leaching, sulfuric acid leaching, mixed acid leaching and two methods of classification acid leaching, affecting on leaching ratio of Al and Fe in red mud. All the five acid leaching experiments have a good effect on the leaching ratios of alumina and iron oxide. The highest leaching ratios of alumina and iron oxide are 90.1% and 99.0% when the volume of hydrochloric acid and sulfuric acid are 25mL in the mixed acid leaching. Finally, obtain better condition of preparing flocculants solution for water treatment by leaching Fe and Al in red mud.

SINTESIS DAN KARAKTERISASI NANOPARTIKEL KITOSAN – EKSTRAK KULIT BUAH MANGGIS (Garcinia Mangostana)

2013 ◽  
Vol 14 (3) ◽  
Author(s):  
Eriawan Rismana ◽  
Susi Kusumaningrum ◽  
Olivia Bunga P ◽  
Idah Rosidah ◽  
Marhamah Marhamah
Keyword(s):  
Particle Size ◽  
Sodium Tripolyphosphate ◽  
Chitosan Solution ◽  
The Other ◽  
Ionic Gelation ◽  
Garcinia Mangostana ◽  
Particle Size Analyzer ◽  
Cadmium Lead ◽  
Solvent Residue ◽  
Mold And Yeast

The chitosan – Garcinia Mangostana extract nanoparticles has been prepared by ionic gelation reaction by mixture 0.2 % chitosan solution in acetic acid with Garcinia Mangostana extract and it’s continued by reaction process with 0.1 % sodium tripolyphosphate. The particle size of material was determined by Particle Size Analyzer (PSA) that it showed in the range of 200 – 500 nm. The color, pH, water, α- mangostin, mercury, arsenic, cadmium, lead, totally microbe aerobic, totally mold and yeast, and solvent residue contents of nanoparticles were also examined by many methods that these resulted are yellow, 4.50 – 5.50, 89 – 90 %, 1.05 %, < 0.005 ppm, < 0.01 ppm, < 0.01 ppm, < 0.05 ppm, < 10 CFU/g, < 10 CFU/g and not detected, respectively. The other characterization was also observed that it’sincluded stability andTLC chromatogram. A mixture of nanoparticles with cosmetics bases was showed that it’s increased stability, homogeneity and easy to formed.

Isolasi Dan Karakterisasi Bentonit Alam Menjadi Nanopartikel Monmorillonit

2018 ◽  
Vol 3 (1) ◽  
pp. 12 ◽  
Author(s):  
Zaimahwati Zaimahwati ◽  
Yuniati Yuniati ◽  
Ramzi Jalal ◽  
Syahman Zhafiri ◽  
Yuli Yetri
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Particle Size ◽  
Surface Morphology ◽  
Average Diameter ◽  
Particle Size Analyzer ◽  
Ft Ir ◽  
Scanning Electron ◽  
Sedimentation Processes

<p>Pada penelitian ini telah dilakukan isolasi dan karakterisasi bentonit alam menjadi nanopartikel montmorillonit. Bentonit alam yang digunakan diambil dari desa Blangdalam, Kecamatan Nisam Kabupaten Aceh Utara.  Proses isolasi meliputi proses pelarutan dengan aquades, ultrasonic dan proses sedimentasi. Untuk mengetahui karakterisasi montmorillonit dilakukan uji FT-IR, X-RD dan uji morfologi permukaan dengan Scanning Electron Microscopy (SEM). Partikel size analyzer untuk menganalisis dan menentukan ukuran nanopartikel dari isolasi bentonit alam. Dari hasil penelitian didapat ukuran nanopartikel montmorillonit hasil isolasi dari bentonit alam diperoleh berdiameter rata-rata 82,15 nm.</p><p><em>In this research we have isolated and characterized natural bentonite into montmorillonite nanoparticles. Natural bentonite used was taken from Blangdalam village, Nisam sub-district, North Aceh district. The isolation process includes dissolving process with aquades, ultrasonic and sedimentation processes.  The characterization of montmorillonite, FT-IR, X-RD and surface morphology test by Scanning Electron Microscopy (SEM). Particle size analyzer to analyze and determine the size of nanoparticles from natural bentonite insulation. From the research results obtained the size of montmorillonite nanoparticles isolated from natural bentonite obtained an average diameter of 82.15 nm.</em></p>

scholarly journals Impact of Iron on the Fe–Co–Ni Ternary Nanocomposites Structural and Magnetic Features Obtained via Chemical Precipitation Followed by Reduction Process for Various Magnetically Coupled Devices Applications

