scholarly journals Microwave Pre-processing Effect on Pectin Yield from Citrus Raw Material

2020 ◽  
Author(s):  
Gennady Alekseev ◽  
Olga Egorova ◽  
Aleksey Egorov
Keyword(s):  
Classical Method ◽  
Raw Materials ◽  
Raw Material ◽  
Microwave Drying ◽  
Drying Methods ◽  
Microwave Exposure ◽  
Yield And Quality ◽  
Mineral Acids ◽  
Environmentally Friendly Method

The article describes a more environmentally friendly method to produce pectin compared to the classical acid scheme, which requires the use of strong mineral acids and toxic solvents. This method of obtaining pectin, like other analogs of the classical method, causes a decrease in the yield of the final product. This study aims to find ways of eliminating these barriers and increase the yield of pectin. The paper investigates the possibility to increase the yield of pectin obtained by acid hydrolysis applying citric acid through the use of preliminary microwave exposure to citrus raw materials. The work compares pectin quality indicators, such as the degree of esterification, molecular weight and gelation, for raw materials dried by the convective method and the combined method consisting of microwave pretreatment and blowing dry air. Curves of comparable pre-drying methods are presented. The rate of pectin yield at the stages of hydrolysis depending on the drying methods is analyzed. Optimal power modes for preliminary microwave drying of citrus raw materials are selected. The data obtained are valuable for both development and improvement of industrial technology of pectin production using environmental methods of extraction without the use of strong mineral acids to increase the yield and quality of pectin.

scholarly journals Pengaruh Kehalusan Bahan Dan Lama Ekstraksi Terhadap Mutu Ekstrak Tempuyung (Sonchus arvensis L.)

2017 ◽  
Vol 15 (2) ◽  
Author(s):  
Feri Manoi
Keyword(s):  
Traditional Medicine ◽  
Raw Materials ◽  
Water Extract ◽  
Raw Material ◽  
The Sun ◽  
Yield And Quality ◽  
Randomized Design ◽  
Sonchus Arvensis ◽  
Material Extraction

Utilization of medicinal plants both for health and treatment increased at this time. Number of Traditional Medicine Industry (IOT), Small Industries Traditional Medicine (IKOT) and Industrial Appliances (PIRT) is increasing. Thus the demand for raw materials is increasing, one of which is tempuyung. Good quality raw material in the form of crude drugs and extracts need to be considered as related to the efficacy and quality of products for further processing. The study aims to determine the effect size and the old material extraction to the yield and quality of the extract. Activity consists of two sub-activities (1). How to drying (a) the sun covered with black cloth, (b) the sun combination of tools, and (c) drier. Sub-activities (2) extraction technique which consists of two factors: the fineness of materials (20,40 and 60 mesh) and the second factor is the length of the extraction (2, 4, and 6 hours). The study design using factorial completely randomized design with three replications. Parameter observations consisted of yield bulbs, phytochemical screening, quality characteristics, extract yield, and quality extracts. The results showed levels of water extract Sonchus arvensis L. greater than the levels of alcohol cider. Quality simplicia Sonchus arvensis L. dried using a dryer is not different from the quality of the dried under the sun. Fineness of materials and time of extraction affects the yield of the extract Sonchus arvensis L Keywords: Subtlety material, extraction, quality

Industrial technologies for processing waste oils

2021 ◽  
pp. 44-57
Author(s):  
L. Stan'kovski ◽  
◽  
V.A. Dorogochinskaya ◽  
B.P. Tonkonogov ◽  
A.A. Molokanov ◽  
...  
Keyword(s):  
Raw Materials ◽  
Raw Material ◽  
Lubricating Oil ◽  
Yield And Quality ◽  
Waste Oils ◽  
The Russian Federation ◽  
Distillate Fractions ◽  
Material Preparation ◽  
Selection Of

A brief review of the state of collection, disposal and processing of used oils shows the availability of their resource in the country and the main trends in the organization of qualified collection, disposal and processing according to the lubricating oil version. The relevant technologies are given for individual stages and in general for enterprises, the choice of which depends on the quality and characteristics of raw materials. The advantage of the technological scheme, including coagulation purification at the stage of raw material preparation and vacuum distillation with the selection of distillate fractions and the residue, followed by additional purification of the residue, is shown. The use of this technology makes it possible to increase the yield and quality of the target product, which is practically impossible for the raw materials currently available in the Russian Federation using other technologies.

