Copper slag as a potential waste filler for polyethylene-based composites manufacturing

2021 ◽  
Vol 47 (2) ◽  
pp. 405-420
Author(s):  
Aleksander Hejna ◽  
Paulina Kosmela ◽  
Mateusz Barczewski ◽  
Olga Mysiukiewicz ◽  
Adam Piascki
Keyword(s):  
Mechanical Properties ◽  
Mechanical Performance ◽  
Copper Slag ◽  
Tensile Tests ◽  
Mechanical Analysis ◽  
Filler Loading ◽  
Copper Production ◽  
Color Analysis ◽  
Composites Manufacturing ◽  
Static Tensile

The present study aimed to analyze the application of waste material from copper production– copper slag (ŻŻL) as filler for composites based on the high-density polyethylene (HDPE). Copper slag filler was introduced in the amounts of 1–20 wt%, and its influence on the appearance (color analysis), chemical structure (Fourier-transform infrared (FTIR) spectroscopy), microstructure (optical microscopy), as well as static (tensile tests) and dynamic (dynamical mechanical analysis (DMA)) mechanical properties of composites were investigated. Proper dispersion of filler implicated that the incorporation of up to 5 wt% of filler caused only slight, 5% drop of tensile strength, with the simultaneous 16% rise of Young’s modulus. Further increase of filler loading resulted in higher values of porosity and the rise of the adhesion factor, determined from DMA results, which led to the deterioration of mechanical performance. Moreover, spectroscopic analysis of PE-ŻŻL composites indicated that the analyzed filler might be applied as a coloring agent, and the appearance of composites may be engineered by adjustment of filler loading. Keywords: polyethylene, copper slag, mechanical properties, structure, composite, particle reinforced composite

scholarly journals Microstructure and Mechanical Performance of Graphene Nanosheets Reinforced Nickel-Based Superalloy FGH95 Composite

Nanomaterials ◽  
2020 ◽  
Vol 10 (1) ◽  
pp. 100
Author(s):  
Yuxi Gao ◽  
Jinwen Zou ◽  
Xuqing Wang ◽  
Xiaofeng Wang ◽  
Jie Yang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
High Temperature ◽  
Room Temperature ◽  
Mechanical Performance ◽  
Graphene Nanosheets ◽  
Tensile Tests ◽  
Interface Debonding ◽  
Failure Behavior ◽  
Nickel Based Superalloy ◽  
Static Tensile

Graphene nanosheet (GNS)-reinforced nickel-based superalloy FGH95 (GNSs/FGH95) matrix composites are prepared via the powder metallurgy approach. Scanning electron microscopy, transmission electron microscope and static tensile tests are used to investigate the microstructure and mechanical properties of GNS-reinforced nickel-based superalloy FGH95. Mechanical properties and failure behavior at room temperature and high temperature are studied. Static tensile tests at room temperature and high temperature confirm that the strength and plasticity of GNS-reinforced FGH95 have been improved, compared to the unreinforced superalloy. The results show that with the increase of temperature, the failure behavior of GNSs/FGH95 composite changes from the interface debonding of the GNSs/matrix to the failure of the FGH95 matrix. This work suggests that GNSs/FGH95 composite has great potential to be a structural material in aero-engine fields.

scholarly journals Mechanical, Thermal and Rheological Properties of Polyethylene-Based Composites Filled with Micrometric Aluminum Powder

Materials ◽  
2020 ◽  
Vol 13 (5) ◽  
pp. 1242
Author(s):  
Olga Mysiukiewicz ◽  
Paulina Kosmela ◽  
Mateusz Barczewski ◽  
Aleksander Hejna
Keyword(s):  
Mechanical Properties ◽  
Melt Flow Index ◽  
Tensile Tests ◽  
Mechanical Analysis ◽  
Flow Index ◽  
Scanning Calorimetry ◽  
Metal Composites ◽  
Pre Treatment ◽  
The Impact ◽  
Properties Of Composites

Investigations related to polymer/metal composites are often limited to the analysis of the electrical and thermal conductivity of the materials. The presented study aims to analyze the impact of aluminum (Al) filler content (from 1 to 20 wt%) on the rarely investigated properties of composites based on the high-density polyethylene (HDPE) matrix. The crystalline structure, rheological (melt flow index and oscillatory rheometry), thermal (differential scanning calorimetry), as well as static (tensile tests, hardness, rebound resilience) and dynamic (dynamical mechanical analysis) mechanical properties of composites were investigated. The incorporation of 1 and 2 wt% of aluminum filler resulted in small enhancements of mechanical properties, while loadings of 5 and 10 wt% provided materials with a similar performance to neat HDPE. Such results were supported by the lack of disturbances in the rheological behavior of composites. The presented results indicate that a significant content of aluminum filler may be introduced into the HDPE matrix without additional pre-treatment and does not cause the deterioration of composites’ performance, which should be considered beneficial when engineering PE/metal composites.

