LASER FLUORESCENCE OF SAND AND CLAY MATERIALS

1977 ◽  
Vol 57 (1) ◽  
pp. 1-8
Author(s):  
A. R. MACK ◽  
E. J. BRACH

Samples of granular materials illuminated with a 20 m Watt (average power) laser energy source at a wavelength of 337.1 nm differed in their fluorescence spectra over a wide range of wavelengths from approximately 380 to 660 nm. The fluorescent yield was usually higher with increased fineness of grain size and with increased concentration of clay (> 10% of under 2-μ grain size). However, sandy soils containing a low content of clay (i.e. < 10%) had a higher yield than the regression estimate. Modifying the fluorosensor for greater resolution at a higher energy level (1 nm bandwidth and 25 m Watt average power) resulted in eight discernible peaks between 384 and 440 nm, at 486 and at 550 nm. Overall fluorescence was markedly increased by removal of Fe coatings from the surface of the grains by a dithionite treatment. Thus, laser-induced fluorescence spectra obtained from various partially vegetated land areas by airborne laser fluorosensing may be influenced by the granular material associated with non-vegetated "open" areas.

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Raju Bheemanahalli ◽  
Montana Knight ◽  
Cherryl Quinones ◽  
Colleen J. Doherty ◽  
S. V. Krishna Jagadish

AbstractHigh night temperatures (HNT) are shown to significantly reduce rice (Oryza sativa L.) yield and quality. A better understanding of the genetic architecture of HNT tolerance will help rice breeders to develop varieties adapted to future warmer climates. In this study, a diverse indica rice panel displayed a wide range of phenotypic variability in yield and quality traits under control night (24 °C) and higher night (29 °C) temperatures. Genome-wide association analysis revealed 38 genetic loci associated across treatments (18 for control and 20 for HNT). Nineteen loci were detected with the relative changes in the traits between control and HNT. Positive phenotypic correlations and co-located genetic loci with previously cloned grain size genes revealed common genetic regulation between control and HNT, particularly grain size. Network-based predictive models prioritized 20 causal genes at the genetic loci based on known gene/s expression under HNT in rice. Our study provides important insights for future candidate gene validation and molecular marker development to enhance HNT tolerance in rice. Integrated physiological, genomic, and gene network-informed approaches indicate that the candidate genes for stay-green trait may be relevant to minimizing HNT-induced yield and quality losses during grain filling in rice by optimizing source-sink relationships.


2007 ◽  
Vol 558-559 ◽  
pp. 1283-1294 ◽  
Author(s):  
Cheng Xu ◽  
Z. Horita ◽  
Terence G. Langdon

It is now well-established that processing through the application of severe plastic deformation (SPD) leads to a significant reduction in the grain size of a wide range of metallic materials. This paper examines the fabrication of ultrafine-grained materials using high-pressure torsion (HPT) where this process is attractive because it leads to exceptional grain refinement with grain sizes that often lie in the nanometer or submicrometer ranges. Two aspects of HPT are examined. First, processing by HPT is usually confined to samples in the form of very thin disks but recent experiments demonstrate the potential for extending HPT also to bulk samples. Second, since the strains imposed in HPT vary with the distance from the center of the disk, it is important to examine the development of inhomogeneities in disk samples processed by HPT.


2017 ◽  
Vol 140 (2) ◽  
Author(s):  
Christopher G. Cooley ◽  
Tan Chai

This study investigates the vibration of and power harvested by typical electromagnetic and piezoelectric vibration energy harvesters when applied to vibrating host systems that rotate at constant speed. The governing equations for these electromechanically coupled devices are derived using Newtonian mechanics and Kirchhoff's voltage law. The natural frequency for these devices is speed-dependent due to the centripetal acceleration from their constant rotation. Resonance diagrams are used to identify excitation frequencies and speeds where these energy harvesters have large amplitude vibration and power harvested. Closed-form solutions are derived for the steady-state response and power harvested. These devices have multifrequency dynamic response due to the combined vibration and rotation of the host system. Multiple resonances are possible. The average power harvested over one oscillation cycle is calculated for a wide range of operating conditions. Electromagnetic devices have a local maximum in average harvested power that occurs near a specific excitation frequency and rotation speed. Piezoelectric devices, depending on their mechanical damping, can have two local maxima of average power harvested. Although these maxima are sensitive to small changes in the excitation frequency, they are much less sensitive to small changes in rotation speed.