PENGARUH LAMA PENYULINGAN DAN KOMPOSISI BAHAN BAKU TERHADAP RENDEMEN DAN MUTU MINYAK ATSIRI DARI DAUN DAN BATANG NILAM (Pogostemon cablin Benth)

2012 ◽  
Vol 4 (2) ◽  
pp. 16
Author(s):  
A Sulaiman
Keyword(s):  
Essential Oil ◽  
Raw Materials ◽  
Raw Material ◽  
Composition Effect ◽  
High Quality ◽  
Yield And Quality ◽  
Pogostemon Cablin ◽  
Time Required ◽  
Better Than

The research of Distillation And Raw Material Composition Effect of Yield And Quality EssentialOil of Leaves And Stem Patchouli (Pogostemon cablin Benth). This study aimed to examine the influence of the length of distillation and composition of raw materials to the yield and quality of essential oil of patchouli leaves and stems to produce essential oils that have a high quality and yield. The time required to obtain the highest yield of patchouli oil is 8 hours, by composition of 100% leaf (1:0), that is equal to 3.631%, while the lowest yield of patchouli oil are produced from 100% stem (1:0) by distillation of 4 hours, in the amount of 0.10%. Composition that produces patchouli oil with the best quality is 100% stems (0:1) but that yield is lower, while the quality of patchouli oil produced by 100% leaf (1:0) and a mixture of leaf-stem (1:1) quality is still lower than the patchouli oil from the stem, but its yield is better than the yield of oil patchouli by 100% composition of the stem (0:1).Keywords:  essential oil, pogostemon cablin benth, yield

scholarly journals BIOSTIMULATOR MADE OF WASTE OF KERATIN-CONTAINING RAW MATERIALS

2020 ◽  
Vol 10 (1) ◽  
pp. 6-14
Author(s):  
Larisa Bryndina
Keyword(s):  
Amino Acids ◽  
Raw Materials ◽  
Maximum Yield ◽  
Raw Material ◽  
Natural Processes ◽  
Yield And Quality ◽  
Keratin Hydrolysis ◽  
The One ◽  
Hydrolysis Of

Ecosystem degradation forces us to introduce highly productive, environmentally friendly biotechnologies in agricultural production. In this regard, interest in organic farming is growing. Demand for organic products is ahead of supply. This, in its turn, causes interest in substances that, on the one hand, are safe for the environment, and on the other hand, increase yield and quality of crops. These substances include biostimulants. They stimulate the natural processes of assimilation of nutrients, increase stress resistance of plants. In this regard, keratin-containing raw materials deserve special attention, which, in terms of chemical composition, is a protein concentrate (90-95%) . But its use is limited due to the low functionality of the keratin protein of this raw material. Enzymatic keratin hydrolysis will provide a biostimulant for plants with a high content of amino acids. The aim of the study was to develop an enzymatic method for keratin hydrolysis with a high content of amino acids in the final product. Fermentation was carried out by Str. chromogeness.g. 0832 proteinase. The content of soluble protein, peptides and amino acids was carried out photocolorimetrically. Temperature (4000C) and pH (8.0) conditions of Str. chromogeness.g. 0832 enzyme complex have been determined, which allowed further hydrolysis of keratin-containing raw materials with a maximum yield of final products - amino acids (99.57 g/100g). Treatment of corn seeds with the obtained amino acid solution enabled to increase growth-promoting activity by 48%.

scholarly journals Prediksi Kadar Air Bubuk Biji Kakao Menggunakan Nirs Dengan Metode PLS

2016 ◽  
Vol 1 (1) ◽  
pp. 1069-1076
Author(s):  
Hasmayani Hasmayani ◽  
Rita Khathir ◽  
Mustafril Mustafril
Keyword(s):  
Refractive Index ◽  
Essential Oil ◽  
Specific Gravity ◽  
Raw Materials ◽  
Raw Material ◽  
Yield And Quality ◽  
Fresh Material ◽  
Index Value ◽  
Red Ginger

