Pengaruh Ukuran Partikel, Perbandingan Jumlah Pelarut dan Waktu Maserasi terhadap Perolehan Rendemen Aquilaria Malaccensis Lam.

Aquilaria Malaccensis Lam. is one of the most popular plants contains essential oil, both of them used by pharmaceutical and also cosmetic industry. The plants used in this study came from Jambi, Indonesia which is known, It’s one of the best quality agarwood in the world. This study aims to determine the best conditions for the yield so that it can be produced on an industrial scale. The study reviewed the effect of yield based on size of particles, ratio of solvent, and the operating time, maceration. The research was carried out in three steps. The first, raw material preparation, fermentation and maceration, and then evaporation. Preparation of raw materials is prepared in three variables, 2-5 cm, ±2cm, and size <40 mesh. Methanol is the solvent that will be used in multiple ratio of solvent to agarwood, its 1:7, 1:9, and 1:11(gr/ml). In addition, the maceration time was varied for each sample, 1 day, 2 days, and 3 days. Based on the research variables, obtained essential oil of agarwood dark brown in colour, with a special fragrance of agarwood. Based on the difference in particle size, it is known that size <40 mesh, yield is 3.16%, while for the larger size, 2-5 cm, the yield is 3.12%. In the variable ratio of the amount of solvent used, it is known that 1:9 (gr/ml) is the best point for yield. At maceration step known that 2-3 days, it doesn’t gives a significant change, 2.12 g for 3 days, and 1.92 g for 2 days.

Potensi Ekstrak Daun Pepaya sebagai Inhibitor Korosi dalam Media Asam Klorida pada Baja ST37

Corrosion is a decrease in the quality of a metal material caused by a reaction with the environment. Reducing the corrosion rate on steel can be done by adding an inhibitor. Papaya leaf extract (Carica papaya.L) can be used as a corrosion inhibitor by immersion method. The effect of inhibitor on corrosion rate had been studied using weight loss method, potentiodynamic polarization method, and observation of steel surface using photooptic. It was found that corrosion rate decrease with increase concentration of papaya leaves extract. The highest inhibiton efficiency is 87.8% in 0.2 M hydrochloric acid with 2% concentration of papaya leaves extract. Potentiodynamic polarization method showed that papaya leaves extract decrease corrotion current. Inhibiton efficiency reached 81.58% in 2% extract concentration in which corrosion current decrease from 0.0266 mA/cm2 to 0.0049 mA/cm2. Analysis of photooptic showed that there is difference on steel surface corroded in hydrochloric acid with inhibitor and without it.

Ekstraksi Minyak Gaharu dengan Pelarut Etanol secara Maserasi

Agarwood is one of the forest products that can be utilized and has a high selling value. Agarwood contains essential oils which have many active compounds and contains a specific aromatic resin that is naturally formed as a form of defense against physical damage or microbial infection. Agarwood essential oil with good quality has a high economic value. This study aims to extract agarwood essential oil using ethanol as a solvent. The optimal yield of agarwood essential oil can be obtained by varying the particle size, the ratio of the weight of the agarwood biomass (kg) to the volume of the solvent (L), and the length of maceration (h). The results showed that the particle size of agarwood did notaffect the yield of agarwood essential oil. The results of the comparison of agarwood biomass with the volume of the solvent showed that the ratio of 1:9 (w/v) obtained the highest yield of 4.02% and the longest maceration time with the highest yield of 4.12% for 72 hours. However, 48 hours of maceration had a greater increase in yield compared to 72 hours of maceration. The increase in yield at 48 hours to 72 hours of maceration was only 0.22% when compared to the increase in yield at 24 hours to 48 hours of maceration, which was 0.56%.