2013 ◽  
Vol 19 (S4) ◽  
pp. 103-104
Author(s):  
C.B. Garcia ◽  
E. Ariza ◽  
C.J. Tavares

Zinc Oxide is a wide band-gap compound semiconductor that has been used in optoelectronic and photovoltaic applications due to its good electrical and optical properties. Aluminium has been an efficient n-type dopant for ZnO to produce low resistivity films and high transparency to visible light. In addition, the improvement of these properties also depends on the morphology, crystalline structure and deposition parameters. In this work, ZnO:Al films were produced by d.c. pulsed magnetron sputtering deposition from a ZnO ceramic target (2.0 wt% Al2O3) on glass substrates, at a temperature of 250 ºC.The crystallographic orientation of aluminum doped zinc oxide (ZnO:Al) thin films has been studied by Electron Backscatter Diffraction (EBSD) technique. EBSD coupled with Scanning Electron Microscopy (SEM) is a powerful tool for the microstructural and crystallographic characterization of a wide range of materials.The investigation by EBSD technique of such films presents some challenges since this analysis requires a flat and smooth surface. This is a necessary condition to avoid any shadow effects during the experiments performed with high tilting conditions (70º). This is also essential to ensure a good control of the three dimensional projection of the crystalline axes on the geometrical references related to the sample.Crystalline texture is described by the inverse pole figure (IPF) maps (Figure 1). Through EBSD analysis it was observed that the external surface of the film presents a strong texture on the basal plane orientation (grains highlighted in red colour). Furthermore it was possible to verify that the grain size strongly depends on the deposition time (Figure 1 (a) and (b)). The electrical and optical film properties improve with increasing of the grain size, which can be mainly, attributed to the decrease in scattering grain boundaries which leads to an increasing in carrier mobility (Figure 2).The authors kindly acknowledge the financial support from the Portuguese Foundation for Science and Technology (FCT) scientific program for the National Network of Electron Microscopy (RNME) EDE/1511/RME/2005.


2004 ◽  
Vol 5 (1) ◽  
pp. 43
Author(s):  
K.G. PEHLIVANOGLOU ◽  
G. TRONTSIOS ◽  
A. TSIRAMBIDES

The Thermaikos Gulf constitutes the NW part of the North Aegean Sea and is limited eastward from the Chalkidiki Peninsula and westward from the Pieria Prefecture. Its plateau covers an area of 3,500 km2. The mechanisms responsible for the grain size distribution into the Gulf, the clay mineralogy and the chemistry of some bottom sediments from the outer Thermaikos Gulf, are examined. Source mixing during transportation, flocculation, differential settling processes and organic matter appear to be the main mechanisms for the distribution of clay minerals in shallow waters. All grain size fractions studied present a wide range of values confirming the extreme variations of the discharged load and the variability in marine processes. Plagioclases predominate over K-feldspars, while quartz is the most abundant mineral present. In addition, micas, chlorites, amphiboles and pyroxenes exist as primary and/or accessory minerals in all samples. Among clay minerals, illite predominates over smectite and smectite over chlorite (+ kaolinite). The ordered interstratified phase of I/S, with 30-35% S layers, is present in the 2-0.25µm fraction. The randomly interstratified phase of I/S, with 50% S layers, is present in the <0.25& micro; m fraction. On average the clay mineral content of the studied samples is: 48% I, 23% S, 17% Ch (+K) and 12% others for the 2-0.25µm fraction and 50% I, 30% S and 20% Ch (+K) for the <0.25 µm fraction. All these minerals are the weathering products of the rocks from the drainage basins of the rivers flowing into the Gulf, as well as of the Neogene and Quaternary unconsolidated sediments of the surrounding coasts. The terrigenous input, the water mass circulation and, to a lesser extent, the quality of the discharged material and the differential settling of grains, control the grain size distribution within the outer Thermaikos Gulf. The chemical composition of the analysed samples is generally in agreement with their mineral composition and signifies their terrigenous origin presenting discretely clastic character.


2014 ◽  
Vol 2 (2) ◽  
pp. 1047-1092 ◽  
Author(s):  
M. Attal ◽  
S. M. Mudd ◽  
M. D. Hurst ◽  
B. Weinman ◽  
K. Yoo ◽  
...  