Abstrak. Minyak atsiri jahe merah merupakan salah satu komoditas dari hasil budidaya jahe merah. Jenis minyak ini didapatkan dengan cara penyulingan jahe merah yang berumur sekitar 10 bulan hingga 1 tahun. Penelitian ini bertujuan untuk mengetahui kajian pengkondisian bahan baku terhadap rendemen dan mutu minyak atsiri yang dihasilkan dari penyulingan jahe merah. Pengkondisian bahan baku jahe merah dilakukan dengan 2 taraf yaitu jahe merah segar dan jahe merah yang dikeringanginkan selama 24 jam dengan 2 kali ulangan. Hasil penelitian menunjukkan bahwa rendemen  minyak atsiri dari penyulingan jahe merah segar diperoleh 0,0705%, sedangkan rendemen pada penyulingan jahe merah dikeringanginkan 0,0435%. Hasil Nilai indeks bias minyak atsiri  jahe merah segar diperoleh sebesar 1,4885 sedangkan nilai indeks bias jahe merah dikeringanginkan diperoleh sebesar 1,4885. Nilai  bobot jenis minyak atsiri pada penyulingan jahe merah segar diperoleh sebesar 0,90423 dan bobot jenis minyak atsiri jahe merah yang dikeringanginkan sebesar 0,89679. Kelarutan dalam alkohol minyak atsiri jahe merah segar dan jahe merah dikeringanginkan jernih pada perbandingan 1:5.The study of raw material conditioning to the quality of the red ginger essential oil Abstract. Red ginger essential oil is one commodity from the cultivation of red ginger. These types of oils obtained by distillation of red ginger have old after 10 months to 1 year cultivation. This study aimed to determine the effect of raw materials conditioning to the yield and quality of essential oils produced. The raw materials conditioning  red ginger is done with two levels i.e fresh red ginger and air-dried red ginger about  24 hours under 2 repeated. The results showed that the yield of essential oil obtained by distillation of fresh red gingerwas  0.0705%, while the yield on the distillation of air- dried red was ginger 0.0435%. Refractive index value of red ginger essential oil from fresh  material was 1.4885  while  the refractive index of air-dried red ginger driedwas 1.4885. Furthermore, the specific grafity of  at the distillation of fresh red ginger obtained at 0.90423 and the specific gravity of red ginger essential oil is dried at 0.89679. Solubility in alcohol red ginger essential oil of fresh and dried red gingerwere clearly at a ratio of 1: 5. 

scholarly journals PROBLEMATICS OF CONSTRUCTION OF MATHEMATICAL MODELS OF THE PROCESS OF MICROWAVE DRYING OF SOY

2019 ◽  
pp. 21-26
Author(s):  
Valentyna Bandura ◽  
Oleksandr Popiak
Keyword(s):  
Mathematical Modeling ◽  
Mathematical Model ◽  
Raw Materials ◽  
Microwave Energy ◽  
Raw Material ◽  
Microwave Drying ◽  
Drying Methods ◽  
Soybean Seeds ◽  
Drying Process ◽  
Moisture Movement

The article reviews various techniques for mathematical modeling of the soybean drying process. The purpose of this paper is to review, analyze and compare existing approaches to mathematically describe the processes of moisture movement during microwave drying of soybeans. The only way to provide mathematical modeling of the processes occurring in the soybean grain is a combination of the transformation of microwave energy into heat, the heating of dipole water molecules existing in the seed, the processes of moving moisture from the center to the grain shell and evaporation of moisture. Today, microwave drying is one of the promising areas for research, because this method is much more efficient than traditional post-harvest grain drying methods and, at the same time, poorly understood. Factors on which the process of microwave drying depends on are the speed of movement of moisture in the micropores of the product, the initial temperature and humidity of the raw material, the placement of the main magnetron relative to the object of drying and the speed of movement of raw materials in the drying chamber. The object of the study in this article was to simplify the mathematical model of soybean seeds. To intensify the process of microwave drying, it is advisable to use a combined effect, such as blowing, which increases the intensity and quality of the process of microwave dehumidification. In addition, in this case, the simultaneous use of two or more factors of influence, which allows for rapid processing of raw materials. This determines the relevance and prospects of this study. The developed criteria criterion is substantiated and described, which allows to simplify the complex calculation of microwave energy transfer processes, sample heating and moisture velocity in it. The basic approaches to the construction of a mathematical model of the soybean drying process are considered, and their expediency is determined. The analysis of various methods of mathematical description of the drying process is carried out, the main disadvantages of these methods are identified. It is established that drying soybean seeds in the microwave field is one of the most promising. A mathematical model for a combined soybean drying process with a combination of microwave drying methods and air blowing is proposed.

TECHNOLOGICAL ASPECTS OF HIGH QUALITY RAW MATERIAL OBTAINING FOR PECTIN PRODUCTION

1970 ◽  
pp. 47-50
Author(s):  
I. A. Ilina ◽  
I. A. Machneva ◽  
E. S. Bakun
Keyword(s):  
Raw Materials ◽  
Thermal Characteristics ◽  
Environmental Safety ◽  
Raw Material ◽  
High Quality ◽  
Temperature Conductivity ◽  
Drying Temperature ◽  
Plant Raw Materials ◽  
Gel Forming Ability

