Microsample Testing of Single Crystalline Ti-52 at%Al and Ti-55.5 at%Al

1998 ◽  
Vol 552 ◽  
Author(s):  
Marc Zupan ◽  
D. M. Dimiduk ◽  
K. J. Hemker
Keyword(s):  
Single Crystals ◽  
Mechanical Performance ◽  
Tensile Tests ◽  
High Temperature Stress ◽  
Two Phase ◽  
Single Crystalline ◽  
Al Content ◽  
Float Zone ◽  
Heat Treated ◽  
Solid Foundation

ABSTRACTDislocation activity in two-phase commercial TiAl alloys occurs most readily in the γ-TiAl phase, and measurements of the CRSS of single crystalline γ-TiAl provides a solid foundation for understanding the mechanical performance of these alloys. Single crystals of γ-TiAl with greater than 54.5 at%Al have been grown using the optical float zone crystal growing technique, but single crystals with lower Al content, closer to that of commercial alloys, have not. In the present study, polycrystalline ingots of Ti-52 at%Al have been heat treated to form very large grains, and microsample tensile specimens, which have a nominal gage cross-section of 250μm × 300μm, a gage length of 250μm and an overall length of 3 mm, have been machined from within single grains. Microsample high-temperature stress-strain curves for Ti-55.5 at%Al single crystals oriented along the [001] and [010] are presented. Tensile tests results for Ti-52 at%Al tested at 1073K along the [237], [173] and [344] orientations will also be discussed.

The Formation of A2/L21 Microstructure in Fe-Al-Ti-Cr Alloys

2011 ◽  
Vol 1295 ◽  
Author(s):  
Suguru Hotta ◽  
Satoru Kobayashi ◽  
Takayuki Takasugi
Keyword(s):  
Phase Field ◽  
Quaternary System ◽  
Two Phase ◽  
Al Content ◽  
Cr Content ◽  
Diffusion Multiple ◽  
Heat Treated

ABSTRACTThe composition areas of the A2/L21 two-phase field in the Fe-Al-Ti-Cr quaternary system at 800 ºC and 700 ºC were investigated using a diffusion-multiple (DM) technique for which Fe-30Al-7Ti, Fe-30Cr-7Ti and Fe-7Ti alloys were diffusion-coupled and heat-treated. The A2/L21 two-phase field was found to expand slightly toward lower Al content when the Cr content is increased. The field is slightly shifted toward lower Al content when the temperature is decreased.

Effect of Shock Loading on the Microstructure of Uniloy 326

1974 ◽  
Vol 32 ◽  
pp. 504-505
Author(s):  
K. P. Staudhammer ◽  
L. E. Murr
Keyword(s):  
Grain Size ◽  
Shock Loading ◽  
Current Investigation ◽  
Two Phase ◽  
05 C ◽  
Shock Deformation ◽  
Heat Treated

The effect of shock loading on a variety of steels has been reviewed recently by Leslie. It is generally observed that significant changes in microstructure and microhardness are produced by explosive shock deformation. While the effect of shock loading on austenitic, ferritic, martensitic, and pearlitic structures has been investigated, there have been no systematic studies of the shock-loading of microduplex structures.In the current investigation, the shock-loading response of millrolled and heat-treated Uniloy 326 (thickness 60 mil) having a residual grain size of 1 to 2μ before shock loading was studied. Uniloy 326 is a two phase (microduplex) alloy consisting of 30% austenite (γ) in a ferrite (α) matrix; with the composition.3% Ti, 1% Mn, .6% Si,.05% C, 6% Ni, 26% Cr, balance Fe.

scholarly journals Wastes from Agricultural Silage Film Recycling Line as a Potential Polymer Materials

Polymers ◽  
2021 ◽  
Vol 13 (9) ◽  
pp. 1383
Author(s):  
Jerzy Korol ◽  
Aleksander Hejna ◽  
Klaudiusz Wypiór ◽  
Krzysztof Mijalski ◽  
Ewelina Chmielnicka
Keyword(s):  
Vinyl Acetate ◽  
Thermal Performance ◽  
Mechanical Performance ◽  
Ethylene Vinyl Acetate ◽  
Tensile Tests ◽  
Solid Particles ◽  
Polymer Materials ◽  
Slight Reduction ◽  
Scanning Calorimetry ◽  
Crystallinity Degree