Abstract. The characteristics of the sediment transported by rivers (e.g., sediment flux, grain size distribution – GSD –) dictate whether rivers aggrade or erode their substrate. They also condition the architecture and properties of sedimentary successions in basins. In this study, we investigate the relationship between landscape steepness and the grain size of hillslope and fluvial sediments. The study area is located within the Feather River Basin in Northern California, and studied basins are underlain exclusively by tonalite lithology. Erosion rates in the study area vary over an order of magnitude, from > 250 mm ka−1 in the Feather River canyon to < 15 mm ka−1 on an adjacent low relief plateau. We find that the coarseness of hillslope sediment increases with increasing hillslope steepness and erosion rates. We hypothesize that, in our soil samples, the measured ten-fold increase in D50 and doubling of the amount of fragments larger than 1 mm when slope increases from 0.38 to 0.83 m m−1 is due to a decrease in the residence time of rock fragments, causing particles to be exposed for shorter periods of time to processes that can reduce grain size. For slopes in excess of 0.7 m m−1, landslides and scree cones supply much coarser sediment to rivers, with D50 and D84 more than one order of magnitude larger than in soils. In the tributary basins of the Feather River, a prominent break in slope developed in response to the rapid incision of the Feather River. Downstream of the break in slope, fluvial sediment grain size increases, due to an increase in flow competence (mostly driven by channel steepening) but also by a change in sediment source and in sediment dynamics: on the plateau upstream of the break in slope, rivers transport easily mobilised fine-grained sediment derived exclusively from soils. Downstream of the break in slope, mass wasting processes supply a wide range of grain sizes that rivers entrain selectively, depending on the competence of their flow. Our results also suggest that in this study site, hillslopes respond rapidly to an increase in the rate of base-level lowering compared to rivers.


2021 ◽  
Vol 5 (4) ◽  
pp. 152
Author(s):  
Shao-Heng He ◽  
Zhi Ding ◽  
Hai-Bo Hu ◽  
Min Gao

In this study, a series of nuclear magnetic resonance (NMR) tests was conducted on calcareous sand, quartz sand, and glass bead with a wide range of grain sizes, to understand the effect of grain size on the micro-pore structure and fractal characteristics of the carbonate-based sand and silicate-based sand. The pore size distribution (PSD) of the tested materials were obtained from the NMR T2 spectra, and fractal theory was introduced to describe the fractal properties of PSD. Results demonstrate that grain size has a significant effect on the PSD of carbonate-based sand and silicate-based sand. As grain size increases, the PSD of sands evolves from a binary structure with two peaks to a ternary structure with three peaks. The increase in the grain size can cause a remarkable increase in the maximum pore size. It is also found that the more irregular the particle shape, the better the continuity between the large and medium pores. In addition, grain size has a considerable effect on the fractal dimension of the micro-pore structure. The increase of grain size can lead to a significant increase in the heterogeneity and fractal dimension in PSD for calcareous sand, quartz sand and glass bead.


2015 ◽  
Vol 2015 ◽  
pp. 1-12 ◽  
Author(s):  
Ehab A. El-Danaf ◽  
Mahmoud S. Soliman ◽  
Ayman A. Al-Mutlaq

The effect of grain size and stacking fault energy (SFE) on the strain hardening rate behavior under plane strain compression (PSC) is investigated for pure Cu and binary Cu-Al alloys containing 1, 2, 4.7, and 7 wt. % Al. The alloys studied have a wide range of SFE from a low SFE of 4.5 mJm−2for Cu-7Al to a medium SFE of 78 mJm−2for pure Cu. A series of PSC tests have been conducted on these alloys for three average grain sizes of ~15, 70, and 250 μm. Strain hardening rate curves were obtained and a criterion relating twinning stress to grain size is established. It is concluded that the stress required for twinning initiation decreases with increasing grain size. Low values of SFE have an indirect influence on twinning stress by increasing the strain hardening rate which is reflected in building up the critical dislocation density needed to initiate mechanical twinning. A study on the effect of grain size on the intensity of the brass texture component for the low SFE alloys has revealed the reduction of the orientation density of that component with increasing grain size.


Materials ◽  
2018 ◽  
Vol 11 (12) ◽  
pp. 2590 ◽  
Author(s):  
Huafeng Liu ◽  
Kai Luo ◽  
Shihao Tang ◽  
Danhua Peng ◽  
Fangjing Hu ◽  
...  

Metamaterial-based absorbers have been extensively investigated in the terahertz (THz) range with ever increasing performances. In this paper, we propose an all-dielectric THz absorber based on doped silicon. The unit cell consists of a silicon cross resonator with an internal cross-shaped air cavity. Numerical results suggest that the proposed absorber can operate from THz to far-infrared regimes, having an average power absorption of ∼95% between 0.6 and 10 THz. Experimental results using THz time-domain spectroscopy show a good agreement with simulations. The underlying mechanisms for broadband absorption are attributed to the combined effects of multiple cavities modes formed by silicon resonators and bulk absorption in the doped silicon substrate, as confirmed by simulated field patterns and calculated diffraction efficiency. This ultra-wideband absorption is polarization insensitive and can operate across a wide range of the incident angle. The proposed absorber can be readily integrated into silicon-based photonic platforms and used for sensing, imaging, energy harvesting and wireless communications applications in the THz/IR range.


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