  The article is devoted to the study of the chemical composition, physical and thermal-pfysical characteristics of damp apple pomaces and the identifying patterns of influence of drying temperature the functional composition and gel-forming ability of pectin. The research is aimed at obtaining initial data for the subsequent calculation of the main technological, hydro-mechanical, thermal, structural and economic characteristics of devices for drying the plant raw materials, ensuring the environmental safety and high quality of pectin-containing raw materials, the reducing heat and energy costs. As a result of the study of the thermal characteristics of apple pomaces, the critical points (temperature conductivity – 16.5 x 10-8 m2/s, thermal conductivity – 0.28 W/m K, heat capacity – 1627 j/(kg K)) at a humidity of 56 % are determined, which characterizing the transition from the extraction of weakly bound moisture to the extraction of moisture with strong bonds (colloidal, adsorption). It was found that the pomaces obtained from apples of late ripening have a higher content of solids (21-23 %), soluble pectin and protopectin (2.5-4.5 %). Dried pomaces obtained from apple varieties of late ripening contain up to 25 % pectin, which allow us to recommend them as a source of raw materials for the production of pectin. The optimum modes of preliminary washing of raw materials are offered, allowing to the remove the ballast substances as much as possible. It is established that when the drying temperature increases, the destructive processes are catalyzed: the strength of the pectin jelly and the uronide component and the degree of pectin esterification are reduced. The optimum drying temperature of damp apple pomaces is 80 0C, at which the quality of pectin extracted from the dried raw materials is maintained as much as possible. It is shown that the most effective for the pectin production is a fraction with a particle size of 3-5 mm, which allow us to extract up to 71 % of pectin from raw materials.

Phamacognostical and Pharmaceutical Evaluation of Chandrashakaladi Vataka - A herbal formulation

2016 ◽  
Vol 1 (3) ◽  
Author(s):  
Dr. Akash S Changole ◽  
Mandip Goyal ◽  
Harish CR
Keyword(s):  
Classical Method ◽  
Raw Materials ◽  
Herbal Medicines ◽  
Vital Role ◽  
Published Data ◽  
Herbal Formulation ◽  
Physico Chemical ◽  
Good Manufacturing Practices ◽  
Solvent Systems

Background: Quality control and the standardization of herbal medicines involve steps like standard source and quality of raw materials, good manufacturing practices and adequate analytical screening. These practices play a vital role in guaranting the quality and stability of herbal preparations. Chandrashakaladi Vataka is an Ayurvedic herbal formulation mentioned to be beneficial in Kushtha. Till date no published data is available on its analytical profile. Aim: To develop the Pharmacognostical and Phyto-chemical profile of Chandrashakaladi Vataka. Material and Methods: Chandrashakaladi Vataka was prepared as per classical method and analytical findings were recorded. Samples were subjected to organoleptic analysis, physico-chemical analysis and HPTLC examination by optimizing the solvent systems. Results and Conclusions: Pharmacognostical profile of Chandrashakaladi Vataka was established. Loss on drying, Ash value, Acid insoluble extract, Methanol soluble extract, Chandrashakaladi Vataka was found within prescribed limits. HPTLC profile of Chandrashakaladi Vataka revealed 12 spots at 254 nm and 13 spots at 366 nm.

scholarly journals A Methodology Based on FT-IR Data Combined with Random Forest Model to Generate Spectralprints for the Characterization of High-Quality Vinegars

Foods ◽  
2021 ◽  
Vol 10 (6) ◽  
pp. 1411
Author(s):  
José Luis P. Calle ◽  
Marta Ferreiro-González ◽  
Ana Ruiz-Rodríguez ◽  
Gerardo F. Barbero ◽  
José Á. Álvarez ◽  
...  
Keyword(s):  
Random Forest ◽  
Raw Materials ◽  
Principal Component ◽  
Hierarchical Cluster ◽  
Raw Material ◽  
Support Vector ◽  
Protected Designation Of Origin ◽  
Ft Ir

Sherry wine vinegar is a Spanish gourmet product under Protected Designation of Origin (PDO). Before a vinegar can be labeled as Sherry vinegar, the product must meet certain requirements as established by its PDO, which, in this case, means that it has been produced following the traditional solera and criadera ageing system. The quality of the vinegar is determined by many factors such as the raw material, the acetification process or the aging system. For this reason, mainly producers, but also consumers, would benefit from the employment of effective analytical tools that allow precisely determining the origin and quality of vinegar. In the present study, a total of 48 Sherry vinegar samples manufactured from three different starting wines (Palomino Fino, Moscatel, and Pedro Ximénez wine) were analyzed by Fourier-transform infrared (FT-IR) spectroscopy. The spectroscopic data were combined with unsupervised exploratory techniques such as hierarchical cluster analysis (HCA) and principal component analysis (PCA), as well as other nonparametric supervised techniques, namely, support vector machine (SVM) and random forest (RF), for the characterization of the samples. The HCA and PCA results present a clear grouping trend of the vinegar samples according to their raw materials. SVM in combination with leave-one-out cross-validation (LOOCV) successfully classified 100% of the samples, according to the type of wine used for their production. The RF method allowed selecting the most important variables to develop the characteristic fingerprint (“spectralprint”) of the vinegar samples according to their starting wine. Furthermore, the RF model reached 100% accuracy for both LOOCV and out-of-bag (OOB) sets.

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