Nanomaterials ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 341
Author(s):  
Tien Hiep Nguyen ◽  
Gopalu Karunakaran ◽  
Yu.V. Konyukhov ◽  
Nguyen Van Minh ◽  
D.Yu. Karpenkov ◽  
...  
Keyword(s):  
Particle Size ◽  
Magnetic Properties ◽  
Reduction Process ◽  
Chemical Precipitation ◽  
Precipitation Method ◽  
Magnetic Characteristics ◽  
Reduction Temperature ◽  
Fe Content ◽  
Magnetic Features ◽  
Co Precipitation

This paper presents the synthesis of Fe–Co–Ni nanocomposites by chemical precipitation, followed by a reduction process. It was found that the influence of the chemical composition and reduction temperature greatly alters the phase formation, its structures, particle size distribution, and magnetic properties of Fe–Co–Ni nanocomposites. The initial hydroxides of Fe–Co–Ni combinations were prepared by the co-precipitation method from nitrate precursors and precipitated using alkali. The reduction process was carried out by hydrogen in the temperature range of 300–500 °C under isothermal conditions. The nanocomposites had metallic and intermetallic phases with different lattice parameter values due to the increase in Fe content. In this paper, we showed that the values of the magnetic parameters of nanocomposites can be controlled in the ranges of MS = 7.6–192.5 Am2/kg, Mr = 0.4–39.7 Am2/kg, Mr/Ms = 0.02–0.32, and HcM = 4.72–60.68 kA/m by regulating the composition and reduction temperature of the Fe–Co–Ni composites. Due to the reduction process, drastic variations in the magnetic features result from the intermetallic and metallic face formation. The variation in magnetic characteristics is guided by the reduction degree, particle size growth, and crystallinity enhancement. Moreover, the reduction of the surface spins fraction of the nanocomposites under their growth induced an increase in the saturation magnetization. This is the first report where the influence of Fe content on the Fe–Co–Ni ternary system phase content and magnetic properties was evaluated. The Fe–Co–Ni ternary nanocomposites obtained by co-precipitation, followed by the hydrogen reduction led to the formation of better magnetic materials for various magnetically coupled device applications.

scholarly journals The Processing of Beach Sand from Sri Lanka for the Recovery of Titanium Using Magnetic Separation

2003 ◽  
Vol 12 (1) ◽  
pp. 13-22 ◽  
Author(s):  
W. A. P. J. Premaratne ◽  
N. A. Rowson
Keyword(s):  
Particle Size ◽  
Sri Lanka ◽  
Chemical Analysis ◽  
Titanium Content ◽  
Beach Sand ◽  
Magnetic Fraction ◽  
Chemical Characteristics ◽  
Magnetic Separator ◽  
Commercial Grade ◽  
Sand Deposit

An investigation has been carried out to study the mineralogical and chemical characteristics of beach sand deposits from Sri Lanka and application and optimisation of different magnetic separators (induced roll magnetic separator and disc magnetic separator) to improve the recovery of titanium from the deposit. Commercial grade titanium concentrates could be achieved employing both induced roll and disc magnetic separators. However, the titanium recovery increased greatly in the magnetic fraction with a titanium content of commercial grade (up to 63.9% TiO2) when paramagnetic titanium-bearing minerals were separated from beach sand using the disc magnetic separator. The results of the mineralogical and chemical analysis tests for the beach sand deposit indicated that 71% of beach sand was smaller than 355 μm in particle size and more than 99% of titanium content of the deposit was contained in this fraction.

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