Extraction Process of Amaranthine Pigment Keeping the Water Wax Fuit Biological Active

2013 ◽  
Vol 295-298 ◽  
pp. 150-154
Author(s):  
Feng Jie Wang ◽  
Xin Qiao Dong ◽  
Xiao Liu

Development natural pigment retained a variety of nutrition composition is extremely research value.Water Wax Trees Fruit was as raw materials,citric acid aqueous solution was as extracting agent.Amaranthine pigment extraction method were studied on fully grasping the stability of the natural amaranthine pigment and no damage to the water wax fruit biological activity.The effect of extraction yield were studied on Water Wax Trees Fruit natural amaranthine pigment.The results show that the better extraction conditions are extraction temperature at 70 °C, extraction time for 3h,citric acid concentration1.0 % , the material/liquid ration(g/ml) 1:5.The extraction yield is 2.95%.Ultraviolet absorption maximum wavelength is 280 nm.

2014 ◽  
Vol 608-609 ◽  
pp. 1128-1130
Author(s):  
Yan Ying Weng ◽  
Guang Kuang Deng

In order to optimize the extraction technology of total Saponin of Gynostemma pentaphyllum by decompressing innner ebullition, the technology was established between the extraction yield of total Saponin and several independent variables (the concentration of desorption agent, solid-liquid ratio, extraction temperature and time) through orthogonal test ,which was based on the single factor experiment. Experiment results show that the optimum extraction conditions for 5.0 g raw materials are as followed: the volume fraction of ethanol solution saturated the materials is 60% , the volume of water is 19 times to material. The extraction process can finish after 5 min at 50 °C twice. The results indicate that orthogonal test design can be an effective method to optimize the extraction technology of total Saponin of Gynostemma pentaphyllum through decompressing innner ebullition.


Molecules ◽  
2020 ◽  
Vol 25 (18) ◽  
pp. 4209
Author(s):  
Anca Becze ◽  
Vanda Liliana Babalau-Fuss ◽  
Cerasel Varaticeanu ◽  
Cecilia Roman

Circular economy principles are based on the use of by-products from one operation as the raw materials in another. The aim of this work is to obtain extracts with high antioxidant capacity and resveratrol content for the superior capitalization of the biomass of Feteasca regala leaves obtained during vineyard horticultural operations in spring. In order to obtain a high-quality extract at an industrial level, an optimal extraction process is needed. Central composite design (CCD) was used for the experiment design, which contained three independent variables: the ratio of extraction solvent to solid matter, temperature (°C) and time (minutes). The evaluation of extracts was done by measuring the total antioxidant capacity of the extracts using photo-chemiluminescent techniques, and the resveratrol content using liquid chromatography. Process optimization was done using response surface methodology (RSM). Minitab software version 17.0 was used for the design of experiments and data analysis. Regression analysis showed that the model predicts 87.5% of the variation for resveratrol and 96% for total antioxidant capacity (TAC). The temperature had the biggest influence on the extraction yield. The optimal operational conditions for the extraction method applied had the following conditions: ratio e/m 2.92; 43.23 °C and 55.4 min. A maximum value of 34,623 µg ascorbic acid equivalent (AAE) /mL total antioxidant capacity and 182.4 µg/mL resveratrol content were obtained when the optimal extraction parameters where used. The values obtained in experiments proved that by using RSM an accurate model can be obtained for extraction of Feteasca regala leaves.


Author(s):  
Wahbi Kalook ◽  
Adib Faleh ◽  
Amir Al-Haj Sakur ◽  
Wassim Abdelwahed

The aim of this research is to extract carotenoids from apricot fruits using a food solvent (ethanol) and a non-food solvent (propanol). In addition, it aims to study the effect of different extraction conditions, i.e., the extraction temperature (20-40-60)°C and the extraction times (4-8-12) hours, on the carotenoids yield in order to improve and develop extraction methods. The extracted carotenoids were determined using high-performance liquid chromatography (HPLC), and the studied carotenoids are α-carotene and β-carotene. It was found that β-carotene constitutes about 80% of the total carotenoids in apricots. The results indicated that the extraction yield using ethanol was low compared to the extraction yield using propanol. Propanol is the most suitable solvent for carotenoids extraction in comparison with ethanol. The temperature also had a significant effect on the extraction yield; at 20°C the extraction yield was very low, and 60°C was the optimum temperature for the extraction of carotene. The extraction yield significantly increased with time in the first hours of extraction, and there was no significant effect from increasing the extraction time for a period of 6-8 hours. Moreover, the pretreatment of fruits by freezing accelerated the extraction process and increased the extraction yield. The optimum conditions for extracting carotenoids were determined in the conditions of food extraction; the optimum conditions for extracting carotenoids are: extraction at 60°C for three hours with pretreatment by freezing as the extraction rate reached up to 6.36 mg/100 g using ethanol as a food solvent.