Enhancement of the Mechanical Properties of PEBAX Graphene Nanocomposite Using Supercritical Fluid Assisted Extrusion Polymer Processing Technique

2017 ◽  
Vol 883 ◽  
pp. 75-84 ◽  
Author(s):  
Nireeksha Karode ◽  
Laurence Fitzhenry ◽  
Siobhán Matthews ◽  
Philip Walsh ◽  
Austin Coffey
Keyword(s):  
Mechanical Properties ◽  
Carbon Dioxide ◽  
Supercritical Carbon Dioxide ◽  
Mechanical Performance ◽  
Mechanical Analysis ◽  
Polymer Processing ◽  
Processing Technique ◽  
Graphene Nanocomposites ◽  
Mechanical Tensile ◽  
Supercritical Carbon

Medical tubing used in minimally invasive devices presents a number of design considerations depending on the material used, design requirements (such as sufficient stiffness, flexibility and biocompatibility) and processing conditions. Currently, manufacturing industries adopt co-extrusion systems to meet design specifications, by using multilayer configuration leading to higher cost per device and increased complexity. This paper investigates the mechanical performance of nanocomposites using supercritical carbon dioxide assisted polymer processing technique. The use of innovative medical compounds such as PEBAX graphene nanocomposites have resulted in measurable improvements in mechanical properties. This study also presents the effect of supercritical carbon dioxide on the mechanical and physical properties of the polymer matrix. The mechanical properties have been investigated using dynamic mechanical analysis (DMA) and mechanical tensile test, where sufficient reinforcement was observed depending on the composition of graphene within PEBAX matrix. ATR-FTIR was used to further analyze the effect of supercritical carbon dioxide and interactions within the polymer composite matrix.

Enhancing the Thermal and Mechanical Characteristics of Polyvinyl Alcohol (PVA)-Hemp Protein Particles (HPP) Composites

2021 ◽  
Vol 36 (2) ◽  
pp. 137-143
Author(s):  
S. A. Awad
Keyword(s):  
Mechanical Properties ◽  
Elevated Temperatures ◽  
Composite Films ◽  
Tensile Tests ◽  
Mechanical Analysis ◽  
Decomposition Temperature ◽  
Scanning Calorimetry ◽  
Solution Casting Method ◽  
Protein Particles

Abstract This paper aims to describe the thermal, mechanical, and surface properties of a PVA/HPP blend whereby the film was prepared using a solution casting method. The improvements in thermal and mechanical properties of HPP-based PVA composites were investigated. The characterization of pure PVA and PVA composite films included tensile tests, thermogravimetric analysis (TGA), and differential scanning calorimetry (DSC). The results of TGA and DSC indicated that the addition of HPP increased the thermal decomposition temperature of the composites. Mechanical properties are significantly improved in PVA/HPP composites. The thermal stability of the PVA composite increased with the increase of HPP filler content. The tensile strength increased from 15.74 ± 0.72 MPa to 27.54 ± 0.45 MPa and the Young’s modulus increased from 282.51 ± 20.56 MPa to 988.69 ± 42.64 MPa for the 12 wt% HPP doped sample. Dynamic mechanical analysis (DMA) revealed that at elevated temperatures, enhanced mechanical properties because of the presence of HPP was even more noticeable. Morphological observations displayed no signs of agglomeration of HPP fillers even in composites with high HPP loading.

