Effect of Homogenization Annealing on Wear Properties of Thixo-Extrued Copper Alloy

2022 ◽  
Vol 327 ◽  
pp. 71-81
Author(s):  
Yun Xin Cui ◽  
Han Xiao ◽  
Chi Xiong ◽  
Rong Feng Zhou ◽  
Zu Lai Li ◽  
...  

The semi-solid extruded CuSn10P1 alloy bushings were homogenization annealed. The effects of annealing process on the hardness and wear properties of bushings were researched. The results show the Brinell hardness increases firstly and then decreases with the increase of annealing temperature and annealing time. With the annealing temperature increasing, the grinding loss rate and friction factor decrease firstly and then increase. At the annealing time of 120 min, the grinding loss rate decreases from 7% at the annealing temperature of 450 °C to 6% at 500 °C, and then increases from 6% at 500 °C to 12% at 600 °C. The friction factor decreases from 0.54 to 0.48 and then increases to 0.83. At the annealing temperature of 500 °C, the grinding loss rate decreases from 11% at the annealing time of 60 min to 6% at 120 min, and then increases to 15% at 150 min. The friction factor decreases from 0.67 to 0.48 and then increases to 0.72. The best wear performance and Brinell hardness can be obtained at annealing temperature of 500 °C for 120 min.

2011 ◽  
Vol 704-705 ◽  
pp. 581-585
Author(s):  
Ying Zhang ◽  
Jin Hua Xu ◽  
Shui Sheng Xie ◽  
Mao Peng Geng ◽  
Hong Min Guo ◽  
...  

The experiment of the roll-casting for semi-solid AZ91D magnesium was carried out on the equipment made by ourselves in our laboratory. Parameters of annealing process and the effect of annealing temperature on structure and hardness of semi-solid magnesium were investigated. It was shown that annealing process can improve the structure and properties of roll-casting strips for semi-solid magnesium. In addition, it can relieve the eutectic structure segregation and make β-Mg17Al12 phase precipitate from primary α-Mg grain, which can cause dispersion strengthening process when the annealing temperature is about 420°C. With the increasing of annealing temperature, semi-solid primary α-Mg grain boundary become obscure gradually, grain growth is indistinct and β-Mg17Al12 phase is precipitated from the inner α-Mg grain. However, the aberrated eutectic α-Mg grain for non-equilibrium solidification increase continuously and separate gradually from β-Mg17Al12 phase, which makes the β-Mg17Al12 phase connect together and distribute on the α-Mg grain boundary closely approaching the equilibrium solidification structure. Hardness in eutectic structure area is higher than primary α-Mg grain. With the increasing of annealing temperature, hardness in eutectic structure area will increase and then decrease, when the temperature is over 400°C, the hardness will increase again, but hardness of primary α-Mg grain nearly unchanged. Keywords: casting-rolling; anneal; semi-solid; magnesium alloy; microstructure


2015 ◽  
Vol 1095 ◽  
pp. 647-650
Author(s):  
Ting Chen ◽  
Jia Nan Zhang

Polystyrene-b-Polylactide (PS-b-PLA) was dissolved in chlorobenzene, and the development of the micro-phase separation morphology in asymmetric PS-b-PLA thin films was investigated by AFM. The thin films were prepared by spinning casting at the speed of 6000 r/min for 60s on Si substrates. We get different morphologies of PS-b-PLA thin film by changing the annealing temperature from 150 °C to 170 °C. In addition, the annealing time influences the morphology of the film. When the annealing time increased from 2 hours to 15 hours and 30 hours, the morphology transformed from parallel to perpendicular to the substrate. By applying temperature gradients, we can control the morphology and orientation of the Block copolymer film self-assembly.


2013 ◽  
Vol 743-744 ◽  
pp. 414-419
Author(s):  
Si Deng Zhang ◽  
Xu Zhen Zhang ◽  
Bin Sun ◽  
Long Chen ◽  
Zhi Yan Ma ◽  
...  

Polypropylene pre-oriented multifilament were made by melt spinning with fast winding, and then hard elastic polypropylene fibers were made followed by annealing treatment under some conditions. The effects of the conditions of melt spinning and annealing process on the elasticity of polypropylene fibers were studied. The structure and property of hard elastic polypropylene fibers were analyzed by DSC,WAXD,SAXS and Sound velocity anisotropy. The results showed that the hard elasticity of annealed fibers increased with the improving of speed of winding, and the elasticity also increased with the improving of annealing temperature and extension of annealing time, and the elastic recovery rate of PP multifilament can be as high as 93.6%. The crystal phase of unannealed and annealed PP fibers did not change. Annealing leaded to form perfectly the characteristic crystalline structure of crystals of being perpendicular to fiber axis.


2008 ◽  
Vol 600-603 ◽  
pp. 585-590
Author(s):  
Ryo Hattori ◽  
Tomokatsu Watanabe ◽  
T. Mitani ◽  
Hiroaki Sumitani ◽  
Tatsuo Oomori

Crystalline recovery mechanism in the activation annealing process of Al implanted 4H-SiC crystals were experimentally investigated. Annealing temperature and annealing time dependence of acceptor activation and activated hole’s behavior were examined. Poly-type recovery from the implantation induced lattice disordering during the annealing was investigated. The existence of meta-stable crystalline states for acceptor activation, and related scattering centers due to annealing is reported To achieve 100% acceptor activation and to reduce strain after ion implantation, annealing at 2000°C for 10 min. was required.