2021 ◽  
Vol 267 ◽  
pp. 02010
Author(s):  
Rui Wang ◽  
Xueqin Zhang ◽  
Qian Zhou

Moringa leaves were used as raw materials, ethanol and ammonium sulfate were used to construct a aqueous two-phase system to extract the flavonoids from Moringa leaves. The solid-liquid ratio, ethanol content, ultrasonic extraction time, and ultrasonic extraction temperature were selected as single factors, and the extraction process of flavonoids was optimized through single-factor experiments and orthogonal experiments. The optimal process was: 1:110 of solid-liquid ratio, 45 % of ethanol concentration, 15 minutes of ultrasonic extraction time, 70 °C of ultrasonic extraction temperature. Under this condition, the extraction rate of Moringa leaf flavonoids reached 8.37 %.


Pro Food ◽  
2017 ◽  
Vol 3 (1) ◽  
pp. 178
Author(s):  
Lisa Yusmita ◽  
Anwar Kasim ◽  
Hazli Nurdin

The aim of this research was to determine the best extraction temperature and concentration of citric acid in the extraction of betacyanin powder from Dentata Ruby leaves (Alternanthera dentata) and to know organoleptic panelist reception in the application of betacyanin pigment as a natural colourant to several food types. The design used in this research is Factorial Random Design (RAL) with 2 factors and 3 replications. The data obtained were analyzed statistically by F test, then if significant effect was continued with HSD-Tukey test at 5% real level. The extraction temperature factor consisting of 2 levels ie cold temperature (8oC) and room temperature (25oC), and the citric acid concentration factor consisting of 4 levels ie 0%, 1%, 3% and 5%. The results showed that the interaction between extraction temperature and citric acid concentration in the extraction process gave significantly different effect on betacyanin concentration, acidity degree (pH), total acid and powder yield. The extract of betacyanin pigment powder extracted at room temperature (25oC) with the addition of 0% citric acid was the best treatment with betacyanin concentration of 214.47 mg / 100 g of material, pH 5.85 and total acid of 1.272% and powder yield of 56.43 %. The application of betacyanin powder extract on jelly, syrup and ice cream can be accepted organoleptically by the best treatment that is the addition at 1.5%concentration. Key words: antioxidants, betacyanin, dentata ruby, colourant   ABSTRAK Penelitian ini bertujuan untuk menentukan suhu ekstraksi dan konsentrasi asam sitrat terbaik pada ekstraksi pigmen betacyanin daun kremah merah (Alternanthera dentata) dan mengetahui penerimaan panelis secara organoleptik terhadap aplikasi pigmen betacyanin sebagai pewarna alami terhadap beberapa jenis pangan. Rancangan yang digunakan dalam penelitian ini adalah Rancangan Acak Lengkap (RAL) faktorial dengan 2 faktor dan 3 kali ulangan. Data yang diperoleh dianalisa secara statistik dengan uji F, kemudian bila berpengaruh nyata dilanjutkan dengan uji HSD-Tukey pada taraf nyata 5%. Faktor suhu ekstraksi yang terdiri dari 2 taraf yaitu suhu dingin ( 8oC) dan suhu kamar (25oC), sedangkan faktor konsentrasi asam sitrat yang terdiri dari 4 taraf yaitu 0 %, 1%, 3% dan 5%. Hasil penelitian menunjukkan interaksi antara suhu ekstraksi dan konsentrasi asam sitrat pada proses ekstraksi memberikan pengaruh yang berbeda nyata terhadap konsentrasi betacyanin, derajat keasaman (pH) dan total asam serta rendemen bubuk. Ekstrak bubuk pigmen betacyanin yang diekstraksi pada suhu kamar (25oC) dengan penambahan asam sitrat 0 % merupakan perlakuan terbaik dengan karakteristik konsentrasi betacyanin sebesar 214,47 mg/100 g bahan, pH 5,85 dan total asam 1,272 % serta rendemen bubuk 56,43 %. Aplikasi penambahan ekstrak bubuk pigmen betacyanin pada jelly, sirup dan es krim dapat diterima secara organoleptik dengan perlakuan terbaik yaitu penambahan pada konsentrasi 1,5 %. Kata kunci: antioksidan, betacyanin, kremah merah, pewarna.


2019 ◽  
Vol 814 ◽  
pp. 527-531
Author(s):  
Trieu Tuan Anh ◽  
Luu Tu Hao ◽  
Long Giang Bach ◽  
Duy Chinh Nguyen ◽  
Tri Duc Lam

Jasminum Subtriplinerve Blume (Oleaceae) is herbal plants widely a tea for weight loss, stimulates milk glands. Extract product it easy used yet had little research. This study was carried out to evaluate the effect of extracting conditions such as water/material ratio, extraction temperature and extracting time on extracting yield, polyphenol content and antioxidant activity of J.subtriplinerve extract. The total phenolic compounds were determined according to the Folin–Ciocalteu method. Extraction yield (0.22g/100 g) was obtained at water/material ratio 15:1 (ml/g), 40°C and 4 hours extraction time. Under these optimized conditions, the polyphenol content of was 2640.4 μg/1g extract. And the extract can harvest 46.11 % of DPPH (30 μg/ mL) at 10 000 μg/ml concentration


Polymers ◽  
2020 ◽  
Vol 12 (3) ◽  
pp. 529 ◽  
Author(s):  
José C. C. Santana ◽  
Roberta B. Gardim ◽  
Poliana F. Almeida ◽  
Giovanna B. Borini ◽  
Ada P. B. Quispe ◽  
...  