Performance of All-Polypropylene Composites at LNG Temperatures

2017 ◽  
Author(s):  
Bilim Atli-Veltin
Keyword(s):  
Composite Materials ◽  
Mechanical Performance ◽  
Cost Effective ◽  
Tensile Tests ◽  
Small Scale ◽  
Failure Behavior ◽  
Polypropylene Composites ◽  
Design Flexibility ◽  
Static Tensile ◽  
Interlaminar Shear

In the small scale LNG infrastructure, composite materials are scarcely employed. Potentially, cost effective solutions for LNG applications could be developed thanks to the advantages of composite materials over metals such as weight savings, design flexibility and recyclability. The research presented in this paper focuses on the mechanical performance of fully recyclable, thermoplastic Polypropylene (PP) composite tapes at cryogenic LNG temperatures. Quasi-static tensile tests performed on [±45] laminates made of plain woven plies of PURE® show that at −196°C the behavior is bilinear with the failure strain of 6.5% and failure stress of 37 MPa. Such non-brittle failure behavior of PP is desirable for cryogenic applications. The other results presented in the paper contains [0/90] laminate results and the interlaminar shear strength characteristics at room and cryogenic temperatures.

scholarly journals Polymeric Composites Based on Polyurea Matrix Reinforced with Carbon Nanotubes

2017 ◽  
Vol 54 (1) ◽  
pp. 41-44 ◽  
Author(s):  
Maria Adina Vulcan ◽  
Celina Damian ◽  
Paul Octavian Stanescu ◽  
Eugeniu Vasile ◽  
Razvan Petre ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Carbon Nanotubes ◽  
Thermal Stability ◽  
Scanning Electron Microscopy ◽  
Tensile Tests ◽  
Mechanical Analysis ◽  
Multi Walled Carbon Nanotubes ◽  
Walled Carbon Nanotubes ◽  
Scanning Electron

This paper deals with the synthesis of polyurea and its use as polymer matrix for nanocomposites reinforced with multi-walled carbon nanotubes (MWCNT). Two types of materials were obtained during this research, the first cathegory uses the polyurea as matrix and the second one uses a mixture between epoxy resin and polyurea. The nanocomposites were characterized by Thermogravimetric Analysis (TGA), Dynamic Mechanical Analysis (DMA), Scanning Electron Microscopy (SEM) and Tensile Tests .The elastomeric features of nanocomposites were highlighted by the results which showed low value of Tg. Also higher thermal stability with ~40oC compared with commercial products (M20) were observed, but lower mechanical properties compared to neat polyurea.

scholarly journals Microstructural Characterization and Mechanical Properties of L-PBF Processed 316 L at Cryogenic Temperature

Materials ◽  
2021 ◽  
Vol 14 (19) ◽  
pp. 5856
Author(s):  
Pragya Mishra ◽  
Pia Åkerfeldt ◽  
Farnoosh Forouzan ◽  
Fredrik Svahn ◽  
Yuan Zhong ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Cryogenic Temperature ◽  
Room Temperature ◽  
Mechanical Performance ◽  
Microstructural Characterization ◽  
Tensile Tests ◽  
Phase Changes ◽  
X Ray Diffraction ◽  
Temperature Range ◽  
Aerospace Applications

Laser powder bed fusion (L-PBF) has attracted great interest in the aerospace and medical sectors because it can produce complex and lightweight parts with high accuracy. Austenitic stainless steel alloy 316 L is widely used in many applications due to its good mechanical properties and high corrosion resistance over a wide temperature range. In this study, L-PBF-processed 316 L was investigated for its suitability in aerospace applications at cryogenic service temperatures and the behavior at cryogenic temperature was compared with room temperature to understand the properties and microstructural changes within this temperature range. Tensile tests were performed at room temperature and at −196 °C to study the mechanical performance and phase changes. The microstructure and fracture surfaces were characterized using scanning electron microscopy, and the phases were analyzed by X-ray diffraction. The results showed a significant increase in the strength of 316 L at −196 °C, while its ductility remained at an acceptable level. The results indicated the formation of ε and α martensite during cryogenic testing, which explained the increase in strength. Nanoindentation revealed different hardness values, indicating the different mechanical properties of austenite (γ), strained austenite, body-centered cubic martensite (α), and hexagonal close-packed martensite (ε) formed during the tensile tests due to mechanical deformation.

The Structure and Mechanical Properties of Plastically Consolidated Al-Ni Alloy

2016 ◽  
Vol 682 ◽  
pp. 245-251 ◽  
Author(s):  
Grzegorz Włoch ◽  
Tomasz Skrzekut ◽  
Jakub Sobota ◽  
Antoni Woźnicki ◽  
Justyna Cisoń
Keyword(s):  
Mechanical Properties ◽  
Vickers Hardness ◽  
Tensile Tests ◽  
Mechanical Analysis ◽  
Intermetallic Phases ◽  
Scanning Calorimetry ◽  
Porosity Formation ◽  
X Ray ◽  
Ni Alloy ◽  
Thermal Stability Of