The recycling of plastics is currently one of the most significant industrial challenges. Due to the enormous amounts of plastic wastes generated by various industry branches, it is essential to look for potential methods for their utilization. In the presented work, we investigated the recycling potential of wastes originated from the agricultural films recycling line. Their structure and properties were analyzed, and they were modified with 2.5 wt % of commercially available compatibilizers. The mechanical and thermal performance of modified wastes were evaluated by tensile tests, thermogravimetric analysis, and differential scanning calorimetry. It was found that incorporation of such a small amount of modifiers may overcome the drawbacks caused by the presence of impurities. The incorporation of maleic anhydride-grafted compounds enhanced the tensile strength of wastes by 13–25%. The use of more ductile compatibilizers—ethylene-vinyl acetate and paraffin increased the elongation at break by 55–64%. The presence of compatibilizers also reduced the stiffness of materials resulting from the presence of solid particles. It was particularly emphasized for styrene-ethylene-butadiene-styrene and ethylene-vinyl acetate copolymers, which caused up to a 20% drop of Young’s modulus. Such effects may facilitate the further applications of analyzed wastes, e.g., in polymer film production. Thermal performance was only slightly affected by compatibilization. It caused a slight reduction in polyethylene melting temperatures (up to 2.8 °C) and crystallinity degree (up to 16%). For more contaminated materials, the addition of compatibilizers caused a minor reduction in the decomposition onset (up to 6 °C). At the same time, for the waste after three washing cycles, thermal stability was improved. Moreover, depending on the desired properties and application, materials do not have to go through the whole recycling line, simplifying the process, reducing energy and water consumption. The presented results indicate that it is possible to efficiently use the materials, which do not have to undergo the whole recycling process. Despite the presence of impurities, they could be applied in the manufacturing of products which do not require exceptional mechanical performance.

scholarly journals Chemical and physical interactions of regenerated cellulose yarns and isocyanate-based matrix systems

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Bernhard Ungerer ◽  
Ulrich Müller ◽  
Antje Potthast ◽  
Enrique Herrero Acero ◽  
Stefan Veigel
Keyword(s):  
Mechanical Performance ◽  
Tensile Force ◽  
Tensile Modulus ◽  
Tensile Tests ◽  
Size Exclusion ◽  
Regenerated Cellulose ◽  
Hydrolytic Cleavage ◽  
Yarn Twist ◽  
Exclusion Chromatography ◽  
Physical And Chemical

AbstractIn the development of structural composites based on regenerated cellulose filaments, the physical and chemical interactions at the fibre-matrix interphase need to be fully understood. In the present study, continuous yarns and filaments of viscose (rayon) were treated with either polymeric diphenylmethane diisocyanate (pMDI) or a pMDI-based hardener for polyurethane resins. The effect of isocyanate treatment on mechanical yarn properties was evaluated in tensile tests. A significant decrease in tensile modulus, tensile force and elongation at break was found for treated samples. As revealed by size exclusion chromatography, isocyanate treatment resulted in a significantly reduced molecular weight of cellulose, presumably owing to hydrolytic cleavage caused by hydrochloric acid occurring as an impurity in pMDI. Yarn twist, fibre moisture content and, most significantly, the chemical composition of the isocyanate matrix were identified as critical process parameters strongly affecting the extent of reduction in mechanical performance. To cope with the problem of degradative reactions an additional step using calcium carbonate to trap hydrogen ions is proposed.

scholarly journals Mechanical Optimization of Concrete with Recycled PET Fibres Based on a Statistical-Experimental Study

Materials ◽  
2021 ◽  
Vol 14 (2) ◽  
pp. 240
Author(s):  
Alejandro Meza ◽  
Pablo Pujadas ◽  
Laura Montserrat Meza ◽  
Francesc Pardo-Bosch ◽  
Rubén D. López-Carreño
Keyword(s):  
Reinforced Concrete ◽  
Aspect Ratio ◽  
Mechanical Performance ◽  
Tensile Tests ◽  
Superior Performance ◽  
Fibre Reinforced Concrete ◽  
Marine Fauna ◽  
Recycled Pet ◽  
Pet Bottles ◽  
Fibre Aspect Ratio

Discarded polyethylene terephthalate (PET) bottles have damaged our ecosystem. Problems of marine fauna conservation and land fertility have been related to the disposal of these materials. Recycled fibre is an opportunity to reduce the levels of waste in the world and increase the mechanical performance of the concrete. PET as concrete reinforcement has demonstrated ductility and post-cracking strength. However, its performance could be optimized. This study considers a statistical-experimental analysis to evaluate recycled PET fibre reinforced concrete with various fibre dose and aspect ratio. 120 samples were experimented under workability, compressive, flexural, and splitting tensile tests. The results pointed out that the fibre dose has more influence on the responses than its fibre aspect ratio, with statistical relation on the tensional toughness, equivalent flexural strength ratio, volumetric weight, and the number of fibres. Moreover, the fibre aspect ratio has a statistical impact on the tensional toughness. In general, the data indicates that the optimal recycled PET fibre reinforced concrete generates a superior performance than control samples, with an improvement similar to those reinforced with virgin fibres.