2011 ◽  
Vol 110-116 ◽  
pp. 1094-1098
Author(s):  
Haleh Kangarlou ◽  
Mehdi Bahrami Gharahasanloo ◽  
Akbar Abdi Saray ◽  
Reza Mohammadi Gharabagh

Ti films of same thickness, and near normal deposition angle, and same deposition rate were deposited on glass substrates, at room temperature, under UHV conditions. Different annealing temperatures as 393K, 493K and 593K with uniform 8 cm3/sec, oxygen flow, were used for producing titanium oxide layers. Their nanostructures were determined by AFM and XRD methods. Roughness of the films changed due to annealing process. The gettering property of Ti and annealing temperature can play an important role in the nanostructure of the films.


1981 ◽  
Vol 7 ◽  
Author(s):  
B.S. Elman ◽  
H. Mazurek ◽  
M.S. Dresselhaus ◽  
G. Dresselhaus

ABSTRACTRaman spectroscopy is used in a variety of ways to monitor different aspects of the lattice damage caused by ion implantation into graphite. Particular attention is given to the use of Raman spectroscopy to monitor the restoration of lattice order by the annealing process, which depends critically on the annealing temperature and on the extent of the original lattice damage. At low fluences the highly disordered region is localized in the implanted region and relatively low annealing temperatures are required, compared with the implantation at high fluences where the highly disordered region extends all the way to the surface. At high fluences, annealing temperatures comparable to those required for the graphitization of carbons are necessary to fully restore lattice order.


2018 ◽  
Vol 924 ◽  
pp. 333-338 ◽  
Author(s):  
Roberta Nipoti ◽  
Alberto Carnera ◽  
Giovanni Alfieri ◽  
Lukas Kranz

The electrical activation of 1×1020cm-3implanted Al in 4H-SiC has been studied in the temperature range 1500 - 1950 °C by the analysis of the sheet resistance of the Al implanted layers, as measured at room temperature. The minimum annealing time for reaching stationary electrical at fixed annealing temperature has been found. The samples with stationary electrical activation have been used to estimate the thermal activation energy for the electrical activation of the implanted Al.


2018 ◽  
Vol 186 ◽  
pp. 02001
Author(s):  
Teng-wei Zhu ◽  
Cheng-liang Miao ◽  
Zheng Cheng ◽  
Zhipeng Wang ◽  
Yang Cui ◽  
...  

The influence of the mechanical properties of X70 pipeline steel under different annealing temperature was studied. The corresponding microstructure was investigated by the Field Emission Scanning Electron Microscopy. The results showed that the yield strength and the tensile strength both experienced from rise to decline with the increase of annealing temperature. The grain sizes were coarse and a large amount of cementite precipitated due to preserving temperature above 550 °, which induced matrix fragmentation and deteriorate the -10 ° DWTT Toughness. There were little changes on the microstructure and mechanical properties when the annealing temperature was under 500 °.


2018 ◽  
Vol 141 (3) ◽  
Author(s):  
Mahsa Ebrahimi ◽  
Abbas Zarei-Hanzaki ◽  
A. H. Shafieizad ◽  
Michaela Šlapáková ◽  
Parya Teymoory

The present work was primarily conducted to study the wear behavior of as-received and severely deformed Al-15%Mg2Si in situ composites. The severe plastic deformation was applied using accumulative back extrusion (ABE) technique (one and three passes). The continuous dynamic recrystallization (CDRX) was recognized as the main strain accommodation and grain refinement mechanism within aluminum matrix during ABE cycles. To investigate the wear properties of the processed material, the dry sliding wear tests were carried out on both the as-received and processed samples under normal load of 10 and 20 N at room temperature, 100 °C, and 200 °C. The results indicated a better wear resistance of processed specimens in comparison to the as-received ones at room temperature. In addition, the wear performance was improved as the ABE pass numbers increased. These were related to the presence of oxide tribolayer. At 100 °C, the as-received material exhibited a better wear performance compared to the processed material; this was attributed to the formation of a work-hardened layer on the worn surface. At 200 °C, both the as-received and processed composites experienced a severe wear condition. In general, elevating the temperature changed the dominant wear mechanism from oxidation and delamination at room temperature to severe adhesion and plastic deformation at 200 °C.


1969 ◽  
Vol 184 (1) ◽  
pp. 875-884 ◽  
Author(s):  
P. F. Thomason

Longitudinal grooves of various depths ranging from 0.001 in to 0.011 in were machined on the cylindrical surface of steel slugs prior to carrying out an automatic two-stage transfer heading operation. The longitudinal grooves were used to estimate the ‘critical groove depth’, which was defined as the depth of longitudinal groove that contained a ductile fracture crack just on the point of ‘opening out’ at the end of the heading process, thus giving a measure of the ductility of the wire. A half-replicate of a two-level factorial experiment was carried out to assess the effects and interactions of annealing temperature, annealing time, cooling rate and ageing temperature on the ductility of four different types of 1/2 in diameter cold heading steel wire. The results show that certain types of steel wires have optimum ductility in the ‘as-received’, cold-drawn, state. Other types of steel are shown to respond favourably to process annealing treatments, in which case annealing at 700°C for 1 hour followed by air cooling should give optimum ductility. It is shown that there is no general correlation between decreasing hardness and increasing ductility for steel wire.


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