Efek Variasi Penambahan Carbomer Terhadap Nilai pH, Viskositas dan Aktivitas Mikroba pada Sediaan Hand Sanitizer

Hand sanitizer is an antiseptic in gel form. The gel texture in hand sanitizers is caused by the carbomer which acts as a gelling agent. Therefore, this research was done to observe the effect of carbomer on the value of pH, viscosity, and microbial activity in hand sanitizers. As for testing pH using pH meters, testing viscosity was carried out using the viscometer method, while microbial activity was carried out using the Total Plate Number, Yeast Mold Number and microbial pathogen tests. Based on the data obtained, the carbomer greatly influences the increase in the viscosity of the hand sanitizer gel, the pH value was obtained at 6.0 - 7.06, while in the microbial activity test none of the microbes grew in each medium. Therefore, it can be concluded that the hand sanitizer with code P3 is the best sample

Kajian Mutu Kimia Bubuk Kopi Espresso Aceh Berdasarkan Rasio Pencampuran Varietas Kopi Arabika dan Robusta dan Teknik Penyangraian

Generally there are two coffee varietes cultivated in Indonesia, known as Arabica and Robusta coffee. Arabica distinctively known for its distinctive quality but limited quantity compared to robusta which is commonly use for commercial coffee production due to its robust productivity. Nowadays, global market demand encourages a huge variety of coffee product, based on coffee such as espresso. The quality of espresso is influence by many factors such as roasting technique and ratio blending of coffee ground. This study aims to determine the influence of blending ratio and roasting techniqus to the chemical compounds of coffee ground and its espresso brewed. This research used Factorial Random Design, consists of 2 factors. First factor is ratio of blending Arabica and Robusta with three levels ratio; B1=70:30; B2=80:20; and B3=90:10). The second factor is roasting technique, consisting of 2 levels of conventional roasting(P1) and torrefacto (P2). Each treatment was repeated 3 replications to obtain 18 units of experiment. Measured parameters are pH of brewed espresso and moisture (%), ash (%), protein (%), lipid (%) and caffeine (%) contents of coffee ground. The results showed that the blending ratio was highly significant (P≤0,01) to the moisture and protein contents of coffee grounds and pH of resulted espresso. The best treatment was obtained from combination of B1P1 treatment (combination blending ratio (70%:30%) and conventional roasting) with 2.00% moisture content, 4.83% ash, 13.04% protein, 10.41% fat, 81.17% carbohydrate and caffeine 1.49%.

Pengaruh Eksitasi Gelombang Iradiasi Ultrasonik Terhadap Kadar Tanin pada Maserasi Biji Pinang Wangi

Nagari Sikucua, Kampung Dalam Subdistrict, Padang Pariaman produces nearly 800 tons of fragrant areca nut every year which is sent to Jambi to meet export needs. Areca nut contains tannins, substances that have many benefits, some of which are anti-inflammatory, corrosion inhibitors, antioxidants. This study aims to obtain tannins in areca nut extract through a kinetic maceration process with pre-treatment with ultrasonic irradiation wave. The dried areca nut was ground and sieved with various sizes of 20, 40 and 70 mesh and then extracted with ethanol as solvent. The concentration of ethanol used consisted of 35%, 50%, 65% and 80%. Ultrasonic irradiation waves were given for the initial 15 minutes of maceration and then continued with kinetic maceration for up to 4 hours in a water bath at 45°C. The extraction results were concentrated in a rotary evaporator and then tested for tannin levels using Follin Denish reagent in the standard series of tannic acid as a comparison with spectrophotometer UV-Vis. The highest yield of tannin content 11.10% was obtained in the 4-hour maceration process with pre-treatment ultrasonic irradiation at concentration of 80% ethanol with a size of 40 mesh.