Effect of copper incorporation on phase transformation behavior of electroless nickel–phosphorous coating and its effect on the tribological behavior

2020 ◽  
pp. 146442072098160
Author(s):  
Abhijit Biswas ◽  
Suman Kalyan Das ◽  
Prasanta Sahoo
Keyword(s):  
Heat Treatment ◽  
Phase Transformation ◽  
Tribological Behavior ◽  
Electroless Nickel ◽  
Two Phase ◽  
Microstructural Changes ◽  
Treatment Conditions ◽  
Heat Treated ◽  
Higher Temperature ◽  
Effect Of Copper

The microstructural changes of electroless Ni–P–Cu coating at various heat-treatment conditions are investigated to understand its implications on the tribological behavior of the coating. Coatings are heat-treated at temperatures ranging between 200°C and 800 °C and for 1–4 h duration. Ni–P–Cu coatings exhibit two-phase transformations in the temperature range of 350–450 °C and the resulting microstructural changes are found to significantly affect their thermal stability and tribological attributes. Hardness of the coating doubles when heat-treated at 452 °C, due to the formation of harder Ni3P phase and crystalline NiCu. Better friction and wear performance are also noted upon heat treatment of the coating at the phase transformation regime, particularly at 400 °C. Wear mechanism is characterized by a mixed adhesive cum abrasive wear phenomena. Heat treatment at higher temperature (600 °C and above) and longer duration (4 h) results in grain coarsening phenomenon, which negatively influences the hardness and tribological characteristics of the coating. Besides, diffusion of iron from the ferrous substrate as well as greater oxide formation are noticed when the coating is heat-treated at higher temperatures and for longer durations (4 h).

scholarly journals Mechanical and thermal stability of retained austenite in plastically deformed bainite-based TRIP-aided medium-Mn steels

2021 ◽  
Vol 21 (3) ◽  
Author(s):  
Aleksandra Kozłowska ◽  
Adam Grajcar ◽  
Aleksandra Janik ◽  
Krzysztof Radwański ◽  
Ulrich Krupp ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Thermal Stability ◽  
Retained Austenite ◽  
Elevated Temperatures ◽  
Mechanical Performance ◽  
Mechanical Stability ◽  
Electron Backscatter Diffraction ◽  
Cost Effective ◽  
Tensile Tests ◽  
Thermal Stability Of

AbstractAdvanced medium-Mn sheet steels show an opportunity for the development of cost-effective and light-weight automotive parts with improved safety and optimized environmental performance. These steels utilize the strain-induced martensitic transformation of metastable retained austenite to improve the strength–ductility balance. The improvement of mechanical performance is related to the tailored thermal and mechanical stabilities of retained austenite. The mechanical stability of retained austenite was estimated in static tensile tests over a wide temperature range from 20 °C to 200 °C. The thermal stability of retained austenite during heating at elevated temperatures was assessed by means of dilatometry. The phase composition and microstructure evolution were investigated by means of scanning electron microscopy, electron backscatter diffraction, X-ray diffraction and transmission electron microscopy techniques. It was shown that the retained austenite stability shows a pronounced temperature dependence and is also stimulated by the manganese addition in a 3–5% range.

Dynamic Crack Propagation in Single-Crystalline Silicon

1998 ◽  
Vol 539 ◽  
Author(s):  
T. Cramer ◽  
A. Wanner ◽  
P. Gumbsch
Keyword(s):  
Crack Propagation ◽  
Crystalline Silicon ◽  
Potential Drop ◽  
Tensile Tests ◽  
Terminal Velocity ◽  
Dynamic Crack Propagation ◽  
Dynamic Crack ◽  
Single Crystalline Silicon ◽  
Single Crystalline ◽  
Crack Propagation Velocity

AbstractTensile tests on notched plates of single-crystalline silicon were carried out at high overloads. Cracks were forced to propagate on {110} planes in a <110> direction. The dynamics of the fracture process was measured using the potential drop technique and correlated with the fracture surface morphology. Crack propagation velocity did not exceed a terminal velocity of v = 3800 m/s, which corresponds to 83%7 of the Rayleigh wave velocity vR. Specimens fractured at low stresses exhibited crystallographic cleavage whereas a transition from mirror-like smooth regions to rougher hackle zones was observed in case of the specimens fractured at high stresses. Inspection of the mirror zone at high magnification revealed a deviation of the {110} plane onto {111} crystallographic facets.

Micromechanical analysis of effective mechanical properties of graphene/ZrO2-hybrid poly (methyl methacrylate) nanocomposites

2021 ◽  
pp. 251659842110388
Author(s):  
Ankit Rathi ◽  
S. I. Kundalwal
Keyword(s):  
Methyl Methacrylate ◽  
Elastic Properties ◽  
Mechanical Performance ◽  
Volume Fraction ◽  
Element Model ◽  
Two Phase ◽  
Effective Elastic Properties ◽  
Poly Methyl Methacrylate ◽  
Three Phase ◽  
Effective Mechanical Properties

In this study, the tensile properties of two-phase and three-phase graphene/ZrO2-hybrid poly (methyl methacrylate) (PMMA) nanocomposites are investigated by developing finite element model using ANSYS. Primarily, the effective elastic properties of two- and three-phase graphene/ZrO2-hybrid PMMA nanocomposites (GRPCs) are estimated by developing mechanics of material (MOM) model. Results indicated that the effective elastic properties of GRPCs increase with an increase in the volume fraction of graphene. Also, the stiffness of GRPCs is increased by 78.12% with increasing in the volume fraction of graphene from 0.1 to 0.5 Vf. The incorporation of an additional ZrO2 interphase significantly improved the mechanical performance of resulting GRPCs.

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