In this research, products with high quality were obtained from natural sources. The sensorial qualities, chemical characterization, and physical properties of gelatin extracted from chicken feet were compared with commercial gelatins. The extraction process was performed using acetic acid on a concentration ranging from 0.318% to 3.682%, processing time between 1.0 h and 8.4 h and extraction temperature between 43.3 °C and 76.8 °C. After the end of each assay, the yield was measured. Results showed that, under the best conditions, the collagen extraction yield was above 8%, and comprised 78.525 g/100 g of protein. Collagen analyzed by ICP-MS was composed of 99.44% of macro-minerals that are of great importance to human health. ATR-FTIR analysis showed that approximately 70.90% of the total protein from chicken feet is collagen, whereas, in commercial gelatin, only 30.31% is collagen. When comparing chicken gelatin with commercial gelatin, most sensory attributes were similar and chicken gelatin gained acceptance by more than 80% of the consumers. Additionally, the collagen films obtained from chicken feet and swine showed water absorption, odors, and texture characteristics similar to commercial material, such as latex and celofane. Consequently, due to its similarity to human skin, it is possible to apply it as a biocurative.


2013 ◽  
Vol 781-784 ◽  
pp. 1886-1890
Author(s):  
Fei Long Sun ◽  
Zhang Peng Li ◽  
Ting Li ◽  
Yong Fan ◽  
Yan Chu ◽  
...  

Natural pigments have raised a growing interest due to their extensive range of colors, innocuous and beneficial health effects. In this paper, the extraction process and stability of strawberry red pigment were studied. An orthogonal test [L16(4)4] was applied to get the best extraction conditions. Results showed that the optimum conditions were that the extraction temperature was 65C, the solid-liquid ratio was 1:5 (g/mL), the ratio of 1.5mol/L hydrochloride to 97.5% ethanol was 3:17 (mL/mL), and the extraction time was 4.5 hours. The effects of heat treatment, oxidant, sugar and preservatives on the stability of strawberry red pigment were also discussed. The stability of strawberry red pigment was found to be affected by high temperature, hydrogen peroxide, and potassium sorbate. This study is expected to provide a basis for further research, development, and utilization of strawberry red pigment.


2021 ◽  
Vol 19 (1) ◽  
pp. 830-842
Author(s):  
Quoc Toan Tran ◽  
The Dan Pham ◽  
Thanh Duong Nguyen ◽  
Van Huyen Luu ◽  
Huu Nghi Do ◽  
...  

Abstract Glycosmis stenocarpa is a species of shrub found in the Northern provinces of Vietnam. Its roots contain different carbazolic derivatives, mainly Murrayafoline A (Mu-A), which exhibits valuable biological activities. In this study, we performed an extraction of Mu-A from the roots of G. stenocarpa and optimized this process using response surface methodology (RSM) according to a central composite design, with three independent parameters including extraction time (min), extraction temperature (°C), and solvent/material ratio (mL/g). Two dependent variables were the Mu-A content (mg/g raw materials) and extraction efficiency (%). The optimal conditions to extract Mu-A were found to be as follows: extraction temperature, 67°C; extraction time, 165 min; and solvent/material ratio, 5:1. Under these conditions, the Mu-A content and extraction efficiency were 38.94 ± 1.31 mg/g raw materials and 34.98 ± 1.18%, respectively. Mu-A exhibited antiproliferation and antitumor-promoting activity against the HepG-2 cell line. The present optimization work of Mu-A extraction from G. stenocarpa roots contributed to the attempt of designing a large-scale extraction process for the compound and further exploitation of its potential in vivo applications.


Author(s):  
Larisa Fialkovska

Іn the article an overview of the methods of extraction of oilseeds is carried out. The purpose of the work was to carry out the study of the extraction process at the installation for extraction in an electromagnetic intensifier (EEMI). The only way to ensure virtually complete oil extraction is the extraction method, in which the forces that convert the oil into a solution exceed the forces that hold oil in the extracted material. Today, the extraction method for oil extraction at Ukrainian plants is leading, as it provides greater yield of oil than with the use of the press process. The object of research is the use of rapeseed and soybean seeds, locally, oil obtained as a result of extraction of oilseeds. Experimental researches were carried out in laboratory conditions at the department "Processes and equipment of processing and food industries of a name of professor P. S. Bernik" of Vinnytsia National Agrarian University. Production tests of the laboratory sample of the extractor were carried out at PJSC "Vinnitsa OZHK". Physical and chemical researches of raw materials and intermediate materials were carried out. The optimum temperature regimes of the extraction process are established. The expediency and necessity of use as a solvent of ethyl alcohol is described. The research of rapeseed and soybean oils obtained as a result of extraction was conducted. The production of oil on the plant for extraction in an electromagnetic intensifier (EEMI) will enable the product to meet the requirements of regulatory documents and has a higher content of biologically active substances - tocopherols in comparison with traditional methods.


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