Pengaruh Penambahan Stabilizer Carboxyl Metyl Celulosa dan Tepung Agar terhadap Karakteristik Fisiko Kimia Velva Sirsak

Fruits are perishable agro materials, so further processing is necessary after the fruit is harvest. Soursop is a fruit dessert with characteristics like ice cream. The purpose of this study was determined the appropriate compotition and agar powder in the manufacture of soursop velva so that a product with physical characteristics such as ice cream. The physical characteristics of soursop velva are total solid, water content, pH, vitamin C, fiber, total acid, melting speed and overrun. The soursop velva research method with six treatments, A (0,4 % CMC added), B (0,5% CMC added), C (0,6% CMC added), D (0,4% agar powder added), E (0,5% agar powder added), F (0,6% agar powder added). Observation were made on the physico-chemical characteristics of soursop velva. The result shows that soursop Velva added with 0,6% agar powder content 24,79% total solid, 75,24% water content, pH 4,30 and 33, 84 mg/100 g material of vitamin C, 2,2% fiber, 2,2% total acid, with 19,69 minutes melting speed and 134,67% overrun.

Pengaruh Penambahan Gliserin dan Polivinil Alkohol Terhadap Karakteristik Biofoam dari Kulit Singkong dan Daun Angsana

Styrofoam is a petroleum-based and synthetic polymer that is only used once. To reduce waste and environmental damage as well as health problems, this study aims to make biofoam from cassava peel and angsana leaves using a combination of extrusion and baking methods. In this study, glycerin and polyvinyl alcohol were also added with volume variations, 10: 30 (sample 1), 20 : 20 (sample 2), and 30: 10 (sample 3) mL to improve the physical properties of biofoam. The physical characteristics observed were color, water content using the gravimetric method, and water absorption capacity of ABNT NBR NM ISO 535. Sample 1 and sample 2 were lighter in color than sample 3. The lowest water content value was found in sample 2, while sample 2 was has the ability to absorb less water is sample 3.

Penentuan Acid Value pada Fatty Acid dengan Metode Titrasi Alkalimetri dan Kromatografi Gas

PT X processes crude palm kernel oil (CPKO) into products such as glycerin, fatty acid, and fatty alcohol. The purpose of this study was to determine the acid value of fatty acid using alkalimetry titration methods and gas chromatography and compare the values obtained with the PT X standard. The results showed that the AV 105 E21 and 105 E22 were following the PT X standard, with ranges respectively 355-365 mg KOH/gr and 268-275 mg KOH /gr. This indicates that the fatty acid samples produced can be sold to consumers.

Pengaruh Doping Ca dan K pada γ-Al2O3 terhadap Sifat Fisik Katalis pada Transesterifikasi Minyak Kelapa

Metal doping plays important role in increasing catalytic activity of catalyst materials. In this work, Ca and K were doped to the γ-Al2O3 by dry impregnation method to study the crystallinity, surface area, activation energy, and yield in the coconut oil transesterification reaction. The success of doping was shown in the characterization of Ca/γ-Al2O3 and K/γ-Al2O­3 using X-Ray Diffraction (XRD) which increasing in crystallinity from 62.2% (γ-Al2O3) to 69.3 (K/γ-Al2O3) and 76.0 (Ca/γ-Al2O3). The emerging peak of 2θ characteristics of K (29.70° and 32.65°) and Ca (25.35°, 26.77°, and 27.17°) on the γ-Al2O3 (37.66°, 45.82° and 67.22 °) was also observed. Characterization by the Surface Area Analyzer (SAA) shows that the K/γ-Al2O3 catalyst has a smaller surface area (34.03 m2/g) than Ca/γ-Al2O3 (83.77 m2/g), but a higher pore diameter (66.12 Å) than Ca/γ-Al2O3 (35.22 Å). The K/γ-Al2O­3 catalyst produced greater FAME yield (93.19%) than Ca/γ-Al2O3 (29.76%) at a catalyst concentration of 2.5%, reaction time 150 s, and ultrasonic frequency of 40 kHz. The quality of the FAME catalyzed by K/γ-Al2O­3 fulfills four test parameters: density, kinematic viscosity, flash point, and pour point according to SNI 04-7182-2006 standards.