Mixed and preliminarily consolidated powders of aluminium and nickel (90 mass % Al and 10 mass % Ni) were hot extruded. As results the rod, 8 mm in diameter, was obtained. As-extruded material was subjected to the microstructural investigations using scanning electron microscopy (SEM/EDS) and X-ray analysis (XRD). The differential scanning calorimetry (DSC) and thermo-mechanical analysis (TMA) were also performed. The mechanical properties of as extruded material were determined by the tensile test and Vickers hardness measurements. In order to evaluate the thermal stability of PM alloy, samples were annealed at the temperature of 475 and 550 °C. After annealing Vickers hardness measurements and tensile tests were carried out. The plastic consolidation of powders during extrusion was found to be very effective, because no pores or voids were observed in the examined material. The detailed microstructural investigations and XRD analyses did not reveal the presence of the intermetallic phases in the as-extruded material. During annealing, the Al3Ni intermetallic compound was formed as the result of chemical reaction between the alloy components. The hardness of the alloy after annealing at the temperature of 475°C was found to be comparable to the hardness in as-extruded state. Annealing of the material at the temperature of 550°C results in hardness decreasing by about 50%, as the consequence of porosity formation and Al3Ni cracking.

Mechanical Properties of Flat Braided Composites With a Circular Hole

1999 ◽  
Author(s):  
Takeru Ohki ◽  
Shinya Ikegaki ◽  
Ken Kurasiki ◽  
Hiroyuki Hamada ◽  
Masaharu Iwamoto
Keyword(s):  
Mechanical Properties ◽  
Tensile Test ◽  
Circular Hole ◽  
Fracture Behavior ◽  
Fatigue Property ◽  
Tensile Tests ◽  
Fatigue Tests ◽  
Braided Composites ◽  
Static Tensile ◽  
The One

Abstract In this study, fracture behavior and strength in the flat braided bar with a circular hole were investigated by static and fatigue test. Two type of specimens were prepared. They are a braided flat bar with an integrally-formed braided hole and a braided flat bar with a machined hole. Moreover, we also examined a specimen that had a metal pin inserted at the circular hole. This specimen was subjected to a static tensile test. The results of the tensile tests indicate that the strength of the flat bar with a braided hole was larger than that of the one with the machined hole. Furthermore, from the results of the fatigue tests, the flat bar with the braided hole showed higher fatigue property than that of the one with the machined hole.

Revaluation of Australian palm residues in polypropylene composites: Statistical influence of fiber treatment

2020 ◽  
pp. 002199832096053 ◽  
Author(s):  
Noelle C Zanini ◽  
Rennan FS Barbosa ◽  
Alana G de Souza ◽  
Derval S Rosa ◽  
Daniella R Mulinari
Keyword(s):  
Mechanical Properties ◽  
Tensile Properties ◽  
Mechanical Performance ◽  
Alkali Treatment ◽  
Mechanical Analysis ◽  
Melt Mixing ◽  
Polypropylene Composites ◽  
Matrix Interactions ◽  
Fiber Treatment ◽  
Fiber Matrix

Australian palm residues are generated by palm heart industry in large quantities and are considered an underused material with a composition rich in lignocellulosic structures. This residue is generally utilized as briquettes for energy or sheep feed; however, few works investigate this residue as composite fillers. This work aimed to revalue Australian palm residues (PR) by preparing polypropylene composites through melt mixing, using different fiber contents (0, 5, 10, 20, and 30 wt%), and evaluate the statistical influence of fibers (residues) alkali treatment (MPR) in composites mechanical properties. PR and MPR were evaluated by FTIR, XRD, SEM, TGA, and composites were assessed using thermal and mechanical analysis, in which ANOVA statistical analysis was applied. The residues addition increased the mechanical properties and their treatment enhanced the stiffness of the composites compared to pristine PP. However, ANOVA demonstrated that at low residues contents, surface treatment does not increase fiber-matrix interactions effectively, then tensile properties were statistically similar to PP. Considering tensile properties, 20% MPR showed statistically distinct properties, with significative enhancements; no filler contents dependence was verified. Flexural properties were more sensitive to residue loading, and composites with 30% PR and MPR presented superior mechanical performance. This difference is associated with a higher sensitivity of tensile stress towards fiber-matrix interactions, which was improved with fiber treatment. Also, the residues content and treatment influenced the composites' thermal stability, with better results for PP-MPR. Results indicate that palm residue is an excellent filler for improving composites' thermal and mechanical properties, with a greener character.

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